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Title: Methodologies to observe and characterize interfacial reaction products in (Al{sub 2}O{sub 3}){sub p}/Al and SiC{sub p}/Al composites -- using SEM, XRD, TEM

Abstract

Improved mechanical properties of metal-matrix composites reinforced with ceramic particles are due to the transfer of shear load at the matrix/reinforcement interface. As a result, composite interfaces play important roles in determining the resultant composite properties. The aim of the present study is twofold: (a) to identify the interfacial reaction products using X-ray diffractometry (XRD) and CBED, and (b) to demonstrate detailed 3-dimensional morphologies of the interfacial reaction products using SEM. Powder extraction procedure employed for XRD and SEM applications is also presented.

Authors:
; ;  [1]
  1. Korea Inst. of Science and Technology, Seoul (Korea, Republic of). Div. of Metals
Publication Date:
OSTI Identifier:
382543
Resource Type:
Journal Article
Journal Name:
Scripta Materialia
Additional Journal Information:
Journal Volume: 35; Journal Issue: 6; Other Information: PBD: 15 Sep 1996
Country of Publication:
United States
Language:
English
Subject:
36 MATERIALS SCIENCE; COMPOSITE MATERIALS; MICROSTRUCTURE; ALUMINIUM OXIDES; ALUMINIUM; SILICON CARBIDES; INTERFACES; CHEMICAL REACTIONS; TRANSMISSION ELECTRON MICROSCOPY; X-RAY DIFFRACTION; SCANNING ELECTRON MICROSCOPY; MORPHOLOGY

Citation Formats

Lee, J C, Lee, J I, and Lee, Ho-In. Methodologies to observe and characterize interfacial reaction products in (Al{sub 2}O{sub 3}){sub p}/Al and SiC{sub p}/Al composites -- using SEM, XRD, TEM. United States: N. p., 1996. Web. doi:10.1016/1359-6462(96)00206-0.
Lee, J C, Lee, J I, & Lee, Ho-In. Methodologies to observe and characterize interfacial reaction products in (Al{sub 2}O{sub 3}){sub p}/Al and SiC{sub p}/Al composites -- using SEM, XRD, TEM. United States. https://doi.org/10.1016/1359-6462(96)00206-0
Lee, J C, Lee, J I, and Lee, Ho-In. 1996. "Methodologies to observe and characterize interfacial reaction products in (Al{sub 2}O{sub 3}){sub p}/Al and SiC{sub p}/Al composites -- using SEM, XRD, TEM". United States. https://doi.org/10.1016/1359-6462(96)00206-0.
@article{osti_382543,
title = {Methodologies to observe and characterize interfacial reaction products in (Al{sub 2}O{sub 3}){sub p}/Al and SiC{sub p}/Al composites -- using SEM, XRD, TEM},
author = {Lee, J C and Lee, J I and Lee, Ho-In},
abstractNote = {Improved mechanical properties of metal-matrix composites reinforced with ceramic particles are due to the transfer of shear load at the matrix/reinforcement interface. As a result, composite interfaces play important roles in determining the resultant composite properties. The aim of the present study is twofold: (a) to identify the interfacial reaction products using X-ray diffractometry (XRD) and CBED, and (b) to demonstrate detailed 3-dimensional morphologies of the interfacial reaction products using SEM. Powder extraction procedure employed for XRD and SEM applications is also presented.},
doi = {10.1016/1359-6462(96)00206-0},
url = {https://www.osti.gov/biblio/382543}, journal = {Scripta Materialia},
number = 6,
volume = 35,
place = {United States},
year = {Sun Sep 15 00:00:00 EDT 1996},
month = {Sun Sep 15 00:00:00 EDT 1996}
}