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Title: THE DETERMINATION OF FISSION PRODUCT RUTHENIUM

Abstract

Improvements in Glendenin's procedure for the determimation of fission product ruthenium have been made. The distillation from perchloric acid has been replaced by ABSTRACTS a more rapid distillation from a dilute suifuric acid- sodium bismuthate mixture. Conditions for the quantitative volatilization and collection of the tetroxide, as well as reduction to the dioxide, have been established. Reduction to the metal for a yield determimation is no longer necessary. The analysis time has been halved and the precision has been improved by a factor of three. (auth)

Authors:
; ;
Publication Date:
Research Org.:
Argonne National Lab., Lemont, Ill.
OSTI Identifier:
4341676
Report Number(s):
ANL-5810
NSA Number:
NSA-12-003566
DOE Contract Number:  
W-31-109-ENG-38
Resource Type:
Technical Report
Resource Relation:
Other Information: Orig. Receipt Date: 31-DEC-58
Country of Publication:
United States
Language:
English
Subject:
CHEMISTRY; BISMUTH COMPOUNDS; BISMUTH OXIDES; CHEMICAL REACTIONS; DISTILLATION; ERRORS; FISSION PRODUCTS; PERCHLORIC ACID; QUALITATIVE ANALYSIS; QUANTITATIVE ANALYSIS; REDUCTION; RUTHENIUM; RUTHENIUM OXIDES; SODIUM COMPOUNDS; SODIUM OXIDES; SULFURIC ACID; VOLATILITY

Citation Formats

Larsen, R.P., Ross, L.E., and Kesser, G. THE DETERMINATION OF FISSION PRODUCT RUTHENIUM. United States: N. p., 1957. Web. doi:10.2172/4341676.
Larsen, R.P., Ross, L.E., & Kesser, G. THE DETERMINATION OF FISSION PRODUCT RUTHENIUM. United States. doi:10.2172/4341676.
Larsen, R.P., Ross, L.E., and Kesser, G. Sun . "THE DETERMINATION OF FISSION PRODUCT RUTHENIUM". United States. doi:10.2172/4341676. https://www.osti.gov/servlets/purl/4341676.
@article{osti_4341676,
title = {THE DETERMINATION OF FISSION PRODUCT RUTHENIUM},
author = {Larsen, R.P. and Ross, L.E. and Kesser, G.},
abstractNote = {Improvements in Glendenin's procedure for the determimation of fission product ruthenium have been made. The distillation from perchloric acid has been replaced by ABSTRACTS a more rapid distillation from a dilute suifuric acid- sodium bismuthate mixture. Conditions for the quantitative volatilization and collection of the tetroxide, as well as reduction to the dioxide, have been established. Reduction to the metal for a yield determimation is no longer necessary. The analysis time has been halved and the precision has been improved by a factor of three. (auth)},
doi = {10.2172/4341676},
journal = {},
number = ,
volume = ,
place = {United States},
year = {1957},
month = {12}
}