Polymeric media comprising polybenzimidazoles N-substituted with organic-inorganic hybrid moiety

Klaehn, John R; Peterson, Eric S; Wertsching, Alan K; Orme, Christopher J; Luther, Thomas A; Jones, Michael G

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A - human necessities
A01 - agriculture
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Title: Polymeric media comprising polybenzimidazoles N-substituted with organic-inorganic hybrid moiety

Abstract

A PBI compound includes imidazole nitrogens at least a portion of which are substituted with an organic-inorganic hybrid moiety may be included in a separator medium. At least 85% of the imidazole nitrogens may be substituted. The organic-inorganic hybrid moiety may be an organosilane moiety, for example, (R)Me.sub.2SiCH.sub.2-- where R is selected from among methyl, phenyl, vinyl, and allyl. The separatory medium may exhibit an H.sub.2, Ar, N.sub.2, O.sub.2, CH.sub.3, or CO.sub.2 gas permeability greater than the gas permeability of a comparable separatory medium comprising the PBI compound without substitution. The separatory medium may further include an electronically conductive medium and/or ionically conductive medium. The separatory medium may be used as a membrane (semi-permeable, permeable, and non-permeable), a barrier, an ion exhcange media, a filter, a gas chromatography coating (such as stationary phase coating in affinity chromatography), etc.

Inventors:

Klaehn, John R ^[1]; Peterson, Eric S ^[1]; Wertsching, Alan K ^[1]; Orme, Christopher J ^[2]; Luther, Thomas A ^[1]; Jones, Michael G ^[3]

Idaho Falls, ID
Shelley, ID
Pocatello, ID

Issue Date:: 2009-12-15

Research Org.:: Idaho National Laboratory (INL), Idaho Falls, ID (United States)

Sponsoring Org.:: USDOE

OSTI Identifier:: 1013555

Patent Number(s):: 7632898

Application Number:: 11/772,872

Assignee:: Battelle Energy Alliance, LLC (Idaho Falls, ID)

Patent Classifications (CPCs):: C - CHEMISTRY C08 - ORGANIC MACROMOLECULAR COMPOUNDS C08G - MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS

C - CHEMISTRY C08 - ORGANIC MACROMOLECULAR COMPOUNDS C08J - WORKING-UP

Show more

C - CHEMISTRY C08 - ORGANIC MACROMOLECULAR COMPOUNDS C08G - MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
C08G73/18 - Polybenzimidazoles

C - CHEMISTRY C08 - ORGANIC MACROMOLECULAR COMPOUNDS C08J - WORKING-UP
C08J2365/02 - Polyphenylenes
C08J2379/06 - Polyhydrazides
C08J5/2256 - {based on macromolecular compounds obtained by reactions other than those involving carbon-to-carbon bonds, e.g. obtained by polycondensation}

C - CHEMISTRY C08 - ORGANIC MACROMOLECULAR COMPOUNDS C08L - COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
C08L79/04 - Polycondensates having nitrogen-containing heterocyclic rings in the main chain

Y - NEW / CROSS SECTIONAL TECHNOLOGIES Y10 - TECHNICAL SUBJECTS COVERED BY FORMER USPC Y10S - TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
Y10S525/933 - Blend of limited gas permeability

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DOE Contract Number:: DE-AC07-99ID13727

Resource Type:: Patent

Country of Publication:: United States

Language:: English

Subject:: 36 MATERIALS SCIENCE

Citation Formats


                    Klaehn, John R, Peterson, Eric S, Wertsching, Alan K, Orme, Christopher J, Luther, Thomas A, and Jones, Michael G. Polymeric media comprising polybenzimidazoles N-substituted with organic-inorganic hybrid moiety.  United States: N. p., 2009. 
        Web.

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                    Klaehn, John R, Peterson, Eric S, Wertsching, Alan K, Orme, Christopher J, Luther, Thomas A, & Jones, Michael G. Polymeric media comprising polybenzimidazoles N-substituted with organic-inorganic hybrid moiety.  United States.

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                    Klaehn, John R, Peterson, Eric S, Wertsching, Alan K, Orme, Christopher J, Luther, Thomas A, and Jones, Michael G. Tue .  
        "Polymeric media comprising polybenzimidazoles N-substituted with organic-inorganic hybrid moiety".  United States.  https://www.osti.gov/servlets/purl/1013555.

