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Title: Silver behenate as a calibration standard of grazing-incidence small-angle X-ray scattering

Abstract

Grazing-incidence small-angle X-ray scattering (GISAXS) patterns of a silver behenate composite film, which has a typical layered structure, are described. The peak position of the film in the GISAXS pattern was varied depending on the incident angle, which was well described by taking into account the refraction and the reflection effects. Since the refractive index of samples depends on sample preparation, it is recommended that the measurement of silver behenate as a standard be done in conventional transmission mode to avoid any complexity.

Authors:
; ; ;
Publication Date:
Research Org.:
Argonne National Lab. (ANL), Argonne, IL (United States). Advanced Photon Source (APS)
Sponsoring Org.:
USDOE
OSTI Identifier:
898681
DOE Contract Number:  
DE-AC02-06CH11357
Resource Type:
Journal Article
Journal Name:
Journal of Applied Crystallography
Additional Journal Information:
Journal Volume: 39; Journal Issue: 5; Journal ID: ISSN 0021-8898
Publisher:
International Union of Crystallography
Country of Publication:
United States
Language:
English
Subject:
37 INORGANIC, ORGANIC, PHYSICAL AND ANALYTICAL CHEMISTRY; CALIBRATION STANDARDS; SMALL ANGLE SCATTERING; X-RAY DIFFRACTION; SILVER COMPOUNDS; CARBOXYLIC ACID SALTS; advanced photon source

Citation Formats

Lee, Byeongdu, Lo, Chieh-Tsung, Seifert, Soenke, and Winans, Randall E. Silver behenate as a calibration standard of grazing-incidence small-angle X-ray scattering. United States: N. p., 2006. Web. doi:10.1107/S0021889806031244.
Lee, Byeongdu, Lo, Chieh-Tsung, Seifert, Soenke, & Winans, Randall E. Silver behenate as a calibration standard of grazing-incidence small-angle X-ray scattering. United States. https://doi.org/10.1107/S0021889806031244
Lee, Byeongdu, Lo, Chieh-Tsung, Seifert, Soenke, and Winans, Randall E. 2006. "Silver behenate as a calibration standard of grazing-incidence small-angle X-ray scattering". United States. https://doi.org/10.1107/S0021889806031244.
@article{osti_898681,
title = {Silver behenate as a calibration standard of grazing-incidence small-angle X-ray scattering},
author = {Lee, Byeongdu and Lo, Chieh-Tsung and Seifert, Soenke and Winans, Randall E.},
abstractNote = {Grazing-incidence small-angle X-ray scattering (GISAXS) patterns of a silver behenate composite film, which has a typical layered structure, are described. The peak position of the film in the GISAXS pattern was varied depending on the incident angle, which was well described by taking into account the refraction and the reflection effects. Since the refractive index of samples depends on sample preparation, it is recommended that the measurement of silver behenate as a standard be done in conventional transmission mode to avoid any complexity.},
doi = {10.1107/S0021889806031244},
url = {https://www.osti.gov/biblio/898681}, journal = {Journal of Applied Crystallography},
issn = {0021-8898},
number = 5,
volume = 39,
place = {United States},
year = {Tue Sep 12 00:00:00 EDT 2006},
month = {Tue Sep 12 00:00:00 EDT 2006}
}