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Title: Process development for electron beam joining of ceramic and glass components

Technical Report ·
DOI:https://doi.org/10.2172/554875· OSTI ID:554875
; ; ; ; ; ;  [1]; ;  [2]
  1. Sandia National Labs., Albuquerque, NM (United States)
  2. Titan Advanced Technologies Group, Albuquerque, NM (United States)

The purpose of this project is to develop and extend the electron beam joining process to applications related to Mo/Al{sub 2}O{sub 3} cermets for neutron tube fabrication, glass seals for flat panel displays, and ceramics for structural applications. The key issue is the identification of the allowable operating ranges that produce thermal conditions favorable to robust joining and sealing. High strength, hermetic braze joints between ceramic components have been produced using high energy electron beams. With a penetration depth into a typical ceramic of {approximately} 1 cm for a 10 MeV electron beam, this method provides the capability for rapid, transient brazing operations where temperature control of heat sensitive components is essential. The method deposits energy directly into a buried joint, allowing otherwise inaccessible interfaces to be brazed. The combination of transient heating, with higher thermal conductivity, lower heat capacity, and lower melting temperature of braze metals relative to the ceramic materials, enables a pulsed high power beam to melt a braze metal without producing excessive ceramic temperatures. The authors have demonstrated the feasibility of this process related to ceramic coupons a well as ceramic and glass tubes and cylindrical shapes. The transient thermal response was predicted, using as input the energy absorption predicted from the coupled electron-photon and thermal transport analysis. The joining experiments were conducted with an RF linear accelerator at 10--13 MV. Joining experiments have provided high strength joints between alumina and alumina and between alumina and cermet joints in cylindrical geometry. These joints provided good hermetic seals.

Research Organization:
Sandia National Lab. (SNL-NM), Albuquerque, NM (United States)
Sponsoring Organization:
USDOE, Washington, DC (United States)
DOE Contract Number:
AC04-94AL85000
OSTI ID:
554875
Report Number(s):
SAND-97-2785; ON: DE98001362; BR: DP0102012; TRN: AHC29801%%138
Resource Relation:
Other Information: PBD: Nov 1997
Country of Publication:
United States
Language:
English