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Title: Method of synthesis of anhydrous thorium(IV) complexes

Abstract

Method of producing anhydrous thorium(IV) tetrahalide complexes, utilizing Th(NO.sub.3).sub.4(H.sub.2O).sub.x, where x is at least 4, as a reagent; method of producing thorium-containing complexes utilizing ThCl.sub.4(DME).sub.2 as a precursor; method of producing purified ThCl.sub.4(ligand).sub.x compounds, where x is from 2 to 9; and novel compounds having the structures: ##STR00001##

Inventors:
;
Issue Date:
Research Org.:
LANL (Los Alamos National Laboratory (LANL), Los Alamos, NM (United States))
Sponsoring Org.:
USDOE
OSTI Identifier:
1083273
Patent Number(s):
8,431,689
Application Number:
12/778,891
Assignee:
Los Alamos National Security, LLC (Los Alamas, NM)
DOE Contract Number:  
AC52-06NA25396
Resource Type:
Patent
Country of Publication:
United States
Language:
English
Subject:
37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CHEMISTRY

Citation Formats

Kiplinger, Jaqueline L, and Cantat, Thibault. Method of synthesis of anhydrous thorium(IV) complexes. United States: N. p., 2013. Web.
Kiplinger, Jaqueline L, & Cantat, Thibault. Method of synthesis of anhydrous thorium(IV) complexes. United States.
Kiplinger, Jaqueline L, and Cantat, Thibault. Tue . "Method of synthesis of anhydrous thorium(IV) complexes". United States. https://www.osti.gov/servlets/purl/1083273.
@article{osti_1083273,
title = {Method of synthesis of anhydrous thorium(IV) complexes},
author = {Kiplinger, Jaqueline L and Cantat, Thibault},
abstractNote = {Method of producing anhydrous thorium(IV) tetrahalide complexes, utilizing Th(NO.sub.3).sub.4(H.sub.2O).sub.x, where x is at least 4, as a reagent; method of producing thorium-containing complexes utilizing ThCl.sub.4(DME).sub.2 as a precursor; method of producing purified ThCl.sub.4(ligand).sub.x compounds, where x is from 2 to 9; and novel compounds having the structures: ##STR00001##},
doi = {},
journal = {},
number = ,
volume = ,
place = {United States},
year = {2013},
month = {4}
}

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Works referenced in this record:

Synthesis and Crystal Structure of UO 2 Cl 2 (THF) 3 :  A Simple Preparation of an Anhydrous Uranyl Reagent
journal, September 1999

  • Wilkerson, Marianne P.; Burns, Carol J.; Paine, Robert T.
  • Inorganic Chemistry, Vol. 38, Issue 18
  • DOI: 10.1021/ic990159g