Lower pressure synthesis of diamond material

Lueking, Angela; Gutierrez, Humberto; Narayanan, Deepa; Burgess Clifford, Caroline E; Jain, Puja

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Title: Lower pressure synthesis of diamond material

Abstract

Methods of synthesizing a diamond material, particularly nanocrystalline diamond, diamond-like carbon and bucky diamond are provided. In particular embodiments, a composition including a carbon source, such as coal, is subjected to addition of energy, such as high energy reactive milling, producing a milling product enriched in hydrogenated tetrahedral amorphous diamond-like carbon compared to the coal. A milling product is treated with heat, acid and/or base to produce nanocrystalline diamond and/or crystalline diamond-like carbon. Energy is added to produced crystalline diamond-like carbon in particular embodiments to produce bucky diamonds.

Inventors:

Lueking, Angela ^[1]; Gutierrez, Humberto ^[1]; Narayanan, Deepa ^[2]; Burgess Clifford, Caroline E ^[1]; Jain, Puja ^[3]

State College, PA
Redmond, WA
King Of Prussia, PA

Issue Date:: 2010-07-13

Research Org.:: The Penn State Research Foundation (University Park, PA)

Sponsoring Org.:: USDOE

OSTI Identifier:: 1013031

Patent Number(s):: 7754179

Application Number:: 11/613,968

Assignee:: The Penn State Research Foundation (University Park, PA)

Patent Classifications (CPCs):: B - PERFORMING OPERATIONS B82 - NANOTECHNOLOGY B82Y - SPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES

C - CHEMISTRY C01 - INORGANIC CHEMISTRY C01B - NON-METALLIC ELEMENTS

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B - PERFORMING OPERATIONS B82 - NANOTECHNOLOGY B82Y - SPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES
B82Y30/00 - Nanotechnology for materials or surface science, e.g. nanocomposites
B82Y40/00 - Manufacture or treatment of nanostructures

C - CHEMISTRY C01 - INORGANIC CHEMISTRY C01B - NON-METALLIC ELEMENTS
C01B32/15 - Nano-sized carbon materials
C01B32/25 - Diamond
C01B32/26 - Preparation

C - CHEMISTRY C30 - CRYSTAL GROWTH C30B - SINGLE-CRYSTAL-GROWTH
C30B29/04 - Diamond
C30B29/605 - {Products containing multiple oriented crystallites, e.g. columnar crystallites}
C30B30/06 - using mechanical vibrations

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DOE Contract Number:: FC26-03NT41874

Resource Type:: Patent

Country of Publication:: United States

Language:: English

Citation Formats


                    Lueking, Angela, Gutierrez, Humberto, Narayanan, Deepa, Burgess Clifford, Caroline E, and Jain, Puja. Lower pressure synthesis of diamond material.  United States: N. p., 2010. 
        Web.

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                    Lueking, Angela, Gutierrez, Humberto, Narayanan, Deepa, Burgess Clifford, Caroline E, & Jain, Puja. Lower pressure synthesis of diamond material.  United States.

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                    Lueking, Angela, Gutierrez, Humberto, Narayanan, Deepa, Burgess Clifford, Caroline E, and Jain, Puja. Tue .  
        "Lower pressure synthesis of diamond material".  United States.  https://www.osti.gov/servlets/purl/1013031.

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@article{osti_1013031,

  title        = {Lower pressure synthesis of diamond material},

  author       = {Lueking, Angela and Gutierrez, Humberto and Narayanan, Deepa and Burgess Clifford, Caroline E and Jain, Puja},

  abstractNote = {Methods of synthesizing a diamond material, particularly nanocrystalline diamond, diamond-like carbon and bucky diamond are provided. In particular embodiments, a composition including a carbon source, such as coal, is subjected to addition of energy, such as high energy reactive milling, producing a milling product enriched in hydrogenated tetrahedral amorphous diamond-like carbon compared to the coal. A milling product is treated with heat, acid and/or base to produce nanocrystalline diamond and/or crystalline diamond-like carbon. Energy is added to produced crystalline diamond-like carbon in particular embodiments to produce bucky diamonds.},

  doi          = {},

  journal      = {},
number       = ,

  volume       = ,

  place        = {United States},

  year         = {2010},

  month        = {7}

}

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Works referenced in this record:

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journal, April 1993

Bacsa, W. S.; Lannin, J. S.; Pappas, D. L.
Physical Review B, Vol. 47, Issue 16
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Resonant Raman spectroscopy of disordered, amorphous, and diamondlike carbon
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Signature of Nanodiamond in Raman Spectra: A Density Functional Theoretical Study
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Raman spectra of carbons at 2600–3300 cm−1 region
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Carbon, Vol. 16, Issue 4
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Carbon redistribution processes in nanocarbons
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Carbon, Vol. 42, Issue 5-6
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Control of sp²/sp³ Carbon Ratio and Surface Chemistry of Nanodiamond Powders by Selective Oxidation in Air
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Osswald, Sebastian; Yushin, Gleb; Mochalin, Vadym
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A comparative Raman study of some transition metal fullerides
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Raman scattering of non–planar graphite: arched edges, polyhedral crystals, whiskers and cones
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Tan, PingHeng; Dimovski, Svetlana; Gogotsi, Yury
Philosophical Transactions of the Royal Society of London. Series A: Mathematical, Physical and Engineering Sciences, Vol. 362, Issue 1824
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Hydrogen desorption property of mechanically prepared nanostructured graphite
journal, August 2001

