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Title: Poc-Scale Testing of an Advanced Fine Coal Dewatering Equipment/Technique

Abstract

In the last quarterly report, it was noticed that the baseline dewatering data varied significantly. This abnormality was attributed to the use of house vacuum which varied significantly during the testing. This quarter tests were repeated using a portable vacuum pump which provided a constant vacuum of 25 inches of mercury. Using 30 secs cake drying time and 30 secs cake formation time, the high- and low-porosity ceramic leaf filters provided 21.5% and 18.0% filter cake moistures, respectively. The solids loading on the high- and low-porosity filters were 0.8 Kg/m 2 and 0.44 Kg/m 2 , respectively. Addition of 10 g/t of an anionic flocculant lowered the filter cake moisture from 22.0% to 14.0% using the high-porosity filter, and 18.0% to 13.5% using the low-porosity filter. Addition of 15 g/t of a cationic flocculant lowered filter cake moisture from 18.0% to 16.0% using the low-porosity filter. High-porosity filter did not provide any lowering of filter cake moisture, however, the solids loading increased from 1.5 kg/m 2 to 5.8 kg/m 2 at a flocculant dosage of 25 g/t. This high solids loading indicated thicker filter cake which would retain a high moisture. Among the three surfactants studied, only the non-ionic andmore » the cationic were effective in lowering the filter cake moisture. 0.4 kg/t of a non-ionic surfactant (octyl phenoxy polyethoxy ethanol) lowered filter cake moisture from 19.5% to 16.8%; and 1 kg/t of the cationic surfactant CPCL, lowered the filter cake moisture from 19.0% to 15.8%. Addition of 0.4 kg/t of copper ions or 0.3 kg/t of aluminum ions lowered the filter cake moisture from 20.5% to 17.0%, using the low-porosity filter. The high-porosity filter which showed increase solids loading (thicker filter cakes) did not provide any lowering of the filter cake moisture. Low-porosity filter was found to be more effective in lowering the filter cake moisture than high-porosity ceramic filter. However, high-porosity was more effective in providing higher solids loading than low-porosity filter.« less

Authors:
; ;
Publication Date:
Research Org.:
Federal Energy Technology Center (FETC), Morgantown, WV, and Pittsburgh, PA
Sponsoring Org.:
USDOE Office of Fossil Energy (FE)
OSTI Identifier:
6838
Report Number(s):
DE-AC22-94PC94155-15
ON: DE00006838
DOE Contract Number:
AC22-94PC94155
Resource Type:
Technical Report
Country of Publication:
United States
Language:
English
Subject:
01 COAL, LIGNITE, AND PEAT; Coal Fines; Water Removal; Progress Report

Citation Formats

B.K. Parekh, D. Tao, and J.G. Groppo. Poc-Scale Testing of an Advanced Fine Coal Dewatering Equipment/Technique. United States: N. p., 1998. Web. doi:10.2172/6838.
B.K. Parekh, D. Tao, & J.G. Groppo. Poc-Scale Testing of an Advanced Fine Coal Dewatering Equipment/Technique. United States. doi:10.2172/6838.
B.K. Parekh, D. Tao, and J.G. Groppo. Wed . "Poc-Scale Testing of an Advanced Fine Coal Dewatering Equipment/Technique". United States. doi:10.2172/6838. https://www.osti.gov/servlets/purl/6838.
@article{osti_6838,
title = {Poc-Scale Testing of an Advanced Fine Coal Dewatering Equipment/Technique},
author = {B.K. Parekh and D. Tao and J.G. Groppo},
abstractNote = {In the last quarterly report, it was noticed that the baseline dewatering data varied significantly. This abnormality was attributed to the use of house vacuum which varied significantly during the testing. This quarter tests were repeated using a portable vacuum pump which provided a constant vacuum of 25 inches of mercury. Using 30 secs cake drying time and 30 secs cake formation time, the high- and low-porosity ceramic leaf filters provided 21.5% and 18.0% filter cake moistures, respectively. The solids loading on the high- and low-porosity filters were 0.8 Kg/m 2 and 0.44 Kg/m 2 , respectively. Addition of 10 g/t of an anionic flocculant lowered the filter cake moisture from 22.0% to 14.0% using the high-porosity filter, and 18.0% to 13.5% using the low-porosity filter. Addition of 15 g/t of a cationic flocculant lowered filter cake moisture from 18.0% to 16.0% using the low-porosity filter. High-porosity filter did not provide any lowering of filter cake moisture, however, the solids loading increased from 1.5 kg/m 2 to 5.8 kg/m 2 at a flocculant dosage of 25 g/t. This high solids loading indicated thicker filter cake which would retain a high moisture. Among the three surfactants studied, only the non-ionic and the cationic were effective in lowering the filter cake moisture. 0.4 kg/t of a non-ionic surfactant (octyl phenoxy polyethoxy ethanol) lowered filter cake moisture from 19.5% to 16.8%; and 1 kg/t of the cationic surfactant CPCL, lowered the filter cake moisture from 19.0% to 15.8%. Addition of 0.4 kg/t of copper ions or 0.3 kg/t of aluminum ions lowered the filter cake moisture from 20.5% to 17.0%, using the low-porosity filter. The high-porosity filter which showed increase solids loading (thicker filter cakes) did not provide any lowering of the filter cake moisture. Low-porosity filter was found to be more effective in lowering the filter cake moisture than high-porosity ceramic filter. However, high-porosity was more effective in providing higher solids loading than low-porosity filter.},
doi = {10.2172/6838},
journal = {},
number = ,
volume = ,
place = {United States},
year = {Wed Oct 21 00:00:00 EDT 1998},
month = {Wed Oct 21 00:00:00 EDT 1998}
}

