Systems and methods for using a boehmite bond-coat with polyimide membranes for gas separation

Polishchuk, Kimberly Ann

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Title: Systems and methods for using a boehmite bond-coat with polyimide membranes for gas separation

Abstract

The subject matter disclosed herein relates to gas separation membranes and, more specifically, to polyimide gas separation membranes. In an embodiment, a gas separation membrane includes a porous substrate, a substantially continuous polyimide membrane layer, and one or more layers of boehmite nanoparticles disposed between the porous substrate and the polyimide membrane layer to form a bond-coat layer. The bond-coat layer is configured to improve the adhesion of the polyimide membrane layer to the porous substrate, and the polyimide membrane layer has a thickness approximately 100 nm or less.

Inventors:: Polishchuk, Kimberly Ann

Issue Date:: Tue Mar 05 00:00:00 EST 2013

Research Org.:: Idaho National Laboratory (INL), Idaho Falls, ID (United States)

Sponsoring Org.:: USDOE

OSTI Identifier:: 1083467

Patent Number(s):: 8388744

Application Number:: 13/221,657

Assignee:: General Electric Company (Schenectady, NY)

Patent Classifications (CPCs):: B - PERFORMING OPERATIONS B01 - PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL B01D - SEPARATION

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B - PERFORMING OPERATIONS B01 - PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL B01D - SEPARATION
B01D53/228 - {characterised by specific membranes}
B01D69/105 - {Support pretreatment}
B01D71/64 - Polyimides

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DOE Contract Number:: AC07-05ID14517

Resource Type:: Patent

Country of Publication:: United States

Language:: English

Subject:: 37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CHEMISTRY

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                    Polishchuk, Kimberly Ann. Systems and methods for using a boehmite bond-coat with polyimide membranes for gas separation.  United States: N. p., 2013. 
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                    Polishchuk, Kimberly Ann. Systems and methods for using a boehmite bond-coat with polyimide membranes for gas separation.  United States.

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                    Polishchuk, Kimberly Ann. Tue .  
        "Systems and methods for using a boehmite bond-coat with polyimide membranes for gas separation".  United States.  https://www.osti.gov/servlets/purl/1083467.

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@article{osti_1083467,

  title        = {Systems and methods for using a boehmite bond-coat with polyimide membranes for gas separation},

  author       = {Polishchuk, Kimberly Ann},

  abstractNote = {The subject matter disclosed herein relates to gas separation membranes and, more specifically, to polyimide gas separation membranes. In an embodiment, a gas separation membrane includes a porous substrate, a substantially continuous polyimide membrane layer, and one or more layers of boehmite nanoparticles disposed between the porous substrate and the polyimide membrane layer to form a bond-coat layer. The bond-coat layer is configured to improve the adhesion of the polyimide membrane layer to the porous substrate, and the polyimide membrane layer has a thickness approximately 100 nm or less.},

  doi          = {},

  journal      = {},
number       = ,

  volume       = ,

  place        = {United States},

  year         = {Tue Mar 05 00:00:00 EST 2013},

  month        = {Tue Mar 05 00:00:00 EST 2013}

}

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A method of producing hydrogen from sodium hydroxide and water is disclosed. The method comprises separating sodium from a first aqueous sodium hydroxide stream in a sodium ion separator, feeding the sodium produced in the sodium ion separator to a sodium reactor, reacting the sodium in the sodium reactor with water, and producing a second aqueous sodium hydroxide stream and hydrogen. The method may also comprise reusing the second aqueous sodium hydroxide stream by combining the second aqueous sodium hydroxide stream with the first aqueous sodium hydroxide stream. A system of producing hydrogen is also disclosed.
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Membranes, methods of making membranes, and methods of separating gases using membranes

Patent Ho, W. S. Winston

Membranes, methods of making membranes, and methods of separating gases using membranes are provided. The membranes can include at least one hydrophilic polymer, at least one cross-linking agent, at least one base, and at least one amino compound. The methods of separating gases using membranes can include contacting a gas stream containing at least one of CO.sub.2, H.sub.2S, and HCl with one side of a nonporous and at least one of CO.sub.2, H.sub.2S, and HCl selectively permeable membrane such that at least one of CO.sub.2, H.sub.2S, and HCl is selectively transported through the membrane.
Full Text Available
Gas Separation Using Organic-Vapor-Resistent Membranes In Conjunctin With Organic-Vapor-Selective Membranes

Patent Baker, Richard W [Palo Alto, CA]; Pinnau, Ingo [Palo Alto, CA]; He, Zhenjie [Fremont, CA]; ...

