Synthesis, scale-up, and characterization of 2,6-diamino-3,5-dinitropyrazine-1-oxide (LLM-105)
Conference
·
OSTI ID:672328
We have synthesized 4OOg of the new, insensitive, energetic heterocycle, 2,6-diamino-3,5-dinitropyrazine-l-oxide (LLM-105) with 81% the energy of HMX and excellent thermal stability. The synthesis is a three step reaction sequence from the commercially available starting material, 2,6-dichloropyrazine, with an overall yield of 36%. In this paper we will describe the scale-up of the synthesis of LLM- 105 and report on performance and shock sensitivity experiments performed on this material.
- Research Organization:
- Lawrence Livermore National Lab. (LLNL), Livermore, CA (United States)
- Sponsoring Organization:
- USDOE, Washington, DC (United States)
- DOE Contract Number:
- W-7405-ENG-48
- OSTI ID:
- 672328
- Report Number(s):
- UCRL-JC-130518; CONF-9806105-; ON: DE98058596; BR: YN0100000; CNN: W-7405-Eng-48
- Resource Relation:
- Conference: Joint Working Group (JOWOG) 9, Aldermaston (United Kingdom), 22-26 Jun 1998; Other Information: PBD: 27 Apr 1998
- Country of Publication:
- United States
- Language:
- English
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