Manufacturing Oxide Dispersion Strengthened (ODS) steel plate via cold spray and friction stir processing

Wang, Xiang; Zhang, Dalong; Darsell, Jens T.; Ross, Kenneth A.; Ma, Xiaolong; Liu, Jia; Liu, Tingkun; Prabhakaran, Ramprashad; Li, Lan; Anderson, Iver E.; Setyawan, Wahyu

doi:10.1016/j.jnucmat.2024.155076

Manufacturing Oxide Dispersion Strengthened (ODS) steel plate via cold spray and friction stir processing

Journal Article · Mon Apr 08 00:00:00 EDT 2024 · Journal of Nuclear Materials

DOI:https://doi.org/10.1016/j.jnucmat.2024.155076· OSTI ID:2439243

^[1]; ^[1]; ^[1]; ^[1]; ^[1]; Liu, Jia ^[1]; ^[1]; ^[1]; Li, Lan ^[1]; Anderson, Iver E. ^[2]; ^[1]

Pacific Northwest National Laboratory (PNNL), Richland, WA (United States)
Ames Laboratory (AMES), Ames, IA (United States)

Oxide dispersion strengthened (ODS) steels, traditionally fabricated by ball milling and conventional powder metallurgy techniques to achieve bulk form, followed by intricate rolling and thermal treatment steps to achieve plate or sheet form. Here, we present a novel processing route that combines cold spray (CS) with friction stir processing (FSP) to manufacture ODS steel plate directly from gas atomization reaction synthesis (GARS)-prepared powder, thus no rolling steps involved. Microstructural and mechanical characterizations were performed to assess the quality and properties of the resulting ODS steel plate. Our findings demonstrate that the slightly porous CS deposited layer was fully consolidated after FSP, yielding a fully dense ODS steel plate that exhibited a favorable tradeoff between strength and ductility upon extraction from the substrate. Furthermore, through microstructural analysis, we revealed the presence of an appreciable density (~10²²/m³) of nano-sized oxide particles, with the majority being smaller than 5 nm via the combined CS + FSP fabrication route. This work serves as a first proof-of-concept demonstration of the manufacturing approach described herein, offering a possible alternative route for producing ODS steel plates.

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This content will become publicly available on Tue Apr 08 00:00:00 EDT 2025

Research Organization:: Pacific Northwest National Laboratory (PNNL), Richland, WA (United States); Ames Laboratory (AMES), Ames, IA (United States)

Sponsoring Organization:: USDOE Office of Science (SC), Fusion Energy Sciences (FES); USDOE Office of Science (SC), Biological and Environmental Research (BER); USDOE

Grant/Contract Number:: AC05-76RL01830; AC02–07CH11358; AC02-07CH11358; AC05–76RL01830; AT2030110-13784.

OSTI ID:: 2439243

Alternate ID(s):: OSTI ID: 2337980; OSTI ID: 2340129

Report Number(s):: PNNL-SA-184484; IS-J-11,314

Journal Information:: Journal of Nuclear Materials, Vol. 596; ISSN 0022-3115

Publisher:: ElsevierCopyright Statement

Country of Publication:: United States

Language:: English

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36 MATERIALS SCIENCE
gas atomization reation synthesis
cold spray
friction stir processing (FSP)
ODS steels
transmission electron microscopy (TEM)
atom probe tomography (APT)
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friction stir processing
manufacturing

Manufacturing Oxide Dispersion Strengthened (ODS) steel plate via cold spray and friction stir processing

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