Two-Step Flux Synthesis of Ultrapure Transition-Metal Dichalcogenides

Liu, Song; Liu, Yang; Holtzman, Luke; Li, Baichang; Holbrook, Madisen; Pack, Jordan; Taniguchi, Takashi; Watanabe, Kenji; Dean, Cory R.; Pasupathy, Abhay N.; Barmak, Katayun; Rhodes, Daniel A.; Hone, James

doi:10.1021/acsnano.3c02511

Two-Step Flux Synthesis of Ultrapure Transition-Metal Dichalcogenides

Journal Article · 23 August 2023 · ACS Nano

DOI:https://doi.org/10.1021/acsnano.3c02511· OSTI ID:2420584

Liu, Song ^[1]; ^[2]; Holtzman, Luke ^[3]; ^[2]; Holbrook, Madisen ^[2]; Pack, Jordan ^[4]; ^[5]; ^[5]; Dean, Cory R. ^[4]; ^[4]; Barmak, Katayun ^[3]; ^[2]; ^[2]

Department of Mechanical Engineering, Columbia University, New York, New York 10027, United States; OSTI
Department of Mechanical Engineering, Columbia University, New York, New York 10027, United States
Department of Applied Physics and Applied Mathematics, Columbia University, New York, New York 10027, United States
Department of Physics, Columbia University, New York, New York 10027, United States
National Institute for Materials Science, Tsukuba, Ibaraki 305-0044, Japan

Not provided.

Research Organization:: Columbia Univ., New York, NY (United States)

Sponsoring Organization:: USDOE Office of Science (SC)

DOE Contract Number:: SC0016703

OSTI ID:: 2420584

Journal Information:: ACS Nano, Journal Name: ACS Nano Journal Issue: 17 Vol. 17; ISSN 1936-0851

Publisher:: American Chemical Society (ACS)

Country of Publication:: United States

Language:: English

References (49)

