Surface sampling concentration and reaction probe

Van Berkel, Gary J; Elnaggar, Mariam S

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Title: Surface sampling concentration and reaction probe

Abstract

A method of analyzing a chemical composition of a specimen is described. The method can include providing a probe comprising an outer capillary tube and an inner capillary tube disposed co-axially within the outer capillary tube, where the inner and outer capillary tubes define a solvent capillary and a sampling capillary in fluid communication with one another at a distal end of the probe; contacting a target site on a surface of a specimen with a solvent in fluid communication with the probe; maintaining a plug volume proximate a solvent-specimen interface, wherein the plug volume is in fluid communication with the probe; draining plug sampling fluid from the plug volume through the sampling capillary; and analyzing a chemical composition of the plug sampling fluid with an analytical instrument. A system for performing the method is also described.

Inventors:: Van Berkel, Gary J; Elnaggar, Mariam S

Issue Date:: 2013-07-16

Research Org.:: Oak Ridge National Laboratory (ORNL), Oak Ridge, TN (United States)

Sponsoring Org.:: USDOE

OSTI Identifier:: 1087878

Patent Number(s):: 8486703

Application Number:: 12/894,872

Assignee:: UT-Battelle, LLC (Oak Ridge, TN)

Patent Classifications (CPCs):: G - PHYSICS G01 - MEASURING G01N - INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES

Y - NEW / CROSS SECTIONAL TECHNOLOGIES Y10 - TECHNICAL SUBJECTS COVERED BY FORMER USPC Y10T - TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION

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G - PHYSICS G01 - MEASURING G01N - INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
G01N1/02 - Devices for withdrawing samples
G01N1/32 - Polishing
G01N2001/028 - {Sampling from a surface, swabbing, vaporising}
G01N2001/383 - {collecting and diluting in a flow of liquid}

Y - NEW / CROSS SECTIONAL TECHNOLOGIES Y10 - TECHNICAL SUBJECTS COVERED BY FORMER USPC Y10T - TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
Y10T436/117497 - with a continuously flowing sample or carrier stream
Y10T436/118339 - with formation of a segmented stream
Y10T436/25 - including sample preparation
Y10T436/2575 - Volumetric liquid transfer

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DOE Contract Number:: AC05-00OR22725

Resource Type:: Patent

Country of Publication:: United States

Language:: English

Subject:: 37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CHEMISTRY

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                    Van Berkel, Gary J, and Elnaggar, Mariam S. Surface sampling concentration and reaction probe.  United States: N. p., 2013. 
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                    Van Berkel, Gary J, & Elnaggar, Mariam S. Surface sampling concentration and reaction probe.  United States.

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                    Van Berkel, Gary J, and Elnaggar, Mariam S. Tue .  
        "Surface sampling concentration and reaction probe".  United States.  https://www.osti.gov/servlets/purl/1087878.

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@article{osti_1087878,

  title        = {Surface sampling concentration and reaction probe},

  author       = {Van Berkel, Gary J and Elnaggar, Mariam S},

  abstractNote = {A method of analyzing a chemical composition of a specimen is described. The method can include providing a probe comprising an outer capillary tube and an inner capillary tube disposed co-axially within the outer capillary tube, where the inner and outer capillary tubes define a solvent capillary and a sampling capillary in fluid communication with one another at a distal end of the probe; contacting a target site on a surface of a specimen with a solvent in fluid communication with the probe; maintaining a plug volume proximate a solvent-specimen interface, wherein the plug volume is in fluid communication with the probe; draining plug sampling fluid from the plug volume through the sampling capillary; and analyzing a chemical composition of the plug sampling fluid with an analytical instrument. A system for performing the method is also described.},

  doi          = {},

  journal      = {},
number       = ,

  volume       = ,

  place        = {United States},

  year         = {2013},

  month        = {7}

}

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Title: Surface sampling concentration and reaction probe

Abstract

Citation Formats

Disposable Containers and Utensils for Sanitizing patent-application, October 2009

Hollow nanoparticle generation on laser-induced cavitation bubbles via bubble interface pinning journal, September 2010

Laser ablation in liquids: Applications in the synthesis of nanocrystals journal, May 2007

Direct flow injection analysis nebulization electrospray and APCI mass spectrometry patent-application, November 2002

Disposable combination cup and base patent, September 1989

Laser desorption—electrospray ion (ESI) source for mass spectrometers patent, April 2009

Automated Analysis Of Complex Matrices Using Mass Spectrometer patent-application, June 2007

Method and apparatus for continuous sample deposition on sample support plates for liquid chromatography-matrix-assisted laser desorption/ionization mass spectrometry patent-application, February 2004

Methods and compositions for assessing a sample by maldi mass spectrometry patent-application, August 2005

Transmission studies of explosive vaporization of a transparent liquid film on an opaque solid surface induced by excimer‐laser‐pulsed irradiation journal, September 1992

Methods for mass spectrometry detection and quantification of specific target proteins in complex biological samples patent, November 2008

Apparatus and method for isolating a nucleic acid from a sample patent-application, June 2008