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The Raman spectrum of nanocrystalline diamond
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Interpretation of Raman spectra of disordered and amorphous carbon
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Radiation-Induced Transformation of Graphite to Diamond
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Hydrogen storage properties on mechanically milled graphite
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Onion-like carbon from ultra-disperse diamond
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Kuznetsov, Vladimir L.; Chuvilin, Andrey L.; Butenko, Yuri V.
Chemical Physics Letters, Vol. 222, Issue 4, p. 343-348
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Nanocrystalline diamond directly transformed from carbon nanotubes under high pressure
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Oxidation of Fe-C alloys at 500�C
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Self-compression and diamond formation in carbon onions
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Similar Records

Title: Lower pressure synthesis of diamond material

Abstract

Citation Formats

Raman scattering of laser-deposited amorphous carbon journal, April 1993

Resonant Raman spectroscopy of disordered, amorphous, and diamondlike carbon journal, July 2001

Signature of Nanodiamond in Raman Spectra: A Density Functional Theoretical Study journal, April 2005

Raman spectra of carbons at 2600–3300 cm−1 region journal, January 1978

Carbon redistribution processes in nanocarbons journal, January 2004

Control of sp2/sp3 Carbon Ratio and Surface Chemistry of Nanodiamond Powders by Selective Oxidation in Air journal, September 2006

A comparative Raman study of some transition metal fullerides journal, April 2003

Raman scattering of non–planar graphite: arched edges, polyhedral crystals, whiskers and cones journal, September 2004

Recommended terminology for the description of carbon as a solid (IUPAC Recommendations 1995) journal, January 1995

Hydrogen desorption property of mechanically prepared nanostructured graphite journal, August 2001

The Raman spectrum of nanocrystalline diamond journal, December 2000

Interpretation of Raman spectra of disordered and amorphous carbon journal, May 2000

Radiation-Induced Transformation of Graphite to Diamond journal, November 1997

Hydrogen storage properties on mechanically milled graphite journal, April 2004

Onion-like carbon from ultra-disperse diamond journal, May 1994

Nanocrystalline diamond directly transformed from carbon nanotubes under high pressure journal, January 2002

Oxidation of Fe-C alloys at 500�C journal, February 1978

Self-compression and diamond formation in carbon onions journal, March 1997

Carbon onions as nanoscopic pressure cells for diamond formation journal, August 1996

An In Situ Raman-Electrochemical Investigation of Carbon Steel Corrosion in Na[sub 2]CO[sub 3]∕NaHCO[sub 3], Na[sub 2]SO[sub 4], and NaCl Solutions journal, January 2006

Synthesis and Raman characterization of boron-doped single-walled carbon nanotubes journal, January 2005

Irradiation-induced transformation of graphite to diamond: A quantitative study journal, August 2000

Raman scattering of laser-deposited amorphous carbon
journal, April 1993

Resonant Raman spectroscopy of disordered, amorphous, and diamondlike carbon
journal, July 2001

Signature of Nanodiamond in Raman Spectra: A Density Functional Theoretical Study
journal, April 2005

Raman spectra of carbons at 2600–3300 cm−1 region
journal, January 1978

Carbon redistribution processes in nanocarbons
journal, January 2004

Control of sp²/sp³ Carbon Ratio and Surface Chemistry of Nanodiamond Powders by Selective Oxidation in Air
journal, September 2006

A comparative Raman study of some transition metal fullerides
journal, April 2003

Raman scattering of non–planar graphite: arched edges, polyhedral crystals, whiskers and cones
journal, September 2004

Recommended terminology for the description of carbon as a solid (IUPAC Recommendations 1995)
journal, January 1995

Hydrogen desorption property of mechanically prepared nanostructured graphite
journal, August 2001

The Raman spectrum of nanocrystalline diamond
journal, December 2000

Interpretation of Raman spectra of disordered and amorphous carbon
journal, May 2000

Radiation-Induced Transformation of Graphite to Diamond
journal, November 1997

Hydrogen storage properties on mechanically milled graphite
journal, April 2004

Onion-like carbon from ultra-disperse diamond
journal, May 1994

Nanocrystalline diamond directly transformed from carbon nanotubes under high pressure
journal, January 2002

Oxidation of Fe-C alloys at 500�C
journal, February 1978

Self-compression and diamond formation in carbon onions
journal, March 1997

Carbon onions as nanoscopic pressure cells for diamond formation
journal, August 1996

An In Situ Raman-Electrochemical Investigation of Carbon Steel Corrosion in Na[sub 2]CO[sub 3]∕NaHCO[sub 3], Na[sub 2]SO[sub 4], and NaCl Solutions
journal, January 2006

Synthesis and Raman characterization of boron-doped single-walled carbon nanotubes
journal, January 2005

Irradiation-induced transformation of graphite to diamond: A quantitative study
journal, August 2000