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Title: Process for synthesizing compounds from elemental powders

Patent Application ·
OSTI ID:5050898

A process for synthesizing intermetallic compounds from elemental powders. The elemental powders are initially combined in ratio a which approximates the stoichiometric composition of the intermetallic compound. The mixed powders are then formed into a compact which is heat treated at a controlled rate of heating such that an exothermic reaction between the elements is initiated. The heat treatment may be performed under controlled conditions ranging from a vacuum (pressureless sintering) to compression (hot pressing) to produce a desired densification of the intermetallic compound. In a preferred form of the invention, elemental powders of Fe and Al are combined to form aluminide compounds of Fe{sub 3}Al and FeAl.

Research Organization:
EG and G Idaho, Inc., Idaho Falls, ID (United States)
Sponsoring Organization:
USDOE; USDOE, Washington, DC (United States)
DOE Contract Number:
AC07-76ID01570
Assignee:
Dept. of Energy
Patent Number(s):
PATENTS-US-A7603650
Application Number:
ON: DE92016211; PPN: US 7-603650
OSTI ID:
5050898
Resource Relation:
Patent File Date: 26 Oct 1990
Country of Publication:
United States
Language:
English