System and method for conditioning a hardwood pulp liquid hydrolysate
Abstract
A system and method for hardwood pulp liquid hydrolysate conditioning includes a first evaporator receives a hardwood mix extract and outputting a quantity of vapor and extract. A hydrolysis unit receives the extract, hyrolyzes and outputs to a lignin separation device, which separates and recovers a quantity of lignin. A neutralization device receives extract from the lignin separation device and a neutralizing agent, producing a mixture of solid precipitate and a fifth extract. The solid precipitate is removed from the fifth extract. A second evaporator removes a quantity of acid from the fifth extract in a vapor form. This vapor may be recycled to improve total acid recovery or discarded. A desalination device receives the diluted extract, separates out some of the acid and salt and outputs a desalinated solution.
- Inventors:
- Issue Date:
- Research Org.:
- Red Shield Acquisition, LLC, Old Town, ME, USA
- Sponsoring Org.:
- USDOE
- OSTI Identifier:
- 1111122
- Patent Number(s):
- 8608970
- Application Number:
- 13/187,818
- Assignee:
- Red Shield Acquisition, LLC (Old Town, ME); University of Maine System Board of Trustees (Bangor, ME)
- Patent Classifications (CPCs):
-
C - CHEMISTRY C13 - SUGAR INDUSTRY C13K - SACCHARIDES, OTHER THAN SUCROSE, OBTAINED FROM NATURAL SOURCES OR BY HYDROLYSIS OF NATURALLY OCCURRING DI-, OLIGO- OR POLYSACCHARIDES
D - TEXTILES D21 - PAPER-MAKING D21C - PRODUCTION OF CELLULOSE BY REMOVING NON-CELLULOSE SUBSTANCES FROM CELLULOSE-CONTAINING MATERIALS
- DOE Contract Number:
- EE0003364
- Resource Type:
- Patent
- Country of Publication:
- United States
- Language:
- English
- Subject:
- 37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CHEMISTRY
Citation Formats
Waite, Darrell M, Arnold, Richard, St. Pierre, James, Pendse, Hemant P, and Ceckler, William H. System and method for conditioning a hardwood pulp liquid hydrolysate. United States: N. p., 2013.
Web.
Waite, Darrell M, Arnold, Richard, St. Pierre, James, Pendse, Hemant P, & Ceckler, William H. System and method for conditioning a hardwood pulp liquid hydrolysate. United States.
Waite, Darrell M, Arnold, Richard, St. Pierre, James, Pendse, Hemant P, and Ceckler, William H. Tue .
"System and method for conditioning a hardwood pulp liquid hydrolysate". United States. https://www.osti.gov/servlets/purl/1111122.
@article{osti_1111122,
title = {System and method for conditioning a hardwood pulp liquid hydrolysate},
author = {Waite, Darrell M and Arnold, Richard and St. Pierre, James and Pendse, Hemant P and Ceckler, William H},
abstractNote = {A system and method for hardwood pulp liquid hydrolysate conditioning includes a first evaporator receives a hardwood mix extract and outputting a quantity of vapor and extract. A hydrolysis unit receives the extract, hyrolyzes and outputs to a lignin separation device, which separates and recovers a quantity of lignin. A neutralization device receives extract from the lignin separation device and a neutralizing agent, producing a mixture of solid precipitate and a fifth extract. The solid precipitate is removed from the fifth extract. A second evaporator removes a quantity of acid from the fifth extract in a vapor form. This vapor may be recycled to improve total acid recovery or discarded. A desalination device receives the diluted extract, separates out some of the acid and salt and outputs a desalinated solution.},
doi = {},
journal = {},
number = ,
volume = ,
place = {United States},
year = {Tue Dec 17 00:00:00 EST 2013},
month = {Tue Dec 17 00:00:00 EST 2013}
}
Works referenced in this record:
Bei hydrolysis process system an improved process for the continuous hydrolysis saccharification of ligno-cellulosics in a two-stage plug-flow-reactor system
patent, May 1995
- Brelsford, Donald L.
- US Patent Document 5,411,594
Production of prehydrolyzed pulp
patent, December 1996
- Tikka, Panu; Kovasin, Kari
- US Patent Document 5,589,033
Process for the production of organic products from diverse biomass sources
patent, June 2002
- Lombard, Charles K.
- US Patent Document 6,409,841
Method for removing acids from an aqueous acid-containing xylose solution
patent, July 1978
- Pfeiffer, Hans Jorg; Rene, Keller; Erich, Frank
- US Patent Document 4,102,705
Methods of saccharification of polysaccharides in plants
patent-application, April 2011
- Howard, John; Fake, Gina
- US Patent Application 12/901507; 20110097786
Technical Economic Evaluation of a Hardwood Biorefinery Using the "Near-Neutral" Hemicellulose Pre-Extraction Process
journal, June 2008
- Mao, H.; Genco, J. M.; Yoon, S. -H.
- Journal of Biobased Materials and Bioenergy, Vol. 2, Issue 2
Pretreatment process for conversion of cellulose to fuel ethanol
patent, June 1999
- Foody, Brian; Tolan, Jeffrey S.; Bernstein, Jerome D.
- US Patent Document 5,916,780
Method of processing lignocellulosic feedstock for enhanced xylose and ethanol production
patent, March 2011
- Griffin, Robert; Nicholson, Colin; Mott, Corinne
- US Patent Document 7,901,511
Method of producing calcium salts from biomass
patent, November 1993
- Oehr, Klaus H.; Scott, Donald S.; Czernik, Stefan
- US Patent Document 5,264,623
Process for extracting sugar from cellulose and cellulosic materials
patent, July 1981
- Whittingham, Barron S.
- US Patent Document 4,278,471
Wood pulping with acetic acid with the addition of formic acid
patent, October 2000
- Nimz, Horst Harry Hermann; Schone, Martin
- US Patent Document 6,139,683
Enzymatic hydrolysis of biomass material
patent, May 1997
- Brink, David L.
- US Patent Document 5,628,830
Biorefinery Process for Extraction, Separation, and Recovery of Fermentable Saccharides, other Useful Compounds, and Yield of Improved Lignocellulosic Material from Plant Biomass
patent-application, June 2011
- Howard, Joel R.; Amidon, Thomas E.; Liu, Shijie
- US Patent Application 12/850662; 20110129886
Integrated process for separation of lignocellulosic components to fermentable sugars for production of ethanol and chemicals
patent-application, March 2008
- Nguyen, Xuan Nghinh
- US Patent Application 11/700718; 20080057555
Pretreatment process for conversion of cellulose to fuel ethanol
patent, July 2000
- Foody, Brian; Tolan, Jeffrey S.; Bernstein, Jerome D.
- US Patent Document 6,090,595
Method of producing glucose from papermaking sludge using concentrated or dilute acid hydrolysis
patent, March 1999
- Klyosov, Anatole; Philippidis, George P.; James, Alan M.
- US Patent Document 5,876,505
Process for producing cinnamic acid from 1,1,1,3-tetrachloro-3-phenylpropane
patent, February 1989
- Hajek, Milan; Silhavy, Premysl
- US Patent Document 4,806,681
Fermentation of lignocellulosic hydrolysates. I: inhibition and detoxification
journal, August 2000
- Palmqvist, Eva; Hahn-Hägerdal, Bärbel
- Bioresource Technology, Vol. 74, Issue 1, p. 17-24
Method and Apparatus for Transforming Waste Into Fuel Ethanol
patent-application, February 2011
- Lehr, Larry L.
- US Patent Application 12/856920; 20110039318
