An evaluation method on degree of graphitization of carbon materials under high temperature and high pressure
- National Taiwan Univ., Taipei (Taiwan, Province of China). Graduate Inst. of Materials Science and Engineering
The majority of early studies used X-ray diffraction, but this requires a model to interpret the diffraction process. A turbostratic model has been applied by Warren, Franklin and Bacon to a wide range of materials including both soft and hard carbons. Maire and Mering applied the same methods to the interpretation of the (001) lines of a series of graphitic carbons. In this case, graphitic carbons undergone high temperature and high pressure graphitization processes have been evaluated by the same methods. It was found that most technological XRD data were obtained by a Rietveld method with the least-squares refinements could be in the simplest way since the full correction technique is very laborious. The behavior of carbon materials as it proceeds through the graphitization process is characterized by changes in the measured interlayer spacings (d) as a function of temperature. A series of graphitic carbons including the transformation of diamond to graphite through the process under high temperature and high pressure have been evaluated. A simple calibration equation has been established.
- OSTI ID:
- 367639
- Report Number(s):
- CONF-960202-; ISBN 0-87339-310-4; TRN: IM9640%%385
- Resource Relation:
- Conference: Annual meeting and exhibition of the Minerals, Metals and Materials Society (TMS), Anaheim, CA (United States), 4-8 Feb 1996; Other Information: PBD: 1996; Related Information: Is Part Of Design fundamentals of high temperature composites, intermetallics, and metal-ceramics systems; Lin, R.Y. [ed.] [Univ. of Cincinnati, OH (United States). Dept. of Materials Science and Engineering]; Chang, Y.A. [ed.] [Univ. of Wisconsin, Madison, WI (United States). Dept. of Materials Science and Engineering]; Reddy, R.G. [ed.] [Univ. of Nevada, Reno, NV (United States). Dept. of Chemical and Metallurgical Engineering]; Liu, C.T. [ed.] [Oak Ridge National Lab., TN (United States). Metals and Ceramics Div.]; PB: 461 p.
- Country of Publication:
- United States
- Language:
- English
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