Skip to main content
U.S. Department of Energy
Office of Scientific and Technical Information

Direct Observation of Sample Dynamics in the Gaseous Environment: A Perspective on Current Trends and Future Directions of In Situ Gas Cell Transmission Electron Microscopy

Journal Article · · Journal of Physical Chemistry. C
 [1];  [2];  [2];  [2];  [2]
  1. Department of Chemistry, University of Kentucky, 506 Library Drive, Lexington, Kentucky 40506, United States; OSTI
  2. Department of Chemistry, University of Kentucky, 506 Library Drive, Lexington, Kentucky 40506, United States
Not provided.
Research Organization:
Univ. of Kentucky, Lexington, KY (United States)
Sponsoring Organization:
USDOE Office of Science (SC)
DOE Contract Number:
SC0022315
OSTI ID:
2422142
Journal Information:
Journal of Physical Chemistry. C, Journal Name: Journal of Physical Chemistry. C Journal Issue: 38 Vol. 127; ISSN 1932-7447
Publisher:
American Chemical Society
Country of Publication:
United States
Language:
English

References (85)

Deep learning detection of nanoparticles and multiple object tracking of their dynamic evolution during in situ ETEM studies journal February 2022
A structure and activity relationship for single-walled carbon nanotube growth confirmed by in situ observations and modeling journal January 2020
Versatile Homebuilt Gas Feed and Analysis System for Operando TEM of Catalysts at Work journal March 2020
Iron-silica interaction during reduction of precipitated silica-promoted iron oxides using in situ XRD and TEM journal March 2021
Dynamic Atom Clusters on AuCu Nanoparticle Surface during CO Oxidation journal February 2020
Oxide Catalysts with Ultrastrong Resistance to SO 2 Deactivation for Removing Nitric Oxide at Low Temperature journal September 2019
In Situ Oxidation Studies of High-Entropy Alloy Nanoparticles journal October 2020
Reshaping Dynamics of Gold Nanoparticles under H 2 and O 2 at Atmospheric Pressure journal January 2019
In Situ Observation of Nanoparticle Exsolution from Perovskite Oxides: From Atomic Scale Mechanistic Insight to Nanostructure Tailoring journal October 2019
Single Atom Dynamics in Chemical Reactions journal January 2020
Exceptional Tunability over Size and Density of Spontaneously Formed Nanoparticles via Nucleation Dynamics journal April 2020
Operando S/TEM Reactions of Pt/TiO 2 Catalysts for Catalytic Fast Pyrolysis journal July 2020
In situ characterization of kinetics and mass transport of PbSe nanowire growth via LS and VLS mechanisms journal January 2019
Lab on a beam—Big data and artificial intelligence in scanning transmission electron microscopy journal July 2019
Atomic origin of CO-Interaction effect of PtPb@Pt catalyst revealed by in situ environmental transmission electron microscopy journal October 2020
In Situ TEM Studies of Catalysts Using Windowed Gas Cells journal July 2020
Revealing Sintering Kinetics of MoS 2 -Supported Metal Nanocatalysts in Atmospheric Gas Environments via Operando Transmission Electron Microscopy journal April 2020
Shape of Cobalt and Platinum Nanoparticles Under a CO Atmosphere: A Combined In Situ TEM and Computational Catalysis Study journal July 2019
Atomic Scale Insight into the Formation, Size, and Location of Platinum Nanoparticles Supported on γ-Alumina journal March 2020
In situ investigation of nanocatalysts in gas atmosphere by transmission electron microscopy journal April 2020
Restructuring effects of the chemical environment in metal nanocatalysis and single-atom catalysis journal April 2020
Investigation of gas-electron interactions with electron holography journal February 2021
Three-Dimensional Quantification of the Facet Evolution of Pt Nanoparticles in a Variable Gaseous Environment journal December 2018
Fast electron tomography: Applications to beam sensitive samples and in situ TEM or operando environmental TEM studies journal May 2019
Dynamic co-catalysis of Au single atoms and nanoporous Au for methane pyrolysis journal April 2020
In‐situ Transmission Electron Microscope Techniques for Heterogeneous Catalysis journal April 2020
In situ transmission electron microscopy and artificial intelligence enabled data analytics for energy materials journal May 2022
An in-situ TEM microreactor for real-time nanomorphology & physicochemical parameters interrelated characterization journal December 2020
Bimetallic Phosphide (Ni,Cu)2P Nanoparticles by Inward Phosphorus Migration and Outward Copper Migration journal July 2019
Fast Electron Tomography for Nanomaterials journal November 2020
The dynamics of overlayer formation on catalyst nanoparticles and strong metal-support interaction journal June 2020
Microreactor-Based TG–TEM Synchronous Analysis journal June 2022
In situ metal-organic chemical vapour deposition growth of III–V semiconductor nanowires in the Lund environmental transmission electron microscope journal February 2020
Structural changes in noble metal nanoparticles during CO oxidation and their impact on catalyst activity journal May 2020
Dynamic restructuring of supported metal nanoparticles and its implications for structure insensitive catalysis journal December 2021
Recent Progresses on Structural Reconstruction of Nanosized Metal Catalysts via Controlled-Atmosphere Transmission Electron Microscopy: A Review journal November 2020
Towards data-driven next-generation transmission electron microscopy journal October 2020
Controllable in Situ Surface Restructuring of Cu Catalysts and Remarkable Enhancement of Their Catalytic Activity journal January 2019
