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Title: Effect of thickness and annealing on stress in tantalum and tantalum nitride thin film hard coatings

Book ·
OSTI ID:467639
; ;  [1]
  1. Univ. of Alabama, Tuscaloosa, AL (United States). Dept. of Metallurgical and Materials Engineering

An understanding of the relationship between stress and the other properties of thin films is extremely useful in the design of hard coatings for long term performance. In the authors` earlier study, sputtered Ta and Ta(N) films were found to exhibit promising hard coating properties. For example, nano hardness as high as 30 GPa was observed in the nitride (pN{sub 2} = 0.100 mTorr) films. In this work, they study the variation in the stress in these films with respect to film thickness and annealing. Films in six different thicknesses (50, 250, 350, 500, 750, and 1,000 nm) were deposited on oxide coated Si(111) wafers. Stresses in the films in the as-deposited state and as a function of temperature (300 C) were determined using a thin film stress measuring unit.

OSTI ID:
467639
Report Number(s):
CONF-960401-; ISBN 1-55899-339-8; TRN: 97:008311
Resource Relation:
Conference: Spring meeting of the Materials Research Society (MRS), San Francisco, CA (United States), 8-12 Apr 1996; Other Information: PBD: 1997; Related Information: Is Part Of Thin films: Stresses and mechanical properties VI; Gerberich, W.W. [ed.] [Univ. of Minnesota, Minneapolis, MN (United States)]; Gao, H. [ed.] [Stanford Univ., CA (United States)]; Sundgren, J.E. [ed.] [Linkoeping Univ. (Sweden)]; Baker, S.P. [ed.] [Max-Planck-Inst. fuer Metallforschung, Stuttgart (Germany)]; PB: 559 p.; Materials Research Society symposium proceedings, Volume 436
Country of Publication:
United States
Language:
English

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