Methods for synthesizing alane without the formation of adducts and free of halides
Abstract
A process is provided to synthesize an alane without the formation of alane adducts as a precursor. The resulting product is a crystallized .alpha.-alane and is a highly stable product and is free of halides.
- Inventors:
- Issue Date:
- Research Org.:
- Savannah River National Laboratory (SRNL), Aiken, SC (United States)
- Sponsoring Org.:
- USDOE
- OSTI Identifier:
- 1082922
- Patent Number(s):
- 8377415
- Application Number:
- 13/313,472
- Assignee:
- Savannah River Nuclear Solutions, LLC (Aiken, SC)
- Patent Classifications (CPCs):
-
C - CHEMISTRY C01 - INORGANIC CHEMISTRY C01B - NON-METALLIC ELEMENTS
Y - NEW / CROSS SECTIONAL TECHNOLOGIES Y02 - TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE Y02E - REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
- DOE Contract Number:
- AC09-08SR22470
- Resource Type:
- Patent
- Country of Publication:
- United States
- Language:
- English
- Subject:
- 37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CHEMISTRY
Citation Formats
Zidan, Ragaiy, Knight, Douglas A, and Dinh, Long V. Methods for synthesizing alane without the formation of adducts and free of halides. United States: N. p., 2013.
Web.
Zidan, Ragaiy, Knight, Douglas A, & Dinh, Long V. Methods for synthesizing alane without the formation of adducts and free of halides. United States.
Zidan, Ragaiy, Knight, Douglas A, and Dinh, Long V. Tue .
"Methods for synthesizing alane without the formation of adducts and free of halides". United States. https://www.osti.gov/servlets/purl/1082922.
@article{osti_1082922,
title = {Methods for synthesizing alane without the formation of adducts and free of halides},
author = {Zidan, Ragaiy and Knight, Douglas A and Dinh, Long V},
abstractNote = {A process is provided to synthesize an alane without the formation of alane adducts as a precursor. The resulting product is a crystallized .alpha.-alane and is a highly stable product and is free of halides.},
doi = {},
journal = {},
number = ,
volume = ,
place = {United States},
year = {Tue Feb 19 00:00:00 EST 2013},
month = {Tue Feb 19 00:00:00 EST 2013}
}
Save to My Library
You must Sign In or Create an Account in order to save documents to your library.
Works referenced in this record:
Process for Preparing Crystalline, Non-solvated Aluminum Hydride
patent, October 1974
- Schmidt, Donald L.; Diesen, Ronald W.
- US Patent Document 3,840,654
Stabilized aluminum hydride polymorphs
patent, September 2003
- Petrie, Mark A.; Bottaro, Jeffrey C.; Schmitt, Robert J.
- US Patent Document 6,617,064
Method for synthesizing aluminum hydride
patent, September 1997
- Klapdor, Astrid; Knott, Wilfried; Windbiel, Dagmar
- US Patent Document 5,670,129
Hydrogen storage materials and method of making by dry homogenation
patent, October 2002
- Jensen, Craig M.; Zidan, Ragaiy
- US Patent Document 6,471,935
Direct synthesis of catalyzed hydride compounds
patent, September 2004
- Gross, Karl J.; Majzoub, Eric
- US Patent Document 6,793,909
Method of fabrication of complex alkali metal hydrides
patent, June 2001
- Zaluska, Alicja; Zaluski, Leszek; Strom-Olsen, John
- US Patent Document 6,251,349
Direct crystallization of aluminum hydride from toluene-ether
patent, April 1974
- Scruggs, James A.
- US Patent Document 3801657
Characterisation of mechanochemically synthesised alane (AlH3) nanoparticles
journal, November 2009
- Paskevicius, M.; Sheppard, D. A.; Buckley, C. E.
- Journal of Alloys and Compounds, Vol. 487, Issue 1-2
A Process for Preparing Lithium Aluminum Hydride-Aluminum Hydride Complexes
patent, June 1974
- Brower, Frank M.; Daniels, Arthur L.; Fujioka, George S.
- US Patent Document 3816192
Stable hydrocarbon solutions of aluminum hydride
patent, February 1977
- Hoffman, Doyt K.; Bach, Ricardo O.; Kamienski, Conrad W.
- US Patent Document 4,006,095