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Title: Tank 241-AN-101, grab samples, 1AN-98-1, 1AN-98-2 and 1AN-98-3 analytical results for the final report

Abstract

This document is the final report for tank 241-AN-101 grab samples. Three grab samples 1AN-98-1, 1AN-98-2 and 1AN-98-3 were taken from riser 16 of tank 241-AN-101 on April 8, 1998 and received by the 222-S Laboratory on April 9, 1998. Analyses were performed in accordance with the ''Compatability Grab Sampling and Analysis Plan'' (TSAP) and the ''Data Quality Objectives for Tank Farms Waste Compatability Program'' (DQO). The analytical results are presented in the data summary report. No notification limits were exceeded.

Authors:
Publication Date:
Research Org.:
HNF Hanford Site (US)
Sponsoring Org.:
US DOE Office of Environmental Management (US)
OSTI Identifier:
781540
Report Number(s):
HNF-1640-REV0; EW3120074
EW3120074; TRN: US0111162
DOE Contract Number:
AC06-96RL13200
Resource Type:
Technical Report
Resource Relation:
Other Information: PBD: 24 Feb 1999
Country of Publication:
United States
Language:
English
Subject:
12 MANAGEMENT OF RADIOACTIVE WASTES, AND NON-RADIOACTIVE WASTES FROM NUCLEAR FACILITIES; SAMPLING; STORAGE FACILITIES; RADIOACTIVE WASTES; CHEMICAL COMPOSITION; DATA

Citation Formats

FULLER, R.K.. Tank 241-AN-101, grab samples, 1AN-98-1, 1AN-98-2 and 1AN-98-3 analytical results for the final report. United States: N. p., 1999. Web. doi:10.2172/781540.
FULLER, R.K.. Tank 241-AN-101, grab samples, 1AN-98-1, 1AN-98-2 and 1AN-98-3 analytical results for the final report. United States. doi:10.2172/781540.
FULLER, R.K.. Wed . "Tank 241-AN-101, grab samples, 1AN-98-1, 1AN-98-2 and 1AN-98-3 analytical results for the final report". United States. doi:10.2172/781540. https://www.osti.gov/servlets/purl/781540.
@article{osti_781540,
title = {Tank 241-AN-101, grab samples, 1AN-98-1, 1AN-98-2 and 1AN-98-3 analytical results for the final report},
author = {FULLER, R.K.},
abstractNote = {This document is the final report for tank 241-AN-101 grab samples. Three grab samples 1AN-98-1, 1AN-98-2 and 1AN-98-3 were taken from riser 16 of tank 241-AN-101 on April 8, 1998 and received by the 222-S Laboratory on April 9, 1998. Analyses were performed in accordance with the ''Compatability Grab Sampling and Analysis Plan'' (TSAP) and the ''Data Quality Objectives for Tank Farms Waste Compatability Program'' (DQO). The analytical results are presented in the data summary report. No notification limits were exceeded.},
doi = {10.2172/781540},
journal = {},
number = ,
volume = ,
place = {United States},
year = {Wed Feb 24 00:00:00 EST 1999},
month = {Wed Feb 24 00:00:00 EST 1999}
}

Technical Report:

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  • This document is the final report for tank 241-AP-106 grab samples. Three grab samples 6AP-98-1, 6AP-98-2 and 6AP-98-3 were taken from riser 1 of tank 241-AP-106 on May 28, 1998 and received by the 222-S Laboratory on May 28, 1998. Analyses were performed in accordance with the ''Compatability Grab Sampling and Analysis Plan'' (TSAP) (Sasaki, 1998) and the ''Data Quality Objectives for Tank Farms Waste Compatability Program (DQO). The analytical results are presented in the data summary report. No notification limits were exceeded. The request for sample analysis received for AP-106 indicated that the samples were polychlorinated biphenyl (PCB) suspects.more » The results of this analysis indicated that no PCBs were present at the Toxic Substance Control Act (TSCA) regulated limit of 50 ppm. The results and raw data for the PCB analysis are included in this document.« less
  • This document is the final report for tank 241-S-304 grab samples. Four grab samples were collected from riser 4 on July 30, 1998. Analyses were performed in accordance with the Compatibility Grab Sampling and Analysis Plan (TSAP) (Sasaki, 1998) and the Data Quality Objectives for Tank Farms Waste Compatibility Program (DQO). The analytical results are presented in the data summary report (Table 1). None of the subsamples submitted for differential scanning calorimetry (DSC), total organic carbon (TOC) and plutonium 239 (Pu239) analyses exceeded the notification limits as stated in TSAP (Saaaki, 1998).
  • This document is the final report for catch tank 241-ER-311 grab samples. Three grab samples ER311-98-1, ER311-98-2 and ER311-98-3 were taken from East riser of tank 241-ER-311 on August 4, 1998 and received by the 222-S Laboratory on August 4, 1998. Analyses were performed in accordance with the Compatibility Grab Sampling and Analysis Plan (TSAP) (Sasaki, 1998)and the Data Quality Objectives for Tank Farms Waste Compatibility Program (DQO) (Mulkey and Miller, 1997). The analytical results are presented in the data summary report (Table 1). No notification limits were exceeded.
  • This document is the final report for tank 241-AX-101 grab samples. Four grab samples were collected from riser 5B on July 29, 1997. Analyses were performed on samples 1AX-97-1, 1AX-97-2 and 1AX-97-3 in accordance with the Compatibility Grab Sampling and Analysis Plan (TSAP) and the Data Quality Objectives for Tank Farms Waste Compatibility Program (DQO) (Rev. 1: Fowler, 1995; Rev. 2: Mulkey and Miller, 1997). The analytical results are presented in Table 1. No notification limits were exceeded. All four samples contained settled solids that appeared to be large salt crystals that precipitated upon cooling to ambient temperature. Less thanmore » 25 % settled solids were present in the first three samples, therefore only the supernate was sampled and analyzed. Sample 1AX-97-4 contained approximately 25.3 % settled solids. Compatibility analyses were not performed on this sample. Attachment 1 is provided as a cross-reference for relating the tank farm customer identification numbers with the 222-S Laboratory sample numbers and the portion of sample analyzed. Table 2 provides the appearance information. All four samples contained settled solids that appeared to be large salt crystal that precipitated upon cooling to ambient temperature. The settled solids in samples 1AX-97-1, 1AX-97-2 and 1AX-97-3 were less than 25% by volume. Therefore, for these three samples, two 15-mL subsamples were pipetted to the surface of the liquid and submitted to the laboratory for analysis. In addition, a portion of the liquid was taken from each of the these three samples to perform an acidified ammonia analysis. No analysis was performed on the settled solid portion of the samples. Sample 1AX-97-4 was reserved for the Process Chemistry group to perform boil down and dissolution testing in accordance with Letter of Instruction for Non-Routine Analysis of Single-Shell Tank 241-AX-101 Grab Samples (Field, 1997) (Correspondence 1). However, prior to the analysis, the sample was inadvertently archived and the solid portion was not represented in the archive.« less