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Title: Imaging columns of the light elements carbon, nitrogen and oxygen with sub angstrom resolution

Journal Article · · Ultramicroscopy
OSTI ID:791187

It is reported that lattice imaging with a 300 kV field emission microscope in combination with numerical reconstruction procedures can be used to reach an interpretable resolution of about 80 pm for the first time. A retrieval of the electron exit wave from focal series allows for the resolution of single atomic columns of the light elements carbon, nitrogen, and oxygen at a projected nearest neighbor spacing down to 85 pm. Lens aberrations are corrected on-line during the experiment and by hardware such that resulting image distortions are below 80 pm. Consequently, the imaging can be aberration-free to this extent. The resolution enhancement results from increased electrical and mechanical stability's of the instrument coupled with a low spherical aberration coefficient of 0.595 + 0.005 mm.

Research Organization:
Lawrence Berkeley National Lab. (LBNL), Berkeley, CA (United States)
Sponsoring Organization:
USDOE Director, Office of Science (US)
DOE Contract Number:
AC03-76SF00098
OSTI ID:
791187
Report Number(s):
LBNL-47162; ULTRD6; R&D Project: 503601; TRN: US0200600
Journal Information:
Ultramicroscopy, Vol. 89, Issue 4; Other Information: Journal Publication Date: November 2001; PBD: 2 Jan 2000; ISSN 0304-3991
Country of Publication:
United States
Language:
English