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@article{osti_1013555,

  title        = {Polymeric media comprising polybenzimidazoles N-substituted with organic-inorganic hybrid moiety},

  author       = {Klaehn, John R and Peterson, Eric S and Wertsching, Alan K and Orme, Christopher J and Luther, Thomas A and Jones, Michael G},

  abstractNote = {A PBI compound includes imidazole nitrogens at least a portion of which are substituted with an organic-inorganic hybrid moiety may be included in a separator medium. At least 85% of the imidazole nitrogens may be substituted. The organic-inorganic hybrid moiety may be an organosilane moiety, for example, (R)Me.sub.2SiCH.sub.2-- where R is selected from among methyl, phenyl, vinyl, and allyl. The separatory medium may exhibit an H.sub.2, Ar, N.sub.2, O.sub.2, CH.sub.3, or CO.sub.2 gas permeability greater than the gas permeability of a comparable separatory medium comprising the PBI compound without substitution. The separatory medium may further include an electronically conductive medium and/or ionically conductive medium. The separatory medium may be used as a membrane (semi-permeable, permeable, and non-permeable), a barrier, an ion exhcange media, a filter, a gas chromatography coating (such as stationary phase coating in affinity chromatography), etc.},

  doi          = {},

  journal      = {},
number       = ,

  volume       = ,

  place        = {United States},

  year         = {2009},

  month        = {12}

}

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Patent:

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Solution-Phase Parallel Synthesis of Carbamates Using Polymer-Bound N -Hydroxysuccinimide
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Polybenzimidazole resin-based new chelating agents. Uranyl and ferric ion selectivity of resins with anchored dimethylglyoxime
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Fluorous Boc ( ^F Boc) Carbamates: New Amine Protecting Groups for Use in Fluorous Synthesis
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Organic Thin Film Transistors from a Soluble Oligothiophene Derivative Containing Thermally Removable Solubilizing Groups
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Structure−Property Relationships for Poly(pyrrolone-imide) Gas Separation Membranes
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Polybenzimidazole resin based new chelating agents uranyl ion selectivity of resins with immobilized glyoxal-bis-2-hydroxyanil and salicylaldehyde-ethylenediimine
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New chelating resins based on polybenzimidazole. Selective sorption of copper(II) from ammoniacal media on resin with anchored l-cysteine
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Similar Records

Title: Polymeric media comprising polybenzimidazoles N-substituted with organic-inorganic hybrid moiety

Abstract

Citation Formats

The solution-diffusion model: a review journal, November 1995

Conversion of Carbamates to Amidosulfones and Amides. Synthesis of the [ 14 C]-Labeled Antiobesity Agent Ro23-7637. journal, May 2002

Removal of uranium from acidic sulfate solution by ion exchange on poly(4-vinylpyridine) and polybenzimidazole in protonated sulfate form journal, May 1992

Substituted aliphatic polybenzimidazoles as membrane separator materials journal, January 1969

Fuel cell materials and components☆☆☆The Golden Jubilee Issue—Selected topics in Materials Science and Engineering: Past, Present and Future, edited by S. Suresh. journal, November 2003

Fibrous weak-base anion exchangers from a polybenzimidazole staple for the extraction of gold cyanide journal, March 1991

Polybenzimidazoles, new thermally stable polymers journal, April 1961

Porous Polybenzimidazole Membranes Doped with Phosphoric Acid: Highly Proton-Conducting Solid Electrolytes journal, February 2004

Solution-Phase Parallel Synthesis of Carbamates Using Polymer-Bound N -Hydroxysuccinimide journal, October 2002

Polybenzimidazole resin-based new chelating agents. Uranyl and ferric ion selectivity of resins with anchored dimethylglyoxime journal, January 1989

Water-soluble polybenzimidazole-based polyelectrolytes journal, August 1992

Fluorous Boc ( F Boc) Carbamates: New Amine Protecting Groups for Use in Fluorous Synthesis journal, June 2001

Organic Thin Film Transistors from a Soluble Oligothiophene Derivative Containing Thermally Removable Solubilizing Groups journal, February 2004

Acid-Doped Polybenzimidazoles: A New Polymer Electrolyte journal, January 1995

The Permeability of Different Rubbers to Gases and Its Relation to Diffusivity and Solubility journal, November 1946