Methods and devices for concentration and purification of analytes for chemical analysis including matrix-assisted laser desorption/ionization (MALDI) mass spectrometry (MS) patent-application, June 2005

Method for selective removal of a material from a wafer's alignment marks patent, December 1993

Pulsed laser‐induced desorption and optical imaging on a nanometer scale with scanning near‐field microscopy using chemically etched fiber tips journal, April 1996

Evidence of near-field laser ablation inductively coupled plasma mass spectrometry (NF-LA-ICP-MS) at nanometre scale for elemental and isotopic analysis on gels and biological samples journal, January 2006

Differential Hemolysis of a Whole Blood Sample patent-application, October 2009

Mass Spectrometry With Laser Ablation patent-application, June 2008

Composite analyzer tester patent, May 1988

Towards Nanoscale Molecular Analysis at Atmospheric Pressure by a Near-Field Laser Ablation Ion Trap/Time-of-Flight Mass Spectrometer journal, September 2008

Sampling probe for microarray read out using electrospray mass spectrometry patent, October 2004

Recyclable corrugated beverage container and holder patent, April 1993

Optical reflectance and scattering studies of nucleation and growth of bubbles at a liquid-solid interface induced by pulsed laser heating journal, March 1993

Possibility of nano-local element analysis by near-field laser ablation inductively coupled plasma mass spectrometry (LA-ICP-MS): New experimental arrangement and first application journal, June 2008

Electrospray-Assisted Laser-Induced Acoustic Desorption Ionization Mass Spectrometer and a Method for Mass Spectrometry patent-application, December 2008

Beverage Pod patent-application, October 2011

Quantitative Analysis of Surface-Derived Samples using Mass Spectrometry patent-application, November 2007

Disposable beverage container patent, February 1988

Laser desorption - electrospray ion (ESI) source for mass spectrometers patent-application, November 2008

Method of Preparing Sample for Matrix-Assisted Laser Desorption Ionization Mass Spectrometry and Matrix-Assisted Laser Desorption Ionization Mass Spectrometry patent-application, February 2010

Method and system for formation and withdrawal of a sample from a surface to be analyzed patent-application, September 2010

Increasing Ionization Efficiency in Mass Spectroscopy patent-application, May 2009

Field enhancement in apertureless near-field scanning optical microscopy journal, January 2001

Near-Field Scanning Optical Microscopy journal, October 1999

Laser ablation in liquids as a new technique of sampling in elemental analysis of solid materials journal, February 2009

Device for Processing a Biological And/or Chemical Sample and Method of Using the Same patent-application, February 2009

Miniaturized fluid transfer device patent, November 2002

High power laser induced acoustic desorption probe patent-application, December 2007

System and method for on-line coupling of liquid capillary separations with matrix-assisted laser desorption/ionization mass spectrometry patent, October 2000

Ion Generation Using Wetted Porous Material patent-application, May 2012

Protein crystallization in microfluidic structures patent, June 2002

Detection of malaria parasites by mass spectrometry patent, September 2007

Means and method for analyzing samples by mass spectrometry patent-application, September 2007

Near-Field Optical Microscopy and Spectroscopy with Pointed Probes journal, May 2006

Method and apparatus for etch of a specific subarea of a semiconductor work object patent, September 2001

Microsecond-resolved imaging of laser ablation at solid–liquid interface: investigation of formation process of nano-size metal colloids journal, May 2004

Method and apparatus for the quantitative measurement of the corrosivity effect of residues present on the surface of electronic circuit assemblies patent, July 1998

Mass spectroscopic reaction-monitoring method patent, May 2010

Looking at the nanoscale: scanning near-field optical microscopy journal, February 2003

Bubble nucleation and pressure generation during laser cleaning of surfaces journal, April 1997

Container and method of making a container patent-application, December 2005

Multi-function laser induced breakdown spectroscopy and laser ablation material analysis system and method patent-application, March 2007

Methods for Molecular Nanoanalysis journal, November 2006

Nanoscale Atmospheric Pressure Laser Ablation-Mass Spectrometry journal, April 2001

Interface members and holders for microfluidic array devices patent, March 2005

Sampling probe for microarray read out using electrospray mass spectrometry patent-application, October 2003

Methods and apparatus for ink delivery to nanolithographic probe systems patent, July 2010

The irradiation effect of a Nd–YAG pulsed laser on the CeO2 target in the liquid journal, January 2004

Disposable Containers and Utensils for Sanitizing
patent-application, October 2009

Hollow nanoparticle generation on laser-induced cavitation bubbles via bubble interface pinning
journal, September 2010

Laser ablation in liquids: Applications in the synthesis of nanocrystals
journal, May 2007

Direct flow injection analysis nebulization electrospray and APCI mass spectrometry
patent-application, November 2002

Disposable combination cup and base
patent, September 1989

Laser desorption—electrospray ion (ESI) source for mass spectrometers
patent, April 2009

Automated Analysis Of Complex Matrices Using Mass Spectrometer
patent-application, June 2007

