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Title: PREPARATION AND CHARACTERIZATION OF NANOSTRUCTURED GRANULAR SUPPORT PARTICLES AND CATALYTIC MATERIALS

Technical Report ·
DOI:https://doi.org/10.2172/792321· OSTI ID:792321

We have set up successfully two experimental systems during the past time of the project. The first system is sol-gel chemical method for preparing {gamma}-Al{sub 2}O{sub 3}, SiO{sub 2}, Cr{sub 2}O{sub 3} granular support particles. The second system is the laser-induced solution deposition (LISD) technique for nanoparticle catalysts containing Fe/Cu, and Co/Cu on the granular support. We have successfully deposited {gamma}-Al{sub 2}O{sub 3}, SiO{sub 2}, Cr{sub 2}O{sub 3} granular support particles by sol-gel method and Co and CoO nanoparticles by LISD novel fabrication technique. The characterization methods we have used include scanning electron microscope (SEM), high-resolution transmission electron microscope (HRTEM) and X-Ray diffraction (XRD). The research toward to the proposed direction is in good progress. We have given three presentations in national and local materials meetings and have submitted another two papers in another two key national meetings in nanotechnology and American Physical Annual March Meeting 2002. A couple of papers are in preparation.

Research Organization:
National Energy Technology Laboratory (NETL), Pittsburgh, PA, Morgantown, WV, and Albany, OR (United States)
Sponsoring Organization:
US Department of Energy (US)
DOE Contract Number:
FG26-00NT40836
OSTI ID:
792321
Report Number(s):
FG26-00NT40836-02; ISSN 0148-7191; TRN: US200205%%124
Resource Relation:
Other Information: PBD: 15 Jan 2002
Country of Publication:
United States
Language:
English