Method for estimating processability of a hydrocarbon-containing feedstock for hydroprocessing

Schabron, John F; Rovani, Joseph F

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Title: Method for estimating processability of a hydrocarbon-containing feedstock for hydroprocessing

Abstract

Disclosed herein is a method involving the steps of (a) precipitating an amount of asphaltenes from a liquid sample of a first hydrocarbon-containing feedstock having solvated asphaltenes therein with one or more first solvents in a column; (b) determining one or more solubility characteristics of the precipitated asphaltenes; (c) analyzing the one or more solubility characteristics of the precipitated asphaltenes; and (d) correlating a measurement of feedstock reactivity for the first hydrocarbon-containing feedstock sample with a mathematical parameter derived from the results of analyzing the one or more solubility characteristics of the precipitates asphaltenes. Determined parameters and processabilities for a plurality of feedstocks can be used to generate a mathematical relationship between parameter and processability; this relationship can be used to estimate the processability for hydroprocessing for a feedstock of unknown processability.

Inventors:: Schabron, John F; Rovani, Jr., Joseph F

Issue Date:: 2014-01-14

Research Org.:: The University of Wyoming Research Corporation, Laramie, WY, USA

Sponsoring Org.:: USDOE

OSTI Identifier:: 1117680

Patent Number(s):: 8628970

Application Number:: 13/909,780

Assignee:: The University of Wyoming Research Corporation (Laramie, WY)

Patent Classifications (CPCs):: C - CHEMISTRY C10 - PETROLEUM, GAS OR COKE INDUSTRIES C10G - CRACKING HYDROCARBON OILS

G - PHYSICS G01 - MEASURING G01N - INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES

Show more

C - CHEMISTRY C10 - PETROLEUM, GAS OR COKE INDUSTRIES C10G - CRACKING HYDROCARBON OILS
C10G7/12 - Controlling or regulating

G - PHYSICS G01 - MEASURING G01N - INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
G01N30/02 - Column chromatography
G01N33/28 - Oils {, i.e. hydrocarbon liquids}

Y - NEW / CROSS SECTIONAL TECHNOLOGIES Y10 - TECHNICAL SUBJECTS COVERED BY FORMER USPC Y10T - TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
Y10T436/116664 - with automated titrator
Y10T436/12 - Condition responsive control
Y10T436/21 - Hydrocarbon
Y10T436/212 - Aromatic
Y10T436/214 - Acyclic [e.g., methane, octane, isoparaffin, etc.]
Y10T436/255 - including use of a solid sorbent, semipermeable membrane, or liquid extraction
Y10T436/25625 - Dilution
Y10T436/2575 - Volumetric liquid transfer
Y10T436/25875 - Gaseous sample or with change of physical state

Show less

DOE Contract Number:: FC26-98FT40322

Resource Type:: Patent

Resource Relation:: Patent File Date: 2013 Jun 04

Country of Publication:: United States

Language:: English

Subject:: 37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CHEMISTRY

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                    Schabron, John F, and Rovani, Jr., Joseph F. Method for estimating processability of a hydrocarbon-containing feedstock for hydroprocessing.  United States: N. p., 2014. 
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                    Schabron, John F, & Rovani, Jr., Joseph F. Method for estimating processability of a hydrocarbon-containing feedstock for hydroprocessing.  United States.

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                    Schabron, John F, and Rovani, Jr., Joseph F. Tue .  
        "Method for estimating processability of a hydrocarbon-containing feedstock for hydroprocessing".  United States.  https://www.osti.gov/servlets/purl/1117680.

