Growth of In/sub 2/S/sub 3/ and CdIn/sub 2/S/sub 4/ single crystals from a solution in a melt
The authors studied the reaction of In/sub 2/S/sub 3/ and CdIn/sub 2/S/sub 4/ with melts based on cadmium chloride. As the initial materials, they used polycrystalline In/sub 2/S/sub 3/ and CdIn/sub 2/S/sub 4/, cadmium chloride, and cadmium sulfide. The studies were carried out by the method of thermal analysis in sealed quartz ampules on an MOM derivatotograph. The solubility curve of In/sub 2/S/sub 3/ in a cadmium chloride melt is given. Nucleation occurs both within the liquid pahse and on the walls of the reaction container. At cooling rates of 4-5 K/h, with a charge of 100 g in a reaction container of diameter 20 mm the authors obtained In/sub 2/S/sub 3/ and CdIn/sub 2/S/sub 4/ crystals measuring 10-12 mm in size.
- Research Organization:
- Institute of Applied Physics, Academy of Sciences of the Moldavian SSSR
- OSTI ID:
- 7034358
- Journal Information:
- Inorg. Mater. (Engl. Transl.); (United States), Vol. 22:3
- Country of Publication:
- United States
- Language:
- English
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Related Subjects
CADMIUM SULFIDES
CRYSTAL GROWTH METHODS
PHASE DIAGRAMS
INDIUM SULFIDES
CADMIUM CHLORIDES
EUTECTICS
MELTING
MONOCRYSTALS
NUCLEATION
PHOTOCONDUCTIVITY
RECRYSTALLIZATION
SOLUBILITY
CADMIUM COMPOUNDS
CADMIUM HALIDES
CHALCOGENIDES
CHLORIDES
CHLORINE COMPOUNDS
CRYSTALS
DIAGRAMS
ELECTRIC CONDUCTIVITY
ELECTRICAL PROPERTIES
HALIDES
HALOGEN COMPOUNDS
INDIUM COMPOUNDS
INORGANIC PHOSPHORS
PHASE TRANSFORMATIONS
PHOSPHORS
PHYSICAL PROPERTIES
SULFIDES
SULFUR COMPOUNDS
360602* - Other Materials- Structure & Phase Studies
360603 - Materials- Properties