Operando Methods in Electrocatalysis journal January 2021
Exsolution of Catalytically Active Iridium Nanoparticles from Strontium Titanate journal July 2020
Sintering of cobalt during FTS: Insights from industrial and model systems journal February 2020
In Situ Studies of Single-Nanoparticle-Level Nickel Thermal Oxidation: From Early Oxide Nucleation to Diffusion-Balanced Oxide Thickening journal April 2022
Recent Progress of In Situ Transmission Electron Microscopy for Energy Materials journal September 2019
Bimetallic Nanoparticle Oxidation in Three Dimensions by Chemically Sensitive Electron Tomography and in Situ Transmission Electron Microscopy journal July 2018
Oxidation-Induced Atom Diffusion and Surface Restructuring in Faceted Ternary Pt–Cu–Ni Nanoparticles journal February 2019
Developments and advances in in situ transmission electron microscopy for catalysis research journal January 2021
In Situ TEM Study of Rh Particle Sintering for Three-Way Catalysts in High Temperatures journal December 2020
Nanoscale oxidation behavior of carbon fibers revealed with in situ gas cell STEM journal July 2021
Direct observation of tungsten oxidation studied by in situ environmental TEM journal April 2021
Insights into fundamental deformation processes from advanced in situ transmission electron microscopy journal June 2019
Quantitative Structure–Activity Relationship of Nanowire Adsorption to SO2 Revealed by In Situ TEM Technique journal February 2021
Real‐Time Imaging of Nanoscale Redox Reactions over Bimetallic Nanoparticles journal July 2019
Development of a gas environmental heating specimen holder system using differential pumping journal June 2021
In Situ Transmission Electron Microscopy on Energy‐Related Catalysis journal December 2019
Structural evolution of atomically dispersed Pt catalysts dictates reactivity journal April 2019
In Situ Transmission Electron Microscopy for Energy Applications journal January 2019
Introducing and Controlling Water Vapor in Gas-Cell Microscopy Experiments journal February 2019
In situ manipulation of the active Au-TiO 2 interface with atomic precision during CO oxidation journal January 2021
Reshaping of Metal Nanoparticles Under Reaction Conditions journal February 2020
Fast Gas-Solid Reaction Kinetics of Nanoparticles Unveiled by Millisecond In Situ Electron Diffraction at Ambient Pressure journal July 2018
Insights into Chemical Dynamics and Their Impact on the Reactivity of Pt Nanoparticles during CO Oxidation by Operando TEM journal February 2020
In situ and operando characterisation techniques for solid oxide electrochemical cells: recent advances journal November 2020
In-situ transmission electron microscopy for probing the dynamic processes in materials journal August 2021
Operando Electron Microscopy Study of Cobalt‐based Fischer‐Tropsch Nanocatalysts journal December 2020
In Situ TEM Technique Revealing the Deactivation Mechanism of Bimetallic Pd–Ag Nanoparticles in Hydrogen Sensors journal February 2022
Synthesis of monolayer carbon-coated TiO2 as visible-light-responsive photocatalysts journal June 2022
Multimodal Operando Electron Microscopy Approach to Study Pt Catalyst During CO Oxidation Reaction journal August 2019
Robust and Coke-free Ni Catalyst Stabilized by 1–2 nm-Thick Multielement Oxide for Methane Dry Reforming journal September 2021
In Situ/Operando Techniques for Characterization of Single-Atom Catalysts journal February 2019
In situ S/TEM Reactions of Ag/ZrO2/SBA-16 Catalysts for Single-Step Conversion of Ethanol to Butadiene journal August 2019
Possibility of an integrated transmission electron microscope: enabling complex in-situ experiments journal January 2021
Quo Vadis Micro-Electro-Mechanical Systems for the Study of Heterogeneous Catalysts Inside the Electron Microscope? journal November 2020
In Situ Transmission Electron Microscopy for Energy Materials and Devices journal June 2019
2D & 3D in situ study of the calcination of Pd nanocatalysts supported on delta-Alumina in an Environmental Transmission Electron Microscope journal August 2019
In situ and operando electron microscopy in heterogeneous catalysis—insights into multi-scale chemical dynamics journal February 2021
Effects of the Encapsulation Membrane in Operando Scanning Transmission Electron Microscopy journal May 2022
Catalysts by pyrolysis: Direct observation of chemical and morphological transformations leading to transition metal-nitrogen-carbon materials journal July 2021
In Situ TEM Study of the Annealing of Titania Nanotubes for Use as Novel Electrochemistry Based Water Purification Devices journal July 2020
Precise Identification of the Active Phase of Cobalt Catalyst for Carbon Nanotube Growth by In Situ Transmission Electron Microscopy journal December 2020
Growth and Termination Dynamics of Multiwalled Carbon Nanotubes at Near Ambient Pressure: An in Situ Transmission Electron Microscopy Study journal August 2019
In Situ Exsolved Metal Nanoparticles: A Smart Approach for Optimization of Catalysts journal June 2020
Non defect-stabilized thermally stable single-atom catalyst journal January 2019
Direct Microscopic Proof of the Fermi Level Pinning Gas-Sensing Mechanism: The Case of Platinum-Loaded WO 3 journal December 2019
Introducing and Controlling Water Vapor in Closed-Cell In Situ Electron Microscopy Gas Reactions journal March 2020
Visualizing Formation of Intermetallic PdZn in a Palladium/Zinc Oxide Catalyst: Interfacial Fertilization by PdH x journal March 2019