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@article{osti_1117680,

  title        = {Method for estimating processability of a hydrocarbon-containing feedstock for hydroprocessing},

  author       = {Schabron, John F and Rovani, Jr., Joseph F},

  abstractNote = {Disclosed herein is a method involving the steps of (a) precipitating an amount of asphaltenes from a liquid sample of a first hydrocarbon-containing feedstock having solvated asphaltenes therein with one or more first solvents in a column; (b) determining one or more solubility characteristics of the precipitated asphaltenes; (c) analyzing the one or more solubility characteristics of the precipitated asphaltenes; and (d) correlating a measurement of feedstock reactivity for the first hydrocarbon-containing feedstock sample with a mathematical parameter derived from the results of analyzing the one or more solubility characteristics of the precipitates asphaltenes. Determined parameters and processabilities for a plurality of feedstocks can be used to generate a mathematical relationship between parameter and processability; this relationship can be used to estimate the processability for hydroprocessing for a feedstock of unknown processability.},

  doi          = {},

  journal      = {},
number       = ,

  volume       = ,

  place        = {United States},

  year         = {2014},

  month        = {1}

}

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Works referencing / citing this record:

Low volume in-line filtration method for evaluation of asphaltenes for hydrocarbon-containing feedstock
patent, June 2017

Rogel, Estrella; Ovalles, Cesar; Moir, Michael E.
US Patent Document 9,671,384
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Methods for estimating properties of hydrocarbons comprising asphaltenes based on their solubility
patent, October 2016

Schabron, John F.; Rovani, Jr., Joseph F.
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Method for determining processability of a hydrocarbon containing feedstock

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Disclosed herein is a method involving the steps of (a) precipitating an amount of asphaltenes from a liquid sample of a first hydrocarbon-containing feedstock having solvated asphaltenes therein with one or more first solvents in a column; (b) determining one or more solubility characteristics of the precipitated asphaltenes; (c) analyzing the one or more solubility characteristics of the precipitated asphaltenes; and (d) correlating a measurement of feedstock reactivity for the first hydrocarbon-containing feedstock sample with a mathematical parameter derived from the results of analyzing the one or more solubility characteristics of the precipitated asphaltenes.
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Method for predicting fouling tendency of a hydrocarbon-containing feedstock

Patent Schabron, John F; Rovani, Jr., Joseph F

Disclosed herein is a method involving the steps of (a) precipitating an amount of asphaltenes from a liquid sample of a first hydrocarbon-containing feedstock having solvated asphaltenes therein with one or more first solvents in a column; (b) determining one or more solubility characteristics of the precipitated asphaltenes; (c) analyzing the one or more solubility characteristics of the precipitated asphaltenes; and (d) correlating a measurement of feedstock fouling tendency for the first hydrocarbon-containing feedstock sample with a mathematical parameter derived from the results of analyzing the one or more solubility characteristics of the precipitated asphaltenes.
Full Text Available
Systems and processes for conversion of ethylene feedstocks to hydrocarbon fuels

Patent Lilga, Michael A.; Hallen, Richard T.; Albrecht, Karl O.; ...

Systems, processes, and catalysts are disclosed for obtaining fuel and fuel blends containing selected ratios of open-chain and closed-chain fuel-range hydrocarbons suitable for production of alternate fuels including gasolines, jet fuels, and diesel fuels. Fuel-range hydrocarbons may be derived from ethylene-containing feedstocks and ethanol-containing feedstocks.
Full Text Available
Systems and processes for conversion of ethylene feedstocks to hydrocarbon fuels

Patent Lilga, Michael A.; Hallen, Richard T.; Albrecht, Karl O.; ...

Systems, processes, and catalysts are disclosed for obtaining fuels and fuel blends containing selected ratios of open-chain and closed-chain fuel-range hydrocarbons suitable for production of alternate fuels including gasolines, jet fuels, and diesel fuels. Fuel-range hydrocarbons may be derived from ethylene-containing feedstocks and ethanol-containing feedstocks.
Full Text Available
Systems and processes for conversion of ethylene feedstocks to hydrocarbon fuels

Patent Lilga, Michael A.; Hallen, Richard T.; Albrecht, Karl O.; ...

