Process for treating used industrial oil

Patent · Tue Feb 14 00:00:00 EST 1984

OSTI ID:6802506

Norman, G R

A process for rerefining used industrial oil comprising the steps of: (i) contacting said oil with an aqueous solution of the basic salt of an alkali metal to precipitate metal contaminants, polar compounds or particulates from said oil and to neutralize acid that may be present in said oil; (ii) separating bulk water and solid contaminants from said oil; (iii) separating fine particulates and remaining suspended water from said oil; (iv) vacuum drying said oil at a temperature in the range of about 250/sup 0/ F. to about 400/sup 0/ F. and a pressure in the range of about 2 to about 50 torr to remove dissolved water and light hydrocarbons from said oil; (v) contacting said oil with (a) from about 0.1 to about 3% by weight based on the weight of said oil of a polyfunctional mineral acid or the anhydride of said acid and (B) from about 0.1 to about 5% by weight based on the weight of said oil of a polyhydroxy compound, with the proviso that component (B) is in excess of component (A), until substantially all metallic contaminants in said oil have reacted with component (A) or (B) to form reaction products; (vi) separating the reaction products formed in step (v) and any unreacted components (A) or (B) from said oil; (vii) hydrotreating said oil in the presence of hydrogen and a hydrogenation catalyst at a temperature in the range of about 500/sup 0/ F. to about 800/sup 0/ F. to remove residual polar materials and unsaturated compounds; and (viii) stripping said oil to remove light hydrocarbons with boiling point below 600/sup 0/ F.

• Assignee: EDB-84-115234
• Patent Number(s): US 4431524
• OSTI ID: 6802506
• Resource Relation: Patent File Date: Filed date 26 Jan 1983; Other Information: PAT-APPL-461034
• Country of Publication: United States
• Language: English

Related Subjects

02 PETROLEUM
LUBRICATING OILS
HYDROGENATION
RECYCLING
REFINING
WASTE OILS
ALKALI METALS
ANHYDRIDES
AQUEOUS SOLUTIONS
BOILING POINTS
DEMETALLIZATION
HYDROGEN
INORGANIC ACIDS
METALS
PARTICULATES
POLAR COMPOUNDS
PRECIPITATION
VISCOSITY
WATER REMOVAL
CHEMICAL REACTIONS
DISPERSIONS
ELEMENTS
HYDROGEN COMPOUNDS
LUBRICANTS
MIXTURES
NONMETALS
OILS
ORGANIC COMPOUNDS
OTHER ORGANIC COMPOUNDS
PARTICLES
PETROLEUM PRODUCTS
PHYSICAL PROPERTIES
PROCESSING
REMOVAL
SEPARATION PROCESSES
SOLUTIONS
THERMODYNAMIC PROPERTIES
TRANSITION TEMPERATURE
020800* - Petroleum- Waste Management