Spatially Selective Enhancement of Photoluminescence in MoS ₂ by Exciton-Mediated Adsorption and Defect Passivation Sivaram, Saujan V.; Hanbicki, Aubrey T.; Rosenberger, Matthew R. ACS Applied Materials & Interfaces, Vol. 11, Issue 17 https://doi.org/10.1021/acsami.9b00390	journal	April 2019
Ambipolar Landau levels and strong band-selective carrier interactions in monolayer WSe2 Gustafsson, Martin V.; Yankowitz, Matthew; Forsythe, Carlos Nature Materials, Vol. 17, Issue 5 https://doi.org/10.1038/s41563-018-0036-2	journal	March 2018
Disorder in van der Waals heterostructures of 2D materials Rhodes, Daniel; Chae, Sang Hoon; Ribeiro-Palau, Rebeca Nature Materials, Vol. 18, Issue 6 https://doi.org/10.1038/s41563-019-0366-8	journal	May 2019
Correlation of crystal quality and extreme magnetoresistance of WTe ₂ Ali, Mazhar N.; Schoop, Leslie; Xiong, Jun EPL (Europhysics Letters), Vol. 110, Issue 6 https://doi.org/10.1209/0295-5075/110/67002	journal	June 2015
Correlated electronic phases in twisted bilayer transition metal dichalcogenides Wang, Lei; Shih, En-Min; Ghiotto, Augusto Nature Materials, Vol. 19, Issue 8 https://doi.org/10.1038/s41563-020-0708-6	journal	June 2020
Quantitative Correlation between Defect Density and Heterogeneous Electron Transfer Rate of Single Layer Graphene Zhong, Jin-Hui; Zhang, Jie; Jin, Xi Journal of the American Chemical Society, Vol. 136, Issue 47 https://doi.org/10.1021/ja508965w	journal	November 2014
Random Strain Fluctuations as Dominant Disorder Source for High-Quality On-Substrate Graphene Devices Couto, Nuno J. G.; Costanzo, Davide; Engels, Stephan Physical Review X, Vol. 4, Issue 4 https://doi.org/10.1103/PhysRevX.4.041019	journal	October 2014
Recent advances in controlled synthesis of two-dimensional transition metal dichalcogenides via vapour deposition techniques Shi, Yumeng; Li, Henan; Li, Lain-Jong Chemical Society Reviews, Vol. 44, Issue 9 https://doi.org/10.1039/C4CS00256C	journal	January 2015
Realizing Large-Scale, Electronic-Grade Two-Dimensional Semiconductors Lin, Yu-Chuan; Jariwala, Bhakti; Bersch, Brian M. ACS Nano, Vol. 12, Issue 2 https://doi.org/10.1021/acsnano.7b07059	journal	January 2018
Defect-Controlled Nucleation and Orientation of WSe ₂ on hBN: A Route to Single-Crystal Epitaxial Monolayers Zhang, Xiaotian; Zhang, Fu; Wang, Yuanxi ACS Nano, Vol. 13, Issue 3 https://doi.org/10.1021/acsnano.8b09230	journal	February 2019
Surface Analysis of WSe 2 Crystals: Spatial and Electronic Variability Addou, Rafik; Wallace, Robert M. ACS Applied Materials & Interfaces, Vol. 8, Issue 39 https://doi.org/10.1021/acsami.6b08847	journal	September 2016
Engineering Point-Defect States in Monolayer WSe ₂ Zhang, Chendong; Wang, Cong; Yang, Feng ACS Nano https://doi.org/10.1021/acsnano.8b07595	journal	February 2019
Odd- and even-denominator fractional quantum Hall states in monolayer WSe2 Shi, Qianhui; Shih, En-Min; Gustafsson, Martin V. Nature Nanotechnology, Vol. 15, Issue 7 https://doi.org/10.1038/s41565-020-0685-6	journal	July 2020
Use of frit-disc crucibles for routine and exploratory solution growth of single crystalline samples Canfield, Paul C.; Kong, Tai; Kaluarachchi, Udhara S. Philosophical Magazine, Vol. 96, Issue 1 https://doi.org/10.1080/14786435.2015.1122248	journal	December 2015
Two-Dimensional Transition Metal Dichalcogenides under Electron Irradiation: Defect Production and Doping Komsa, Hannu-Pekka; Kotakoski, Jani; Kurasch, Simon Physical Review Letters, Vol. 109, Issue 3 https://doi.org/10.1103/PhysRevLett.109.035503	journal	July 2012
Spin–orbit-driven band inversion in bilayer graphene by the van der Waals proximity effect Island, J. O.; Cui, X.; Lewandowski, C. Nature, Vol. 571, Issue 7763 https://doi.org/10.1038/s41586-019-1304-2	journal	June 2019
Atomic Healing of Defects in Transition Metal Dichalcogenides Lu, Junpeng; Carvalho, Alexandra; Chan, Xinhui Kim Nano Letters, Vol. 15, Issue 5 https://doi.org/10.1021/acs.nanolett.5b00952	journal	April 2015
One-Dimensional Electrical Contact to a Two-Dimensional Material Wang, L.; Meric, I.; Huang, P. Y. Science, Vol. 342, Issue 6158 https://doi.org/10.1126/science.1244358	journal	October 2013
The vapour pressure and resistivity of selenium at high temperatures Baker, E. H. Journal of the Chemical Society A: Inorganic, Physical, Theoretical https://doi.org/10.1039/j19680001089	journal	January 1968
Fermi Level Pinning Dependent 2D Semiconductor Devices: Challenges and Prospects Liu, Xiaochi; Choi, Min Sup; Hwang, Euyheon Advanced Materials, Vol. 34, Issue 15 https://doi.org/10.1002/adma.202108425	journal	February 2022
Thermally Induced Defects on WSe ₂ Blades, William H.; Frady, Nicholas J.; Litwin, Peter M. The Journal of Physical Chemistry C, Vol. 124, Issue 28 https://doi.org/10.1021/acs.jpcc.0c04440	journal	June 2020
Upward mobility rocks! Schlom, Darrell G.; Pfeiffer, Loren N. Nature Materials, Vol. 9, Issue 11 https://doi.org/10.1038/nmat2888	journal	October 2010
Synthesis of hexagonal boron nitride heterostructures for 2D van der Waals electronics Kim, Ki Kang; Lee, Hyun Seok; Lee, Young Hee Chemical Society Reviews, Vol. 47, Issue 16 https://doi.org/10.1039/C8CS00450A	journal	January 2018
Ultrafast growth of large single crystals of monolayer WS2 and WSe2 Zhang, Zhengwei; Chen, Peng; Yang, Xiangdong National Science Review, Vol. 7, Issue 4 https://doi.org/10.1093/nsr/nwz223	journal	January 2020