Systems, processes, and catalysts are disclosed for obtaining fuel and fuel blends containing selected ratios of open-chain and closed-chain fuel-range hydrocarbons suitable for production of alternate fuels including gasolines, jet fuels, and diesel fuels. Fuel-range hydrocarbons may be derived from ethylene-containing feedstocks and ethanol-containing feedstocks.
Full Text Available

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Title: Method for estimating processability of a hydrocarbon-containing feedstock for hydroprocessing

Abstract

Citation Formats

Selective separation of heavy oil using a mixture of polar and nonpolar solvents patent, January 1985

Optical method to study the stability of colloidal systems patent, December 1986

Sequential elution process patent, January 1987

Separation of oil into fractions of asphaltenes, resins, aromatics, and saturated hydrocarbons patent, September 1989

Method for spectroscopic analysis of hydrocarbons patent, January 1991

Method for determining the producibility of a hydrocarbon formation patent, February 1991

Process for separating extractable organic material from compositions comprising said extractable organic material intermixed with solids and water using a solvent mixture patent, March 1992

Method for determining thermodynamic and molecular properties in the liquid phase patent, November 1996

Cracking property determination patent, January 1999

Measurement and control of asphaltene agglomeration in hydrocarbon Liquids patent, October 1999

Predicting proximity to coke formation patent, August 2004

Processing and analysis techniques involving in-vessel material generation patent, January 2011

Processing and analysis techniques involving in-vessel material generation patent, August 2012

Processing and analysis techniques involving in-vessel material generation patent, September 2012

Method for determining asphaltene stability of a hydrocarbon-containing material patent, February 2013

Method for predicting fouling tendency of a hydrocarbon-containing feedstock patent, July 2013

Continuous on-line process control of residua distillation patent-application, November 2003

Method for Determining Asphaltene Stability of a Hydrocarbon-Containing Material patent-application, March 2011

Method for Predicting Reactivity of a Hydrocarbon-Containing Feedstock for Hydroprocessing patent-application, March 2011

Processing and Analysis Techniques Involving In-Vessel Material Generation patent-application, May 2011

Processing and Analysis Techniques Involving In-Vessel Material Generation patent-application, January 2012

Methods for Predicting Fouling Tendencies of Hydrocarbon Containing Feedstocks patent-application, June 2012

Aggregation of asphaltenes as determined by calorimetry journal, March 1991

Acoustic method for measuring asphaltene flocculation in crude oils journal, September 2000

Thermal cracking of petroleum residues: 1. Kinetic analysis of the reaction journal, January 1993

Ultrasonic Measurements in Particle Size Analysis book, September 2006

Viscosity/Concentration Relationships for Emulsions journal, October 1989

Relationships Between Asphaltenes, Heithaus Compatibility Parameters, and Asphalt Viscosity journal, October 1998

Equilibria in Non-electrolyte Solutions in Relation to the Vapor Pressures and Densities of the Components. journal, April 1931

The Solubility and Three-Dimensional Structure of Asphaltenes journal, March 1998

Molecular weight polarity map for residua pyrolysis journal, March 2001

Non-pyrolytic heat induced deposition from heavy oils journal, May 2001

Residua coke formation predictability maps journal, December 2002

Predicting coke formation tendencies journal, August 2001

Characteristic changes of asphaltenes during visbreaking of North Gujarat short residue journal, March 1990

Some factors affecting the solubility of polymers journal, February 1953

A phase-separation kinetic model for coke formation journal, November 1993

Two-Dimensional Solubility Parameter Mapping of Heavy oils journal, January 1996

Initial studies using ultrasonic spectroscopy for monitoring changes in residua with pyrolysis journal, October 2006

Kinetic models for the thermal cracking of Athabasca bitumen journal, May 1985

Precipitation-redissolution liquid chromatography of styrene-ethyl acrylate copolymers journal, August 1999

Influence of Vine Vigor on Grape ( Vitis vinifera L. Cv. Pinot Noir) Anthocyanins. 2. Anthocyanins and Pigmented Polymers in Wine journal, August 2007

Determination of Saturate, Aromatic, Resin, and Asphaltenic (SARA) Components in Crude Oils by Means of Infrared and Near-Infrared Spectroscopy journal, September 2001

Composition of asphalt based on generic fractionation, using solvent deasphaltening, elution-adsorption chromatography, and densimetric characterization journal, April 1969

Rapid and Accurate SARA Analysis of Medium Gravity Crude Oils journal, November 2002