A process for treating a gas mixture containing at least an organic compound gas or vapor and a second gas, such as natural gas, refinery off-gas or air. The process uses two sequential membrane separation steps, one using membrane selective for the organic compound over the second gas, the other selective for the second gas over the organic vapor. The second-gas-selective membranes use a selective layer made from a polymer having repeating units of a fluorinated polymer, and demonstrate good resistance to plasticization by the organic components in the gas mixture under treatment, and good recovery after exposure to liquidmore » « less
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Process for separating carbon dioxide from flue gas using sweep-based membrane separation and absorption steps

Patent Wijmans, Johannes G.; Baker, Richard W.; Merkel, Timothy C.

A gas separation process for treating flue gases from combustion processes, and combustion processes including such gas separation. The invention involves routing a first portion of the flue gas stream to be treated to an absorption-based carbon dioxide capture step, while simultaneously flowing a second portion of the flue gas across the feed side of a membrane, flowing a sweep gas stream, usually air, across the permeate side, then passing the permeate/sweep gas to the combustor.
Full Text Available
Method of preparation of bonded polyimide fuel cell package

Patent Morse, Jeffrey D [Martinez, CA]; Jankowski, Alan [Livermore, CA]; Graff, Robert T [Modesto, CA]; ...

Described herein are processes for fabricating microfluidic fuel cell systems with embedded components in which micron-scale features are formed by bonding layers of DuPont Kapton.TM. polyimide laminate. A microfluidic fuel cell system fabricated using this process is also described.
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Title: Systems and methods for using a boehmite bond-coat with polyimide membranes for gas separation

Abstract

Citation Formats

A new anhydrous proton conducting material based on phosphoric acid doped polyimide journal, October 2005

Effect of poly(amic acid) imidization on solution characteristics and membrane morphology journal, September 2000

The role of additives on dope rheology and membrane formation of defect-free Torlon® hollow fibers for gas separation journal, November 2009

Synthesis and characterization of sulfonated polyimide membranes for direct methanol fuel cell journal, August 2003

Relation of gas permeability with structure of aromatic polyimides II journal, March 1996

Multilayer composite membranes for gas separation based on crosslinked PTMSP gutter layer and partially crosslinked Matrimid® 5218 selective layer journal, September 2009

Synthesis of hyperbranched copolyimides and their application as selective layers in composite membranes journal, September 2009

Poly(imide)s book, January 2008

Characterizations and stability of polyimide–phosphotungstic acid composite electrolyte membranes for fuel cell journal, July 2007

Gas permeability, diffusivity, solubility, and aging characteristics of 6FDA-durene polyimide membranes journal, May 2001

Adsorption and Transport in Nanoporous Materials book, November 2004

Simulation of multicomponent gas separation in a hollow fiber membrane by orthogonal collocation — hydrogen recovery from refinery gases journal, July 2000

The gas separation effects of annealing polyimide–organosilicate hybrid membranes journal, January 2003

Gas transport properties in thermally cured aromatic polyimide membranes journal, September 1996

Poly(amide-imide)/TiO2 nano-composite gas separation membranes: Fabrication and characterization journal, November 1997

Synthetic 6FDA–ODA copolyimide membranes for gas separation and pervaporation: Functional groups and separation properties journal, August 2007

The permeation of binary gas mixtures through support structures of composite membranes journal, November 1998

Preparation and characterization of silica—polyimide composite membranes coated on porous tubes for CO2 separation journal, June 1996

