Melt-castable energetic compounds comprising oxadiazoles and methods of production thereof

Pagoria, Philip F; Zhang, Mao X

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Title: Melt-castable energetic compounds comprising oxadiazoles and methods of production thereof

Abstract

In one embodiment, a melt-castable energetic material comprises at least one of: 3,5-bis(4-nitro-1,2,5-oxadiazol-3-yl)-1,2,4-oxadiazole (DNFO), and 3-(4-amino-1,2,5-oxadiazol-3-yl)-5-(4-nitro-1,2,5-oxadiazol-3-yl)-1,2- ,4-oxadiazole (ANFO). In another embodiment, a method for forming a melt-castable energetic material includes reacting 3,5-bis(4-amino-1,2,5-oxadiazol-3-yl)-1,2,4-oxadiazole (DAFO) with oxygen or an oxygen-containing compound to form a mixture of at least: DNFO, and ANFO.

Inventors:: Pagoria, Philip F; Zhang, Mao X

Issue Date:: 2013-11-12

Research Org.:: Lawrence Livermore National Laboratory (LLNL), Livermore, CA (United States)

Sponsoring Org.:: USDOE

OSTI Identifier:: 1108600

Patent Number(s):: 8580054

Application Number:: 13/439,780

Assignee:: Lawrence Livermore National Security, LLC (Livermore, CA)

Patent Classifications (CPCs):: C - CHEMISTRY C06 - EXPLOSIVES C06B - EXPLOSIVES OR THERMIC COMPOSITIONS

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C - CHEMISTRY C06 - EXPLOSIVES C06B - EXPLOSIVES OR THERMIC COMPOSITIONS
C06B21/005 - {By a process involving melting at least part of the ingredients}
C06B25/34 - the compound being a nitrated acyclic, alicyclic or heterocyclic amine

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DOE Contract Number:: AC52-07NA27344

Resource Type:: Patent

Country of Publication:: United States

Language:: English

Subject:: 36 MATERIALS SCIENCE

Citation Formats


                    Pagoria, Philip F, and Zhang, Mao X. Melt-castable energetic compounds comprising oxadiazoles and methods of production thereof.  United States: N. p., 2013. 
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                    Pagoria, Philip F, & Zhang, Mao X. Melt-castable energetic compounds comprising oxadiazoles and methods of production thereof.  United States.

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                    Pagoria, Philip F, and Zhang, Mao X. Tue .  
        "Melt-castable energetic compounds comprising oxadiazoles and methods of production thereof".  United States.  https://www.osti.gov/servlets/purl/1108600.

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@article{osti_1108600,

  title        = {Melt-castable energetic compounds comprising oxadiazoles and methods of production thereof},

  author       = {Pagoria, Philip F and Zhang, Mao X},

  abstractNote = {In one embodiment, a melt-castable energetic material comprises at least one of: 3,5-bis(4-nitro-1,2,5-oxadiazol-3-yl)-1,2,4-oxadiazole (DNFO), and 3-(4-amino-1,2,5-oxadiazol-3-yl)-5-(4-nitro-1,2,5-oxadiazol-3-yl)-1,2- ,4-oxadiazole (ANFO). In another embodiment, a method for forming a melt-castable energetic material includes reacting 3,5-bis(4-amino-1,2,5-oxadiazol-3-yl)-1,2,4-oxadiazole (DAFO) with oxygen or an oxygen-containing compound to form a mixture of at least: DNFO, and ANFO.},

  doi          = {},

  journal      = {},
number       = ,

  volume       = ,

  place        = {United States},

  year         = {2013},

  month        = {11}

}

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Title: Melt-castable energetic compounds comprising oxadiazoles and methods of production thereof

Abstract

Citation Formats

<title>Subsurface imaging using the spectral polarization difference technique and NIR illumination</title> conference, July 1999

15N NMR study of the mechanism of the reaction of amidoximes with nitrites in the presence of ZnCl2 and HCl journal, April 1994

Aberrant porphyrin metabolism in hepatocellular carcinoma journal, April 1984

New synthesis of 1,2,4-oxadiazoles journal, January 1990

Heme biosynthesis in human breast cancer—mimetic “in vitro” studies and some heme enzymic activity levels journal, January 1990

Method for detecting cancerous tissue using optical spectroscopy and fourier analysis patent, June 1998

Endoscope system using normal light and fluorescence patent, February 2007

Destruction of erythroleukaemic cells by photoactivation of endogenous porphyrins journal, November 1987

Characteristics of large-sized Ce:YAG scintillation crystal grown by temperature gradient technique journal, June 2003

Recent developments in neutron detection journal, April 2000

Signal enhancement for fluorescence microscopy patent, January 2001

Near-infrared spectroscopic tissue imaging for medical applications patent, March 2006

