Synthesis and X-ray powder structures of three novel titanium phosphate compounds
Journal Article
·
· Journal of Solid State Chemistry
- Texas A&M Univ., College Station, TX (United States)
Three titanium phosphate porous compounds were prepared hydrothermally and their structures solved from their X-ray powder diffraction patterns collected on a laboratory X-ray source. The compound, [Ti{sub 3}(PO{sub 4}){sub 4}(H{sub 2}O){sub 2}] {center_dot} NH{sub 3} (1), crystallizes in triclinic symmetry with a = 8.2506(4), b = 8.7879(4), c = 5.1022(2) {angstrom}; {alpha} = 90.703(1), {beta} = 91.083(1), {gamma} = 110.158(1){degrees}; space group P{bar 1}, and Z = 1. The structure was solved ab initio by direct methods and refined by Rietveld methods.
- OSTI ID:
- 567616
- Journal Information:
- Journal of Solid State Chemistry, Vol. 132, Issue 1; Other Information: PBD: Aug 1997
- Country of Publication:
- United States
- Language:
- English
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