Technical Report:

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  • Froth flotation technique is an effective and efficient process for recovering of ultra-fine (minus 74 mm) clean coal. Economical dewatering of an ultra-fine clean coal product to a 20% level moisture will be an important step in successful implementation of the advanced cleaning processes. This project is a step in the Department of Energy's program to show that ultra-clean coal could be effectively dewatered to 20% or lower moisture using either conventional or advanced dewatering techniques. The cost-sharing contract effort is for 45 months beginning September 30, 1994. This report discusses technical progress made during the quarter from January 1more » - March 31, 1998.« less
  • The main objective of the proposed program is to evaluate a novel surface modification technique, which utilizes the synergistic effect of metal ions-surfactant combination, for dewatering of ultra-fine clean coal on a proof-of-concept scale of 1 to 2 tph. The novel surface modification technique developed at the UKCAER will be evaluated using vacuum, centrifuge, and hyperbaric filtration equipment. Dewatering tests will be conducted using the fine clean-coal froth produced by the column flotation units at the Powell Mountain Coal Company, Mayflower Preparation Plant in St. Charles, Virginia. The POC-scale studies will be conducted on two different types of clean coal,more » namely, high-sulfur and low-sulfur clean coal. The Mayflower Plant processes coals from five different seams, thus the dewatering studies results could be generalized for most of the bituminous coals.« less
  • Economical dewatering of an ultra-fine clean coal product to a 20% or lower level moisture will be an important step in successful implementation of the advanced fine coal cleaning processes. The main objective of the proposed program is to evaluate a novel surface modification technique, which utilizes the synergistic effect of metal ions-surfactant combination, for dewatering of ultra-fine clean coal on a proof-of-concept (POC) scale of 1 to 2 tph. The novel surface modification technique developed at the UKCAER will be evaluated using vacuum, centrifuge, and hyperbaric filtration equipment. Dewatering tests will be conducted using the fine clean coal frothmore » produced by the column flotation units at the Powell Mountain Coal Company, Mayflower Preparation Plant in St. Charles, Virginia. The POC-scale studies will be conducted on two different types of clean coal, namely, high sulfur and low sulfur clean coal. The Mayflower Plant processes coals from five different seams, thus the dewatering studies results could be generalized for most of the bituminous coals. During this quarter, addition of reagents such as ferric ions and a novel concept of in-situ polymerization (ISP) was studied in the laboratory. Using the ISP approach with vacuum filtration provided 25% moisture filter cake compared to 65.5% moisture obtained conventionally without using the ISP. A series of dewatering tests were conducted using the Andritz hyperbaric pilot filter unit with high sulfur clean coal slurry.« less
  • Froth flotation technique is an effective and efficient process for recovering of ultra-fine (minus 74 {mu}m) clean coal. Economical dewatering of an ultra-fine clean coal product to a 20 percent level moisture will be an important step in successful implementation of the advanced cleaning processes. This project is a step in the Department of Energy`s program to show that ultra-clean coal could be effectively dewatered to 20 percent or lower moisture using either conventional or advanced dewatering techniques. The cost-sharing contract effort is for 36 months beginning September 30, 1994. This report discusses technical progress made during the quarter frommore » July 1 - September 29, 1995.« less
  • Froth flotation technique is an effective and efficient process for recovering of ultra-fine (minus 74{mu}m) clean coal. Economical dewatering of an ultrafine clean coal product to a 20% level moisture will be an important step in successful implementation of the advanced cleaning processes. The main objective of the proposed program is to evaluate a novel surface modification technique, which utilizes the synergistic effect of metal ions-surfactant combination, for dewatering of ultra-fine clean coal on a proof-of-concept scale of 1 to 2 tph. The novel surface modification technique developed at the the University of Kentucky Center for Applied Energy Research willmore » be evaluated using vacuum, centrifuge, and hyperbaric filtration equipment. Dewatering tests will be conducted using the fine clean coal froth produced by the column flotation units at the Powell Mountain Coal Company, Mayflower Preparation Plant in St. Charles, Virginia. The POC-scale studies will be conducted on two different types of clean coal, namely, high sulfur and low sulfur clean coal. Accomplishments for the past quarter are described.« less