Effect of crosslinked chain length in sulfonated polyimide membranes on water sorption, proton conduction, and methanol permeation properties journal, November 2006

Transport properties of cross-linked polyimide membranes induced by different generations of diaminobutane (DAB) dendrimers journal, July 2004

Development of polyimide flexible tactile sensor skin journal, February 2003

Efficient development of effective hollow fiber membranes for gas separations from novel polymers journal, July 2006

Synthesis, proton conductivity and methanol permeability of a novel sulfonated polyimide from 3-(2′,4′-diaminophenoxy)propane sulfonic acid journal, July 2003

Characterization of polyethersulfone/polyimide blend membranes prepared by a dry/wet phase inversion: Precipitation kinetics, morphology and gas separation journal, April 2010

Polymer Membranes for Hydrogen Separations journal, October 2006

Highly selective polymeric membranes for gas separation journal, June 2006

Protective coating for separators for electrochemical cells patent, February 2001

Polymeric Facilitated Transport Membranes for Hydrogen Purification journal, October 2006

Preparation and characterization of polyimide–silica hybrid membranes on kieselguhr–mullite supports journal, April 2002

A novel strategy for surface modification of polyimide membranes by vapor-phase ethylenediamine (EDA) for hydrogen purification journal, October 2009

Gas separation membranes developed through integration of polymer blending and dual-layer hollow fiber spinning process for hydrogen and natural gas enrichments journal, March 2010

The upper bound revisited journal, July 2008

Effects of carbon dioxide-induced plasticization on the gas transport properties of glassy polyimide membranes journal, July 2007

Comparison of asymmetric and thin-film composite membranes having Matrimid 5218 selective layer journal, November 2006

Transport properties of crosslinkable polyimide blends journal, December 1997

Modelling of biohydrogen production and recovery by membrane gas separation journal, May 2009

Molecular modelling of polyimide membranes for gas separation journal, September 2002

Aliphatic–aromatic polyimide blends for H2 separation journal, September 2010

A vapor-phase surface modification method to enhance different types of hollow fiber membranes for industrial scale hydrogen separation journal, September 2010

The solution-diffusion model: a review journal, November 1995

Polymeric membranes for the hydrogen economy: Contemporary approaches and prospects for the future journal, February 2009

Formation of defect-free polyimide hollow fiber membranes for gas separations journal, March 2000

Amplifying the molecular sieving capability of polyimide membranes via coupling of diamine networking and molecular architecture journal, July 2009

Relation of gas permeability with structure of aromatic polyimides I journal, March 1996

Methods of preparing prismatic cells patent, February 2001

Sorption and diffusion of gases in glassy polymers journal, March 1987

Polymeric Membrane Materials and Potential Use in Gas Separation book, September 2008

Enhanced gas separation performance of dual-layer hollow fiber membranes via substructure resistance reduction using mixed matrix materials journal, December 2007

Ultra-thin polyimide film as a gas-separation layer for composite membranes journal, June 1996

Sulfonated polyimide membranes grafted with sulfoalkylated side chains for proton exchange membrane fuel cell (PEMFC) applications journal, April 2008

Sol-gel polyimide-silica composite membrane: gas transport properties journal, July 1997

Application of gas separation to recover biohydrogen produced by Thiocapsa roseopersicina journal, March 2004

The effect of shear rates on gas separation performance of 6FDA-durene polyimide hollow fibers journal, March 2000

Survey of sulfonated polyimide membrane as a good candidate for nafion substitution in fuel cell journal, September 2010

Hydrogen separation and purification in membranes of miscible polymer blends with interpenetration networks journal, March 2008

Sol-gel derived ceramic electrolyte films on porous substrates report, May 1992

Membranes for gas separation journal, August 2001

The Loeb-Sourirajan Membrane: How It Came About book, May 1981

Novel highly permselective 6F-poly(amide-imide)s as membrane host for nano-sized catalysts journal, February 1995

Influence of temperature on the upper bound: Theoretical considerations and comparison with experimental results journal, September 2010