Autofluorescence characteristics of immortalized and carcinogen-transformed human bronchial epithelial cells journal, January 2001

Endoscope system patent, November 2002

Endoscope with LED illumination patent, May 2004

Autofluorescence detection and imaging of bladder cancer realized through a cystoscope patent, August 2007

Solution-grown crystals for neutron radiation detectors, and methods of solution growth patent, June 2012

Imaging apparatus patent, August 2004

Growth, optical, thermal and mechanical studies of methyl 4-hydroxybenzoate single crystals journal, August 2003

Endodiagnostic method using differential thermal relaxation and IR imaging patent, December 1999

Method for determining if tissue is malignant as opposed to non-malignant using time-resolved fluorescence spectroscopy patent, November 1995

Linked list traversal with reduced memory accesses patent, April 2011

Apparatus for measuring neutrons and gamma rays patent, November 1984

Stereo laparoscope with synchronized optics patent, November 1999

A convenient synthesis of 3-substituted 5-guanidino-1,2,4-oxadiazoles journal, January 1994

Endoscope patent, September 2005

Tissue imaging for cancer detection using NIR autofluorescence conference, May 2002

Laser induced fluorescence spectroscopy from native cancerous and normal tissue journal, December 1984

Solid scintillator counting compositions patent, September 1987

Synthesis and properties of 4-amino-3-cyanofurazan journal, May 1994

Method for determining if tissue is malignant as opposed to non-malignant using time-resolved fluorescence spectroscopy patent, September 1994

Therapeutic laser device and method including noninvasive subsurface monitoring and controlling means patent, July 2002

Spectroradiometric Apparatus And Method For Measuring Radiation patent, June 1974

Synthesis of 2-amino-5-(5R-1,2,4-oxadiazolyl-3)-1,3,4-oxadiazoles journal, December 1993

Diagnostic apparatus for intrinsic fluorescence of malignant tumor patent, September 1990

Scintillation substances (variants) patent-application, April 2006

Image processing apparatus patent, February 2006

Development of organic scintillators journal, June 1979

Imaging system with automatic gain control for reflectance and fluorescence endoscopy patent, October 2002

Imaging of objects based upon the polarization or depolarization of light patent, December 1998

Omniview motionless camera endoscopy system patent, May 1994

Cell death genes of Drosophila melanogaster and vertebrate analogs patent, January 1997

Apparatus for performing hyperspectral endoscopy patent, March 2003

Endoscope for imaging infrared emissions within the range of 2 to 14 microns patent, November 1998

Scintillation Detection in Well Logging Using Fast and Slow Phosphors patent, December 1963

Spectroscopic Diagnosis Of Colonic Dysplasia journal, June 1991

Compounds for neutron radiation detectors and systems thereof patent, June 2013

Method for determining if a tissue is a malignant tumor tissue, a benign tumor tissue, or a normal or benign tissue using Raman spectroscopy patent, November 1993

Method and apparatus for distinguishing cancerous tissue from benign tumor tissue, benign tissue or normal tissue using native fluorescence patent, July 1992

Multi-modal optical tissue diagnostic system patent, December 2005

Medical imaging, diagnosis, and therapy using a scanning single optical fiber system patent, December 2005

Simultaneous Acquisition of Differing Image Types patent-application, October 2008

Secure document reader and method therefor patent, July 2001

Scanning endoscope patent-application, January 2005

Solution-Grown Crystals For Neutron Radiation Detectors, And Methods Of Solution Growth patent-application, December 2012

Hyperspectral microscope for in vivo imaging of microstructures and cells in tissues patent, May 2011

Dual mode real-time screening and rapid full-area, selective-spectral, remote imaging and analysis device and process patent-application, August 2003

Photon-sorting spectroscopic microscope system patent, February 2004

Method and apparatus for detecting cancerous tissue using luminescence excitation spectra patent, August 1991

Process for producing single crystal of gallium-containing nitride patent-application, August 2007

Method of simultaneously applying multiple illumination schemes for simultaneous image acquisition in an imaging system patent-application, October 2001

Spectroscopic diagnostic methods and system patent-application, December 2003

<title>Subsurface imaging using the spectral polarization difference technique and NIR illumination</title>
conference, July 1999

15N NMR study of the mechanism of the reaction of amidoximes with nitrites in the presence of ZnCl2 and HCl
journal, April 1994

Aberrant porphyrin metabolism in hepatocellular carcinoma
journal, April 1984

New synthesis of 1,2,4-oxadiazoles
journal, January 1990

Heme biosynthesis in human breast cancer—mimetic “in vitro” studies and some heme enzymic activity levels
journal, January 1990

Method for detecting cancerous tissue using optical spectroscopy and fourier analysis
patent, June 1998

