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Title: Synthesis and structural analysis of Sr{sub 5.8}La{sub 4.4}Ti{sub 7.8}S{sub 24}O{sub 4} and La{sub 14}Ti{sub 8}S{sub 33}O{sub 4}: Two new oxysulfides containing a common {sub {infinity}}{sup 2} [(Ti{sub 4}S{sub 2}O{sub 4})(TiS{sub 6}){sub 4/2}]{sup 12{minus}} layer

Abstract

The synthesis of Sr{sub 5.8}La{sub 4.4}Ti{sub 7.8}S{sub 24}O{sub 4} and La{sub 14}Ti{sub 8}S{sub 33}O{sub 4} by high-temperature methods is described. Electron diffraction and X-ray diffraction of single crystals and powders were used in the structural characterization of these compounds. The structure of these compounds are discussed.

Authors:
; ;  [1]
  1. Univ. of Maryland, College Park, MD (United States)
Publication Date:
OSTI Identifier:
508432
Resource Type:
Journal Article
Journal Name:
Chemistry of Materials
Additional Journal Information:
Journal Volume: 8; Journal Issue: 9; Other Information: PBD: Sep 1996
Country of Publication:
United States
Language:
English
Subject:
40 CHEMISTRY; 36 MATERIALS SCIENCE; STRONTIUM COMPOUNDS; CHEMICAL PREPARATION; CRYSTAL STRUCTURE; LANTHANUM COMPOUNDS; TITANIUM COMPOUNDS; OXYSULFIDES; STOICHIOMETRY; ELECTRON DIFFRACTION; X-RAY DIFFRACTION

Citation Formats

Tranchitella, L.J., Fettinger, J.C., and Eichhorn, B.W. Synthesis and structural analysis of Sr{sub 5.8}La{sub 4.4}Ti{sub 7.8}S{sub 24}O{sub 4} and La{sub 14}Ti{sub 8}S{sub 33}O{sub 4}: Two new oxysulfides containing a common {sub {infinity}}{sup 2} [(Ti{sub 4}S{sub 2}O{sub 4})(TiS{sub 6}){sub 4/2}]{sup 12{minus}} layer. United States: N. p., 1996. Web. doi:10.1021/cm960001j.
Tranchitella, L.J., Fettinger, J.C., & Eichhorn, B.W. Synthesis and structural analysis of Sr{sub 5.8}La{sub 4.4}Ti{sub 7.8}S{sub 24}O{sub 4} and La{sub 14}Ti{sub 8}S{sub 33}O{sub 4}: Two new oxysulfides containing a common {sub {infinity}}{sup 2} [(Ti{sub 4}S{sub 2}O{sub 4})(TiS{sub 6}){sub 4/2}]{sup 12{minus}} layer. United States. doi:10.1021/cm960001j.
Tranchitella, L.J., Fettinger, J.C., and Eichhorn, B.W. Sun . "Synthesis and structural analysis of Sr{sub 5.8}La{sub 4.4}Ti{sub 7.8}S{sub 24}O{sub 4} and La{sub 14}Ti{sub 8}S{sub 33}O{sub 4}: Two new oxysulfides containing a common {sub {infinity}}{sup 2} [(Ti{sub 4}S{sub 2}O{sub 4})(TiS{sub 6}){sub 4/2}]{sup 12{minus}} layer". United States. doi:10.1021/cm960001j.
@article{osti_508432,
title = {Synthesis and structural analysis of Sr{sub 5.8}La{sub 4.4}Ti{sub 7.8}S{sub 24}O{sub 4} and La{sub 14}Ti{sub 8}S{sub 33}O{sub 4}: Two new oxysulfides containing a common {sub {infinity}}{sup 2} [(Ti{sub 4}S{sub 2}O{sub 4})(TiS{sub 6}){sub 4/2}]{sup 12{minus}} layer},
author = {Tranchitella, L.J. and Fettinger, J.C. and Eichhorn, B.W.},
abstractNote = {The synthesis of Sr{sub 5.8}La{sub 4.4}Ti{sub 7.8}S{sub 24}O{sub 4} and La{sub 14}Ti{sub 8}S{sub 33}O{sub 4} by high-temperature methods is described. Electron diffraction and X-ray diffraction of single crystals and powders were used in the structural characterization of these compounds. The structure of these compounds are discussed.},
doi = {10.1021/cm960001j},
journal = {Chemistry of Materials},
number = 9,
volume = 8,
place = {United States},
year = {1996},
month = {9}
}