Devices for collecting chemical compounds
Abstract
A device for sampling chemical compounds from fixed surfaces and related methods are disclosed. The device may include a vacuum source, a chamber and a sorbent material. The device may utilize vacuum extraction to volatilize the chemical compounds from a fixed surface so that they may be sorbed by the sorbent material. The sorbent material may then be analyzed using conventional thermal desorption/gas chromatography/mass spectrometry (TD/GC/MS) instrumentation to determine presence of the chemical compounds. The methods may include detecting release and presence of one or more chemical compounds and determining the efficacy of decontamination. The device may be useful in collection and analysis of a variety of chemical compounds, such as residual chemical warfare agents, chemical attribution signatures and toxic industrial chemicals.
- Inventors:
- Issue Date:
- Research Org.:
- Idaho National Lab. (INL), Idaho Falls, ID (United States)
- Sponsoring Org.:
- USDOE
- OSTI Identifier:
- 1111477
- Patent Number(s):
- 8613233
- Application Number:
- 13/104,853
- Assignee:
- Battelle Energy Alliance, LLC (Idaho Falls, ID)
- Patent Classifications (CPCs):
-
G - PHYSICS G01 - MEASURING G01N - INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- DOE Contract Number:
- AC07-05ID14517
- Resource Type:
- Patent
- Country of Publication:
- United States
- Language:
- English
- Subject:
- 47 OTHER INSTRUMENTATION
Citation Formats
Scott, Jill R, and Groenewold, Gary S. Devices for collecting chemical compounds. United States: N. p., 2013.
Web.
Scott, Jill R, & Groenewold, Gary S. Devices for collecting chemical compounds. United States.
Scott, Jill R, and Groenewold, Gary S. Tue .
"Devices for collecting chemical compounds". United States. https://www.osti.gov/servlets/purl/1111477.
@article{osti_1111477,
title = {Devices for collecting chemical compounds},
author = {Scott, Jill R and Groenewold, Gary S},
abstractNote = {A device for sampling chemical compounds from fixed surfaces and related methods are disclosed. The device may include a vacuum source, a chamber and a sorbent material. The device may utilize vacuum extraction to volatilize the chemical compounds from a fixed surface so that they may be sorbed by the sorbent material. The sorbent material may then be analyzed using conventional thermal desorption/gas chromatography/mass spectrometry (TD/GC/MS) instrumentation to determine presence of the chemical compounds. The methods may include detecting release and presence of one or more chemical compounds and determining the efficacy of decontamination. The device may be useful in collection and analysis of a variety of chemical compounds, such as residual chemical warfare agents, chemical attribution signatures and toxic industrial chemicals.},
doi = {},
journal = {},
number = ,
volume = ,
place = {United States},
year = {2013},
month = {12}
}
Works referenced in this record:
Recovery of phosphonate surface contaminants from glass using a simple vacuum extractor with a solid-phase microextraction fiber
journal, July 2011
- Groenewold, Gary S.; Scott, Jill R.; Rae, Catherine
- Analytica Chimica Acta, Vol. 697, Issue 1-2
Detection of gas-phase chemical warfare agents using field-portable gas chromatography–mass spectrometry systems: instrument and sampling strategy considerations
journal, April 2004
- Smith, Philip A.; Koch, David; Hook, Gary L.
- TrAC Trends in Analytical Chemistry, Vol. 23, Issue 4