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Title: Method of evaluating the integrity of the outer carbon layer of triso-coated reactor fuel particles

Patent ·
OSTI ID:863679

This invention relates to a method for determining defective final layers of carbon on triso-coated fuel particles and the like. Samples of the particles are subjected to a high temperature treatment with gaseous chlorine and thereafter radiographed. The chlorine penetrates through any defective carbon layer and reacts with the underlying silicon carbide resulting in the volatilization of the silicon as SiCl.sub.4 leaving carbon as a porous layer. This porous carbon layer is easily detected by the radiography.

Research Organization:
Oak Ridge National Laboratory (ORNL), Oak Ridge, TN (United States)
Assignee:
United States of America as represented by United States (Washington, DC)
Patent Number(s):
US 4227081
OSTI ID:
863679
Country of Publication:
United States
Language:
English