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Title: High throughput liquid absorption preconcentrator sampling instrument

Patent ·
OSTI ID:868604

A system for detecting trace concentrations of an analyte in air includes a preconcentrator for the analyte and an analyte detector. The preconcentrator includes an elongated tubular container comprising a wettable material. The wettable material is continuously wetted with an analyte-sorbing liquid which flows from one part of the container to a lower end. Sampled air flows through the container in contact with the wetted material with a swirling motion which results in efficient transfer of analyte vapors or aerosol particles to the sorbing liquid and preconcentration of traces of analyte in the liquid. The preconcentrated traces of analyte may be either detected within the container or removed therefrom for injection into a separate detection means or for subsequent analysis.

Research Organization:
Argonne National Laboratory (ANL), Argonne, IL (United States)
DOE Contract Number:
W-31109-ENG-38
Assignee:
United States of America as represented by United States (Washington, DC)
Patent Number(s):
US 5173264
OSTI ID:
868604
Country of Publication:
United States
Language:
English

References (6)

Silicone rubber tubing for elimination of background conductivity in anion chromatography journal May 1984
Sampling and determination of gas-phase hydrogen peroxide following removal of ozone by gas-phase reaction with nitric oxide journal July 1986
Sequential air sampler journal
Carbon dioxide permeable tubings for post-suppression in ion chromatography journal June 1984
Technique for calibrating air samplers and certain other analytical devices journal January 1988
Simple permeation absorber for sampling and preconcentrating hazardous air contaminants journal January 1988