Method and apparatus for continuous sample deposition on sample support plates for liquid chromatography-matrix-assisted laser desorption/ionization mass spectrometry
patent-application, February 2004

Methods and compositions for assessing a sample by maldi mass spectrometry
patent-application, August 2005

Transmission studies of explosive vaporization of a transparent liquid film on an opaque solid surface induced by excimer‐laser‐pulsed irradiation
journal, September 1992

Methods for mass spectrometry detection and quantification of specific target proteins in complex biological samples
patent, November 2008

Apparatus and method for isolating a nucleic acid from a sample
patent-application, June 2008

Methods and devices for concentration and purification of analytes for chemical analysis including matrix-assisted laser desorption/ionization (MALDI) mass spectrometry (MS)
patent-application, June 2005

Method for selective removal of a material from a wafer's alignment marks
patent, December 1993

Pulsed laser‐induced desorption and optical imaging on a nanometer scale with scanning near‐field microscopy using chemically etched fiber tips
journal, April 1996

Evidence of near-field laser ablation inductively coupled plasma mass spectrometry (NF-LA-ICP-MS) at nanometre scale for elemental and isotopic analysis on gels and biological samples
journal, January 2006

Differential Hemolysis of a Whole Blood Sample
patent-application, October 2009

Mass Spectrometry With Laser Ablation
patent-application, June 2008

Composite analyzer tester
patent, May 1988

Towards Nanoscale Molecular Analysis at Atmospheric Pressure by a Near-Field Laser Ablation Ion Trap/Time-of-Flight Mass Spectrometer
journal, September 2008

Sampling probe for microarray read out using electrospray mass spectrometry
patent, October 2004

Recyclable corrugated beverage container and holder
patent, April 1993

Optical reflectance and scattering studies of nucleation and growth of bubbles at a liquid-solid interface induced by pulsed laser heating
journal, March 1993

Possibility of nano-local element analysis by near-field laser ablation inductively coupled plasma mass spectrometry (LA-ICP-MS): New experimental arrangement and first application
journal, June 2008

Electrospray-Assisted Laser-Induced Acoustic Desorption Ionization Mass Spectrometer and a Method for Mass Spectrometry
patent-application, December 2008

Beverage Pod
patent-application, October 2011

Quantitative Analysis of Surface-Derived Samples using Mass Spectrometry
patent-application, November 2007

Disposable beverage container
patent, February 1988

Laser desorption - electrospray ion (ESI) source for mass spectrometers
patent-application, November 2008

Method of Preparing Sample for Matrix-Assisted Laser Desorption Ionization Mass Spectrometry and Matrix-Assisted Laser Desorption Ionization Mass Spectrometry
patent-application, February 2010

Method and system for formation and withdrawal of a sample from a surface to be analyzed
patent-application, September 2010

Increasing Ionization Efficiency in Mass Spectroscopy
patent-application, May 2009

Field enhancement in apertureless near-field scanning optical microscopy
journal, January 2001

Near-Field Scanning Optical Microscopy
journal, October 1999

Laser ablation in liquids as a new technique of sampling in elemental analysis of solid materials
journal, February 2009

Device for Processing a Biological And/or Chemical Sample and Method of Using the Same
patent-application, February 2009

Miniaturized fluid transfer device
patent, November 2002

High power laser induced acoustic desorption probe
patent-application, December 2007

System and method for on-line coupling of liquid capillary separations with matrix-assisted laser desorption/ionization mass spectrometry
patent, October 2000

Ion Generation Using Wetted Porous Material
patent-application, May 2012

Protein crystallization in microfluidic structures
patent, June 2002

Detection of malaria parasites by mass spectrometry
patent, September 2007

Means and method for analyzing samples by mass spectrometry
patent-application, September 2007

Near-Field Optical Microscopy and Spectroscopy with Pointed Probes
journal, May 2006

Method and apparatus for etch of a specific subarea of a semiconductor work object
patent, September 2001

Microsecond-resolved imaging of laser ablation at solid–liquid interface: investigation of formation process of nano-size metal colloids
journal, May 2004

Method and apparatus for the quantitative measurement of the corrosivity effect of residues present on the surface of electronic circuit assemblies
patent, July 1998

Mass spectroscopic reaction-monitoring method
patent, May 2010

Looking at the nanoscale: scanning near-field optical microscopy
journal, February 2003

Bubble nucleation and pressure generation during laser cleaning of surfaces
journal, April 1997

Container and method of making a container
patent-application, December 2005

Multi-function laser induced breakdown spectroscopy and laser ablation material analysis system and method
patent-application, March 2007

Methods for Molecular Nanoanalysis
journal, November 2006

Nanoscale Atmospheric Pressure Laser Ablation-Mass Spectrometry
journal, April 2001

Interface members and holders for microfluidic array devices
patent, March 2005

Sampling probe for microarray read out using electrospray mass spectrometry
patent-application, October 2003

Methods and apparatus for ink delivery to nanolithographic probe systems
patent, July 2010

The irradiation effect of a Nd–YAG pulsed laser on the CeO₂ target in the liquid
journal, January 2004