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Title: Plasma Synthesis of Lithium Based Intercalation Powders for Solid Polymer Electrolyte Batteries

Abstract

The invention relates to a process for preparing lithium intercalation compounds by plasma reaction comprising the steps of: forming a feed solution by mixing lithium nitrate or lithium hydroxide or lithium oxide and the required metal nitrate or metal hydroxide or metal oxide and between 10-50% alcohol by weight; mixing the feed solution with O2 gas wherein the O2 gas atomizes the feed solution into fine reactant droplets, inserting the atomized feed solution into a plasma reactor to form an intercalation powder; and if desired, heating the resulting powder to form a very pure single phase product.

Inventors:
; ;
Publication Date:
Research Org.:
Originating Research Org. not identified (US)
Sponsoring Org.:
US Department of Energy (US)
OSTI Identifier:
836211
Patent Number(s):
PATENTS-US-A6838072
Application Number:
U.S. Patent Application 10/261,675; DOE Case S-91,881; TRN: US200503%%437
Assignee:
DOEGC
DOE Contract Number:  
AC07-941D13223
Resource Type:
Patent Application
Resource Relation:
Other Information: Supercedes Report DE00836211; PBD: 4 Jan 2005
Country of Publication:
United States
Language:
English
Subject:
25 ENERGY STORAGE; SOLID ELECTROLYTES; LITHIUM HYDROXIDES; LITHIUM NITRATES; LITHIUM OXIDES; POLYMERS; SYNTHESIS; CLATHRATES; ELECTRIC BATTERIES

Citation Formats

Kong, Peter C, Pink, Robert J, and Nelson, Lee O. Plasma Synthesis of Lithium Based Intercalation Powders for Solid Polymer Electrolyte Batteries. United States: N. p., 2005. Web.
Kong, Peter C, Pink, Robert J, & Nelson, Lee O. Plasma Synthesis of Lithium Based Intercalation Powders for Solid Polymer Electrolyte Batteries. United States.
Kong, Peter C, Pink, Robert J, and Nelson, Lee O. Tue . "Plasma Synthesis of Lithium Based Intercalation Powders for Solid Polymer Electrolyte Batteries". United States. https://www.osti.gov/servlets/purl/836211.
@article{osti_836211,
title = {Plasma Synthesis of Lithium Based Intercalation Powders for Solid Polymer Electrolyte Batteries},
author = {Kong, Peter C and Pink, Robert J and Nelson, Lee O},
abstractNote = {The invention relates to a process for preparing lithium intercalation compounds by plasma reaction comprising the steps of: forming a feed solution by mixing lithium nitrate or lithium hydroxide or lithium oxide and the required metal nitrate or metal hydroxide or metal oxide and between 10-50% alcohol by weight; mixing the feed solution with O2 gas wherein the O2 gas atomizes the feed solution into fine reactant droplets, inserting the atomized feed solution into a plasma reactor to form an intercalation powder; and if desired, heating the resulting powder to form a very pure single phase product.},
doi = {},
journal = {},
number = ,
volume = ,
place = {United States},
year = {2005},
month = {1}
}

Patent Application:

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