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Title: System and method for conditioning a hardwood pulp liquid hydrolysate

Abstract

A system and method for hardwood pulp liquid hydrolysate conditioning includes a first evaporator receives a hardwood mix extract and outputting a quantity of vapor and extract. A hydrolysis unit receives the extract, hyrolyzes and outputs to a lignin separation device, which separates and recovers a quantity of lignin. A neutralization device receives extract from the lignin separation device and a neutralizing agent, producing a mixture of solid precipitate and a fifth extract. The solid precipitate is removed from the fifth extract. A second evaporator removes a quantity of acid from the fifth extract in a vapor form. This vapor may be recycled to improve total acid recovery or discarded. A desalination device receives the diluted extract, separates out some of the acid and salt and outputs a desalinated solution.

Inventors:
; ; ; ;
Issue Date:
Research Org.:
Red Shield Acquisition, LLC, Old Town, ME, USA
Sponsoring Org.:
USDOE
OSTI Identifier:
1111122
Patent Number(s):
8608970
Application Number:
13/187,818
Assignee:
Red Shield Acquisition, LLC (Old Town, ME); University of Maine System Board of Trustees (Bangor, ME)
Patent Classifications (CPCs):
C - CHEMISTRY C13 - SUGAR INDUSTRY C13K - SACCHARIDES, OTHER THAN SUCROSE, OBTAINED FROM NATURAL SOURCES OR BY HYDROLYSIS OF NATURALLY OCCURRING DI-, OLIGO- OR POLYSACCHARIDES
D - TEXTILES D21 - PAPER-MAKING D21C - PRODUCTION OF CELLULOSE BY REMOVING NON-CELLULOSE SUBSTANCES FROM CELLULOSE-CONTAINING MATERIALS
DOE Contract Number:  
EE0003364
Resource Type:
Patent
Country of Publication:
United States
Language:
English
Subject:
37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CHEMISTRY

Citation Formats

Waite, Darrell M, Arnold, Richard, St. Pierre, James, Pendse, Hemant P, and Ceckler, William H. System and method for conditioning a hardwood pulp liquid hydrolysate. United States: N. p., 2013. Web.
Waite, Darrell M, Arnold, Richard, St. Pierre, James, Pendse, Hemant P, & Ceckler, William H. System and method for conditioning a hardwood pulp liquid hydrolysate. United States.
Waite, Darrell M, Arnold, Richard, St. Pierre, James, Pendse, Hemant P, and Ceckler, William H. Tue . "System and method for conditioning a hardwood pulp liquid hydrolysate". United States. https://www.osti.gov/servlets/purl/1111122.
@article{osti_1111122,
title = {System and method for conditioning a hardwood pulp liquid hydrolysate},
author = {Waite, Darrell M and Arnold, Richard and St. Pierre, James and Pendse, Hemant P and Ceckler, William H},
abstractNote = {A system and method for hardwood pulp liquid hydrolysate conditioning includes a first evaporator receives a hardwood mix extract and outputting a quantity of vapor and extract. A hydrolysis unit receives the extract, hyrolyzes and outputs to a lignin separation device, which separates and recovers a quantity of lignin. A neutralization device receives extract from the lignin separation device and a neutralizing agent, producing a mixture of solid precipitate and a fifth extract. The solid precipitate is removed from the fifth extract. A second evaporator removes a quantity of acid from the fifth extract in a vapor form. This vapor may be recycled to improve total acid recovery or discarded. A desalination device receives the diluted extract, separates out some of the acid and salt and outputs a desalinated solution.},
doi = {},
journal = {},
number = ,
volume = ,
place = {United States},
year = {Tue Dec 17 00:00:00 EST 2013},
month = {Tue Dec 17 00:00:00 EST 2013}
}

Works referenced in this record:

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patent, December 1996


Method for removing acids from an aqueous acid-containing xylose solution
patent, July 1978


Methods of saccharification of polysaccharides in plants
patent-application, April 2011


Technical Economic Evaluation of a Hardwood Biorefinery Using the "Near-Neutral" Hemicellulose Pre-Extraction Process
journal, June 2008


Pretreatment process for conversion of cellulose to fuel ethanol
patent, June 1999


Method of producing calcium salts from biomass
patent, November 1993


Wood pulping with acetic acid with the addition of formic acid
patent, October 2000


Pretreatment process for conversion of cellulose to fuel ethanol
patent, July 2000


Method of producing glucose from papermaking sludge using concentrated or dilute acid hydrolysis
patent, March 1999


Fermentation of lignocellulosic hydrolysates. I: inhibition and detoxification
journal, August 2000


Method and Apparatus for Transforming Waste Into Fuel Ethanol
patent-application, February 2011