Endoscope system using normal light and fluorescence
patent, February 2007

Destruction of erythroleukaemic cells by photoactivation of endogenous porphyrins
journal, November 1987

Characteristics of large-sized Ce:YAG scintillation crystal grown by temperature gradient technique
journal, June 2003

Recent developments in neutron detection
journal, April 2000

Signal enhancement for fluorescence microscopy
patent, January 2001

Near-infrared spectroscopic tissue imaging for medical applications
patent, March 2006

Autofluorescence characteristics of immortalized and carcinogen-transformed human bronchial epithelial cells
journal, January 2001

Endoscope system
patent, November 2002

Endoscope with LED illumination
patent, May 2004

Autofluorescence detection and imaging of bladder cancer realized through a cystoscope
patent, August 2007

Solution-grown crystals for neutron radiation detectors, and methods of solution growth
patent, June 2012

Imaging apparatus
patent, August 2004

Growth, optical, thermal and mechanical studies of methyl 4-hydroxybenzoate single crystals
journal, August 2003

Endodiagnostic method using differential thermal relaxation and IR imaging
patent, December 1999

Method for determining if tissue is malignant as opposed to non-malignant using time-resolved fluorescence spectroscopy
patent, November 1995

Linked list traversal with reduced memory accesses
patent, April 2011

Apparatus for measuring neutrons and gamma rays
patent, November 1984

Stereo laparoscope with synchronized optics
patent, November 1999

A convenient synthesis of 3-substituted 5-guanidino-1,2,4-oxadiazoles
journal, January 1994

Endoscope
patent, September 2005

Tissue imaging for cancer detection using NIR autofluorescence
conference, May 2002

Laser induced fluorescence spectroscopy from native cancerous and normal tissue
journal, December 1984

Solid scintillator counting compositions
patent, September 1987

Synthesis and properties of 4-amino-3-cyanofurazan
journal, May 1994

Method for determining if tissue is malignant as opposed to non-malignant using time-resolved fluorescence spectroscopy
patent, September 1994

Therapeutic laser device and method including noninvasive subsurface monitoring and controlling means
patent, July 2002

Spectroradiometric Apparatus And Method For Measuring Radiation
patent, June 1974

Synthesis of 2-amino-5-(5R-1,2,4-oxadiazolyl-3)-1,3,4-oxadiazoles
journal, December 1993

Diagnostic apparatus for intrinsic fluorescence of malignant tumor
patent, September 1990

Scintillation substances (variants)
patent-application, April 2006

Image processing apparatus
patent, February 2006

Development of organic scintillators
journal, June 1979

Imaging system with automatic gain control for reflectance and fluorescence endoscopy
patent, October 2002

Imaging of objects based upon the polarization or depolarization of light
patent, December 1998

Omniview motionless camera endoscopy system
patent, May 1994

Cell death genes of Drosophila melanogaster and vertebrate analogs
patent, January 1997

Apparatus for performing hyperspectral endoscopy
patent, March 2003

Endoscope for imaging infrared emissions within the range of 2 to 14 microns
patent, November 1998

Scintillation Detection in Well Logging Using Fast and Slow Phosphors
patent, December 1963

Spectroscopic Diagnosis Of Colonic Dysplasia
journal, June 1991

Compounds for neutron radiation detectors and systems thereof
patent, June 2013

Method for determining if a tissue is a malignant tumor tissue, a benign tumor tissue, or a normal or benign tissue using Raman spectroscopy
patent, November 1993

Method and apparatus for distinguishing cancerous tissue from benign tumor tissue, benign tissue or normal tissue using native fluorescence
patent, July 1992

Multi-modal optical tissue diagnostic system
patent, December 2005

Medical imaging, diagnosis, and therapy using a scanning single optical fiber system
patent, December 2005

Simultaneous Acquisition of Differing Image Types
patent-application, October 2008

Secure document reader and method therefor
patent, July 2001

Scanning endoscope
patent-application, January 2005

Solution-Grown Crystals For Neutron Radiation Detectors, And Methods Of Solution Growth
patent-application, December 2012

Hyperspectral microscope for in vivo imaging of microstructures and cells in tissues
patent, May 2011

Dual mode real-time screening and rapid full-area, selective-spectral, remote imaging and analysis device and process
patent-application, August 2003

Photon-sorting spectroscopic microscope system
patent, February 2004

Method and apparatus for detecting cancerous tissue using luminescence excitation spectra
patent, August 1991

Process for producing single crystal of gallium-containing nitride
patent-application, August 2007

Method of simultaneously applying multiple illumination schemes for simultaneous image acquisition in an imaging system
patent-application, October 2001

Spectroscopic diagnostic methods and system
patent-application, December 2003