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Title: Interstitial impurity interactions and dislocation microdynamics in Mo crystals

Thesis/Dissertation ·
DOI:https://doi.org/10.2172/4197705· OSTI ID:4197705
 [1]
  1. Stony Brook Univ., NY (United States)

The effects of interstitial impurities on the mechanical properties of molybdenum are explored by comparing results obtained for crystals of various interstitial contents controlled by ultra-high vacuum outgassing. Results show a modulus reduction for as-grown samples and for outgassed specimens at low applied stresses. As a function of plastic microstrain, the values of modulus defect for both as-grown and outgassed specimens saturate at the same value. Interstitial impurities act as pinning agents to dislocation bowing, but when all the easy dislocation loops have broken away from local interstitial pins, the modulus defect reaches a constant saturation value. Etch pitting techniques were used to correlate microstrain observations with dislocation generation and motion. It has been found that edge dislocation generation and movement are active in the microstrain region while screw dislocations are relatively inactive until the macrostrain region is reached. Dislocation velocities range from 10-6 to 10-3 cm/s and the average distance between interstitial impurity pinning points is found to be approximately 8 x 10-4 cm.

Research Organization:
Stony Brook Univ., NY (United States)
Sponsoring Organization:
US Energy Research and Development Administration (ERDA)
DOE Contract Number:
AT(11-1)-3476
NSA Number:
NSA-32-020306
OSTI ID:
4197705
Report Number(s):
COO-3476-11
Resource Relation:
Other Information: Thesis. Orig. Receipt Date: 31-DEC-75
Country of Publication:
United States
Language:
English