On-column precipitation and re-dissolution of asphaltenes in petroleum residua journal, February 2008

Ion-exchange, coordination, and adsorption chromatographic separation of heavy-end petroleum distillates journal, July 1972

TLC–FID (Iatroscan) analysis of heavy oil and tar sand samples journal, August 2008

Analysis of petroleum fractions by TLC-FID: applications to petroleum reservoir description journal, January 1991

Issues with Comparing SARA Methodologies journal, November 2007

Dynamics of Bitumen Fractions by Thin-Layer Chromatography/Flame Ionization Detection journal, July 2001

Preparative hydrocarbon group type determination by automated medium pressure liquid chromatography journal, March 1980

The Oil Compatibility Model and Crude Oil Incompatibility journal, December 1999

Determination of Asphaltenes in Crude Oil and Petroleum Products by the on Column Precipitation Method journal, September 2009

Characterization of Heavy Crude Oils, Their Fractions, and Hydrovisbroken Products by the Asphaltene Solubility Fraction Method journal, December 2011

Adsorption of Athabasca Vacuum Residues and Their Visbroken Products over Macroporous Solids: Influence of Their Molecular Characteristics journal, September 2011

Asphaltene Chemical Characterization as a Function of Solubility: Effects on Stability and Aggregation journal, December 2011

Waxphaltene Determinator Method for Automated Precipitation and Redissolution of Wax and Asphaltene Components journal, March 2012

Reactivity of Fluid Catalytic Cracking Feedstocks as a Function of Reactive Hydrogen Content journal, January 2004

456. A new chromatographic procedure and its application to high polymers journal, January 1956

Fouling of a Sweet Crude Oil under Inert and Oxygenated Conditions journal, January 2000

Thermodynamic Model of Sediment Deposition in the LC-FINING Process † journal, September 2008

Low volume in-line filtration method for evaluation of asphaltenes for hydrocarbon-containing feedstock patent, June 2017

Methods for estimating properties of hydrocarbons comprising asphaltenes based on their solubility patent, October 2016

Selective separation of heavy oil using a mixture of polar and nonpolar solvents
patent, January 1985

Optical method to study the stability of colloidal systems
patent, December 1986

Sequential elution process
patent, January 1987

Separation of oil into fractions of asphaltenes, resins, aromatics, and saturated hydrocarbons
patent, September 1989

Method for spectroscopic analysis of hydrocarbons
patent, January 1991

Method for determining the producibility of a hydrocarbon formation
patent, February 1991

Process for separating extractable organic material from compositions comprising said extractable organic material intermixed with solids and water using a solvent mixture
patent, March 1992

Method for determining thermodynamic and molecular properties in the liquid phase
patent, November 1996

Cracking property determination
patent, January 1999

Measurement and control of asphaltene agglomeration in hydrocarbon Liquids
patent, October 1999

Predicting proximity to coke formation
patent, August 2004

Processing and analysis techniques involving in-vessel material generation
patent, January 2011

Processing and analysis techniques involving in-vessel material generation
patent, August 2012

Processing and analysis techniques involving in-vessel material generation
patent, September 2012

Method for determining asphaltene stability of a hydrocarbon-containing material
patent, February 2013

Method for predicting fouling tendency of a hydrocarbon-containing feedstock
patent, July 2013

Continuous on-line process control of residua distillation
patent-application, November 2003

Method for Determining Asphaltene Stability of a Hydrocarbon-Containing Material
patent-application, March 2011

Method for Predicting Reactivity of a Hydrocarbon-Containing Feedstock for Hydroprocessing
patent-application, March 2011

Processing and Analysis Techniques Involving In-Vessel Material Generation
patent-application, May 2011

Processing and Analysis Techniques Involving In-Vessel Material Generation
patent-application, January 2012

Methods for Predicting Fouling Tendencies of Hydrocarbon Containing Feedstocks
patent-application, June 2012

Aggregation of asphaltenes as determined by calorimetry
journal, March 1991

Acoustic method for measuring asphaltene flocculation in crude oils
journal, September 2000

Thermal cracking of petroleum residues: 1. Kinetic analysis of the reaction
journal, January 1993