Membranes for Hydrogen Separation journal, October 2007

Ex situ hydrolytic degradation of sulfonated polyimide membranes for fuel cells journal, June 2006

Pore Size, Pore Size Distribution, and Roughness at the Membrane Surface book, January 2008

Carbon membranes from blends of PBI and polyimides for N2/CH4 and CO2/CH4 separation and hydrogen purification journal, February 2009

Gas permeation through PSF-PI miscible blend membranes journal, February 1996

Properties of a polyimide gas separation membrane in natural gas streams journal, July 1995

Zeolite-filled polyimide membrane containing 2,4,6-triaminopyrimidine journal, July 2001

Comparison of diamino cross-linking in different polyimide solutions and membranes by precipitation observation and gas transport journal, April 2008

Preparation and characterization of a poly(imide siloxane) and zeolite L mixed matrix membrane journal, June 2006

Biohydrogen recovery and purification by gas separation method journal, November 2006

Hydrogen Membrane Separation Techniques journal, February 2006

A new anhydrous proton conducting material based on phosphoric acid doped polyimide
journal, October 2005

Effect of poly(amic acid) imidization on solution characteristics and membrane morphology
journal, September 2000

The role of additives on dope rheology and membrane formation of defect-free Torlon® hollow fibers for gas separation
journal, November 2009

Synthesis and characterization of sulfonated polyimide membranes for direct methanol fuel cell
journal, August 2003

Relation of gas permeability with structure of aromatic polyimides II
journal, March 1996

Multilayer composite membranes for gas separation based on crosslinked PTMSP gutter layer and partially crosslinked Matrimid® 5218 selective layer
journal, September 2009

Synthesis of hyperbranched copolyimides and their application as selective layers in composite membranes
journal, September 2009

Poly(imide)s
book, January 2008

Characterizations and stability of polyimide–phosphotungstic acid composite electrolyte membranes for fuel cell
journal, July 2007

Gas permeability, diffusivity, solubility, and aging characteristics of 6FDA-durene polyimide membranes
journal, May 2001

Adsorption and Transport in Nanoporous Materials
book, November 2004

Simulation of multicomponent gas separation in a hollow fiber membrane by orthogonal collocation — hydrogen recovery from refinery gases
journal, July 2000

The gas separation effects of annealing polyimide–organosilicate hybrid membranes
journal, January 2003

Gas transport properties in thermally cured aromatic polyimide membranes
journal, September 1996

Poly(amide-imide)/TiO2 nano-composite gas separation membranes: Fabrication and characterization
journal, November 1997

Synthetic 6FDA–ODA copolyimide membranes for gas separation and pervaporation: Functional groups and separation properties
journal, August 2007

The permeation of binary gas mixtures through support structures of composite membranes
journal, November 1998

Preparation and characterization of silica—polyimide composite membranes coated on porous tubes for CO2 separation
journal, June 1996

Effect of crosslinked chain length in sulfonated polyimide membranes on water sorption, proton conduction, and methanol permeation properties
journal, November 2006

Transport properties of cross-linked polyimide membranes induced by different generations of diaminobutane (DAB) dendrimers
journal, July 2004

Development of polyimide flexible tactile sensor skin
journal, February 2003

Efficient development of effective hollow fiber membranes for gas separations from novel polymers
journal, July 2006

Synthesis, proton conductivity and methanol permeability of a novel sulfonated polyimide from 3-(2′,4′-diaminophenoxy)propane sulfonic acid
journal, July 2003

Characterization of polyethersulfone/polyimide blend membranes prepared by a dry/wet phase inversion: Precipitation kinetics, morphology and gas separation
journal, April 2010

Polymer Membranes for Hydrogen Separations
journal, October 2006

Highly selective polymeric membranes for gas separation
journal, June 2006

Protective coating for separators for electrochemical cells
patent, February 2001

Polymeric Facilitated Transport Membranes for Hydrogen Purification
journal, October 2006

Preparation and characterization of polyimide–silica hybrid membranes on kieselguhr–mullite supports
journal, April 2002

