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Title: Magnetic agglomeration method for size control in the synthesis of magnetic nanoparticles

Abstract

A method for controlling the size of chemically synthesized magnetic nanoparticles that employs magnetic interaction between particles to control particle size and does not rely on conventional kinetic control of the reaction to control particle size. The particles are caused to reversibly agglomerate and precipitate from solution; the size at which this occurs can be well controlled to provide a very narrow particle size distribution. The size of particles is controllable by the size of the surfactant employed in the process; controlling the size of the surfactant allows magnetic control of the agglomeration and precipitation processes. Agglomeration is used to effectively stop particle growth to provide a very narrow range of particle sizes.

Inventors:
 [1]
  1. Albuquerque, NM
Issue Date:
Research Org.:
Sandia National Laboratories (SNL), Albuquerque, NM, and Livermore, CA (United States)
Sponsoring Org.:
USDOE
OSTI Identifier:
1021904
Patent Number(s):
7972410
Application Number:
12/364,261
Assignee:
Sandia Corporation (Albuquerque, NM)
Patent Classifications (CPCs):
B - PERFORMING OPERATIONS B22 - CASTING B22F - WORKING METALLIC POWDER
B - PERFORMING OPERATIONS B82 - NANOTECHNOLOGY B82Y - SPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES
DOE Contract Number:  
AC04-94AL85000
Resource Type:
Patent
Country of Publication:
United States
Language:
English
Subject:
77 NANOSCIENCE AND NANOTECHNOLOGY

Citation Formats

Huber, Dale L. Magnetic agglomeration method for size control in the synthesis of magnetic nanoparticles. United States: N. p., 2011. Web.
Huber, Dale L. Magnetic agglomeration method for size control in the synthesis of magnetic nanoparticles. United States.
Huber, Dale L. Tue . "Magnetic agglomeration method for size control in the synthesis of magnetic nanoparticles". United States. https://www.osti.gov/servlets/purl/1021904.
@article{osti_1021904,
title = {Magnetic agglomeration method for size control in the synthesis of magnetic nanoparticles},
author = {Huber, Dale L},
abstractNote = {A method for controlling the size of chemically synthesized magnetic nanoparticles that employs magnetic interaction between particles to control particle size and does not rely on conventional kinetic control of the reaction to control particle size. The particles are caused to reversibly agglomerate and precipitate from solution; the size at which this occurs can be well controlled to provide a very narrow particle size distribution. The size of particles is controllable by the size of the surfactant employed in the process; controlling the size of the surfactant allows magnetic control of the agglomeration and precipitation processes. Agglomeration is used to effectively stop particle growth to provide a very narrow range of particle sizes.},
doi = {},
journal = {},
number = ,
volume = ,
place = {United States},
year = {2011},
month = {7}
}

Works referenced in this record:

Synthesis and characterization of surfactant-coated superparamagnetic monodispersed iron oxide nanoparticles
journal, January 2001


The preparation of magnetic nanoparticles for applications in biomedicine
journal, June 2003


Giant magnetic susceptibility enhancement in field-structured nanocomposites
journal, September 2008


Synthesis of highly magnetic iron nanoparticles suitable for field structuring using a β-diketone surfactant
journal, July 2004