Permeation, diffusion and solution of gases in organic polymers journal, January 1939

Thermolytic Synthesis of Imprinted Amines in Bulk Silica journal, July 2003

Aramid and imidazole based polyelectrolytes: physical properties and ternary phase behavior with poly(benzobisthiazole) in methanesulfonic acid journal, October 1993

Structure−Property Relationships for Poly(pyrrolone-imide) Gas Separation Membranes journal, April 2003

Polybenzimidazole resin based new chelating agents uranyl ion selectivity of resins with immobilized glyoxal-bis-2-hydroxyanil and salicylaldehyde-ethylenediimine journal, September 1990

New chelating resins based on polybenzimidazole. Selective sorption of copper(II) from ammoniacal media on resin with anchored l-cysteine journal, December 1991

Polybenzimidazole resin based new chelating agents. Palladium(II) and platinum(IV) sorption on resin with immobilized dithiooxamide journal, February 1990

Non-Fluorinated Polymer Materials for Proton Exchange Membrane Fuel Cells journal, August 2003

Anhydrous Proton-Conducting Polymers journal, August 2003

Recent advances in the functionalisation of polybenzimidazole and polyetherketone for fuel cell applications journal, April 2001

The solution-diffusion model: a review
journal, November 1995

Conversion of Carbamates to Amidosulfones and Amides. Synthesis of the [ ¹⁴ C]-Labeled Antiobesity Agent Ro23-7637.
journal, May 2002

Removal of uranium from acidic sulfate solution by ion exchange on poly(4-vinylpyridine) and polybenzimidazole in protonated sulfate form
journal, May 1992

Substituted aliphatic polybenzimidazoles as membrane separator materials
journal, January 1969

Fuel cell materials and components☆☆☆The Golden Jubilee Issue—Selected topics in Materials Science and Engineering: Past, Present and Future, edited by S. Suresh.
journal, November 2003

Fibrous weak-base anion exchangers from a polybenzimidazole staple for the extraction of gold cyanide
journal, March 1991

Polybenzimidazoles, new thermally stable polymers
journal, April 1961

Porous Polybenzimidazole Membranes Doped with Phosphoric Acid: Highly Proton-Conducting Solid Electrolytes
journal, February 2004

Solution-Phase Parallel Synthesis of Carbamates Using Polymer-Bound N -Hydroxysuccinimide
journal, October 2002

Polybenzimidazole resin-based new chelating agents. Uranyl and ferric ion selectivity of resins with anchored dimethylglyoxime
journal, January 1989

Water-soluble polybenzimidazole-based polyelectrolytes
journal, August 1992

Fluorous Boc ( ^F Boc) Carbamates: New Amine Protecting Groups for Use in Fluorous Synthesis
journal, June 2001

Organic Thin Film Transistors from a Soluble Oligothiophene Derivative Containing Thermally Removable Solubilizing Groups
journal, February 2004

Acid-Doped Polybenzimidazoles: A New Polymer Electrolyte
journal, January 1995

The Permeability of Different Rubbers to Gases and Its Relation to Diffusivity and Solubility
journal, November 1946

Permeation, diffusion and solution of gases in organic polymers
journal, January 1939

Thermolytic Synthesis of Imprinted Amines in Bulk Silica
journal, July 2003

Aramid and imidazole based polyelectrolytes: physical properties and ternary phase behavior with poly(benzobisthiazole) in methanesulfonic acid
journal, October 1993

Structure−Property Relationships for Poly(pyrrolone-imide) Gas Separation Membranes
journal, April 2003

Polybenzimidazole resin based new chelating agents uranyl ion selectivity of resins with immobilized glyoxal-bis-2-hydroxyanil and salicylaldehyde-ethylenediimine
journal, September 1990

New chelating resins based on polybenzimidazole. Selective sorption of copper(II) from ammoniacal media on resin with anchored l-cysteine
journal, December 1991

Polybenzimidazole resin based new chelating agents. Palladium(II) and platinum(IV) sorption on resin with immobilized dithiooxamide
journal, February 1990

Non-Fluorinated Polymer Materials for Proton Exchange Membrane Fuel Cells
journal, August 2003

Anhydrous Proton-Conducting Polymers
journal, August 2003

Recent advances in the functionalisation of polybenzimidazole and polyetherketone for fuel cell applications
journal, April 2001