A novel strategy for surface modification of polyimide membranes by vapor-phase ethylenediamine (EDA) for hydrogen purification
journal, October 2009

Gas separation membranes developed through integration of polymer blending and dual-layer hollow fiber spinning process for hydrogen and natural gas enrichments
journal, March 2010

The upper bound revisited
journal, July 2008

Effects of carbon dioxide-induced plasticization on the gas transport properties of glassy polyimide membranes
journal, July 2007

Comparison of asymmetric and thin-film composite membranes having Matrimid 5218 selective layer
journal, November 2006

Transport properties of crosslinkable polyimide blends
journal, December 1997

Modelling of biohydrogen production and recovery by membrane gas separation
journal, May 2009

Molecular modelling of polyimide membranes for gas separation
journal, September 2002

Aliphatic–aromatic polyimide blends for H2 separation
journal, September 2010

A vapor-phase surface modification method to enhance different types of hollow fiber membranes for industrial scale hydrogen separation
journal, September 2010

The solution-diffusion model: a review
journal, November 1995

Polymeric membranes for the hydrogen economy: Contemporary approaches and prospects for the future
journal, February 2009

Formation of defect-free polyimide hollow fiber membranes for gas separations
journal, March 2000

Amplifying the molecular sieving capability of polyimide membranes via coupling of diamine networking and molecular architecture
journal, July 2009

Relation of gas permeability with structure of aromatic polyimides I
journal, March 1996

Methods of preparing prismatic cells
patent, February 2001

Sorption and diffusion of gases in glassy polymers
journal, March 1987

Polymeric Membrane Materials and Potential Use in Gas Separation
book, September 2008

Enhanced gas separation performance of dual-layer hollow fiber membranes via substructure resistance reduction using mixed matrix materials
journal, December 2007

Ultra-thin polyimide film as a gas-separation layer for composite membranes
journal, June 1996

Sulfonated polyimide membranes grafted with sulfoalkylated side chains for proton exchange membrane fuel cell (PEMFC) applications
journal, April 2008

Sol-gel polyimide-silica composite membrane: gas transport properties
journal, July 1997

Application of gas separation to recover biohydrogen produced by Thiocapsa roseopersicina
journal, March 2004

The effect of shear rates on gas separation performance of 6FDA-durene polyimide hollow fibers
journal, March 2000

Survey of sulfonated polyimide membrane as a good candidate for nafion substitution in fuel cell
journal, September 2010

Hydrogen separation and purification in membranes of miscible polymer blends with interpenetration networks
journal, March 2008

Sol-gel derived ceramic electrolyte films on porous substrates
report, May 1992

Membranes for gas separation
journal, August 2001

The Loeb-Sourirajan Membrane: How It Came About
book, May 1981

Novel highly permselective 6F-poly(amide-imide)s as membrane host for nano-sized catalysts
journal, February 1995

Influence of temperature on the upper bound: Theoretical considerations and comparison with experimental results
journal, September 2010

Membranes for Hydrogen Separation
journal, October 2007

Ex situ hydrolytic degradation of sulfonated polyimide membranes for fuel cells
journal, June 2006

Pore Size, Pore Size Distribution, and Roughness at the Membrane Surface
book, January 2008

Carbon membranes from blends of PBI and polyimides for N2/CH4 and CO2/CH4 separation and hydrogen purification
journal, February 2009

Gas permeation through PSF-PI miscible blend membranes
journal, February 1996

Properties of a polyimide gas separation membrane in natural gas streams
journal, July 1995

Zeolite-filled polyimide membrane containing 2,4,6-triaminopyrimidine
journal, July 2001

Comparison of diamino cross-linking in different polyimide solutions and membranes by precipitation observation and gas transport
journal, April 2008

Preparation and characterization of a poly(imide siloxane) and zeolite L mixed matrix membrane
journal, June 2006

Biohydrogen recovery and purification by gas separation method
journal, November 2006

Hydrogen Membrane Separation Techniques
journal, February 2006