Ultrasonic Measurements in Particle Size Analysis
book, September 2006

Viscosity/Concentration Relationships for Emulsions
journal, October 1989

Relationships Between Asphaltenes, Heithaus Compatibility Parameters, and Asphalt Viscosity
journal, October 1998

Equilibria in Non-electrolyte Solutions in Relation to the Vapor Pressures and Densities of the Components.
journal, April 1931

The Solubility and Three-Dimensional Structure of Asphaltenes
journal, March 1998

Molecular weight polarity map for residua pyrolysis
journal, March 2001

Non-pyrolytic heat induced deposition from heavy oils
journal, May 2001

Residua coke formation predictability maps
journal, December 2002

Predicting coke formation tendencies
journal, August 2001

Characteristic changes of asphaltenes during visbreaking of North Gujarat short residue
journal, March 1990

Some factors affecting the solubility of polymers
journal, February 1953

A phase-separation kinetic model for coke formation
journal, November 1993

Two-Dimensional Solubility Parameter Mapping of Heavy oils
journal, January 1996

Initial studies using ultrasonic spectroscopy for monitoring changes in residua with pyrolysis
journal, October 2006

Kinetic models for the thermal cracking of Athabasca bitumen
journal, May 1985

Precipitation-redissolution liquid chromatography of styrene-ethyl acrylate copolymers
journal, August 1999

Influence of Vine Vigor on Grape ( Vitis vinifera L. Cv. Pinot Noir) Anthocyanins. 2. Anthocyanins and Pigmented Polymers in Wine
journal, August 2007

Determination of Saturate, Aromatic, Resin, and Asphaltenic (SARA) Components in Crude Oils by Means of Infrared and Near-Infrared Spectroscopy
journal, September 2001

Composition of asphalt based on generic fractionation, using solvent deasphaltening, elution-adsorption chromatography, and densimetric characterization
journal, April 1969

Rapid and Accurate SARA Analysis of Medium Gravity Crude Oils
journal, November 2002

On-column precipitation and re-dissolution of asphaltenes in petroleum residua
journal, February 2008

Ion-exchange, coordination, and adsorption chromatographic separation of heavy-end petroleum distillates
journal, July 1972

TLC–FID (Iatroscan) analysis of heavy oil and tar sand samples
journal, August 2008

Analysis of petroleum fractions by TLC-FID: applications to petroleum reservoir description
journal, January 1991

Issues with Comparing SARA Methodologies
journal, November 2007

Dynamics of Bitumen Fractions by Thin-Layer Chromatography/Flame Ionization Detection
journal, July 2001

Preparative hydrocarbon group type determination by automated medium pressure liquid chromatography
journal, March 1980

The Oil Compatibility Model and Crude Oil Incompatibility
journal, December 1999

Determination of Asphaltenes in Crude Oil and Petroleum Products by the on Column Precipitation Method
journal, September 2009

Characterization of Heavy Crude Oils, Their Fractions, and Hydrovisbroken Products by the Asphaltene Solubility Fraction Method
journal, December 2011

Adsorption of Athabasca Vacuum Residues and Their Visbroken Products over Macroporous Solids: Influence of Their Molecular Characteristics
journal, September 2011

Asphaltene Chemical Characterization as a Function of Solubility: Effects on Stability and Aggregation
journal, December 2011

Waxphaltene Determinator Method for Automated Precipitation and Redissolution of Wax and Asphaltene Components
journal, March 2012

Reactivity of Fluid Catalytic Cracking Feedstocks as a Function of Reactive Hydrogen Content
journal, January 2004

456. A new chromatographic procedure and its application to high polymers
journal, January 1956

Fouling of a Sweet Crude Oil under Inert and Oxygenated Conditions
journal, January 2000

Thermodynamic Model of Sediment Deposition in the LC-FINING Process ^†
journal, September 2008

Low volume in-line filtration method for evaluation of asphaltenes for hydrocarbon-containing feedstock
patent, June 2017

Methods for estimating properties of hydrocarbons comprising asphaltenes based on their solubility
patent, October 2016