Charge Scattering and Mobility in Atomically Thin Semiconductors Ma, Nan; Jena, Debdeep Physical Review X, Vol. 4, Issue 1 https://doi.org/10.1103/PhysRevX.4.011043	journal	March 2014
General synthesis of two-dimensional van der Waals heterostructure arrays Li, Jia; Yang, Xiangdong; Liu, Yang Nature, Vol. 579, Issue 7799 https://doi.org/10.1038/s41586-020-2098-y	journal	March 2020
Hysteresis-Free High Mobility Graphene Encapsulated in Tungsten Disulfide Soundarapandian, Karuppasamy Pandian; De Fazio, Domenico; Tongay, Sefaattin arXiv https://doi.org/10.48550/arXiv.2207.12836	preprint	January 2022
Low-resistance metal contacts to encapsulated semiconductor monolayers with long transfer length Liu, Yang; Liu, Song; Wang, Zhiying Nature Electronics, Vol. 5, Issue 9 https://doi.org/10.1038/s41928-022-00808-9	journal	September 2022
End-Bonded Metal Contacts on WSe₂ Field-Effect Transistors Chu, Chun-Hao; Lin, Ho-Chun; Yeh, Chao-Hui ACS Nano, Vol. 13, Issue 7 https://doi.org/10.1021/acsnano.9b03250	journal	June 2019
Spontaneous doping of the basal plane of MoS2 single layers through oxygen substitution under ambient conditions Pető, János; Ollár, Tamás; Vancsó, Péter Nature Chemistry, Vol. 10, Issue 12 https://doi.org/10.1038/s41557-018-0136-2	journal	September 2018
Hofstadter’s butterfly and the fractal quantum Hall effect in moiré superlattices Dean, C. R.; Wang, L.; Maher, P. Nature, Vol. 497, Issue 7451 https://doi.org/10.1038/nature12186	journal	May 2013
Atomic structure of defects and dopants in 2D layered transition metal dichalcogenides Wang, Shanshan; Robertson, Alex; Warner, Jamie H. Chemical Society Reviews, Vol. 47, Issue 17 https://doi.org/10.1039/C8CS00236C	journal	January 2018
Conformal hexagonal-boron nitride dielectric interface for tungsten diselenide devices with improved mobility and thermal dissipation Liu, Donghua; Chen, Xiaosong; Yan, Yaping Nature Communications, Vol. 10, Issue 1 https://doi.org/10.1038/s41467-019-09016-0	journal	March 2019
Origin of phonon-limited mobility in two-dimensional metal dichalcogenides Chang, Hao; Wang, Hao; Song, Ke-Ke Journal of Physics: Condensed Matter, Vol. 34, Issue 1 https://doi.org/10.1088/1361-648X/ac29e1	journal	October 2021
Adsorption and Dissociation of H₂O on Monolayered MoS₂ Edges: Energetics and Mechanism from ab Initio Simulations Ghuman, Kulbir Kaur; Yadav, Shwetank; Singh, Chandra Veer The Journal of Physical Chemistry C, Vol. 119, Issue 12 https://doi.org/10.1021/jp510899m	journal	March 2015
2D materials and van der Waals heterostructures Novoselov, K. S.; Mishchenko, A.; Carvalho, A. Science, Vol. 353, Issue 6298 https://doi.org/10.1126/science.aac9439	journal	July 2016
2D transition metal dichalcogenides Manzeli, Sajedeh; Ovchinnikov, Dmitry; Pasquier, Diego Nature Reviews Materials, Vol. 2, Issue 8 https://doi.org/10.1038/natrevmats.2017.33	journal	June 2017
Air Passivation of Chalcogen Vacancies in Two-Dimensional Semiconductors Liu, Yuanyue; Stradins, Pauls; Wei, Su-Huai Angewandte Chemie, Vol. 128, Issue 3 https://doi.org/10.1002/ange.201508828	journal	November 2015
Identifying substitutional oxygen as a prolific point defect in monolayer transition metal dichalcogenides Barja, Sara; Refaely-Abramson, Sivan; Schuler, Bruno Nature Communications, Vol. 10, Issue 1 https://doi.org/10.1038/s41467-019-11342-2	journal	July 2019
Electronics and optoelectronics of two-dimensional transition metal dichalcogenides Wang, Qing Hua; Kalantar-Zadeh, Kourosh; Kis, Andras Nature Nanotechnology, Vol. 7, Issue 11, p. 699-712 https://doi.org/10.1038/nnano.2012.193	journal	November 2012
Approaching the Intrinsic Limit in Transition Metal Diselenides via Point Defect Control Edelberg, Drew; Rhodes, Daniel; Kerelsky, Alexander Nano Letters, Vol. 19, Issue 7 https://doi.org/10.1021/acs.nanolett.9b00985	journal	June 2019
Point Defects and Localized Excitons in 2D WSe ₂ Zheng, Yu Jie; Chen, Yifeng; Huang, Yu Li ACS Nano, Vol. 13, Issue 5 https://doi.org/10.1021/acsnano.9b02316	journal	April 2019
Defect Structure of Localized Excitons in a WSe 2 Monolayer Zhang, Shuai; Wang, Chen-Guang; Li, Ming-Yang Physical Review Letters, Vol. 119, Issue 4 https://doi.org/10.1103/PhysRevLett.119.046101	journal	July 2017
A practical guide for crystal growth of van der Waals layered materials May, Andrew F.; Yan, Jiaqiang; McGuire, Michael A. Journal of Applied Physics, Vol. 128, Issue 5 https://doi.org/10.1063/5.0015971	journal	August 2020
Mixed-dimensional van der Waals heterostructures Jariwala, Deep; Marks, Tobin J.; Hersam, Mark C. Nature Materials, Vol. 16, Issue 2 https://doi.org/10.1038/nmat4703	journal	August 2016
Interaction- and defect-free van der Waals contacts between metals and two-dimensional semiconductors Kwon, Gihyeon; Choi, Yoon-Ho; Lee, Hyangsook Nature Electronics, Vol. 5, Issue 4 https://doi.org/10.1038/s41928-022-00746-6	journal	April 2022
Boron nitride substrates for high-quality graphene electronics Dean, C. R.; Young, A. F.; Meric, I. Nature Nanotechnology, Vol. 5, Issue 10, p. 722-726 https://doi.org/10.1038/nnano.2010.172	journal	August 2010
Composition of liquid-Saturated selenium vapor Rao, Y. K. Metallurgical Transactions B, Vol. 14, Issue 2 https://doi.org/10.1007/BF02661030	journal	June 1983
Hexagonal Boron Nitride Single Crystal Growth from Solution with a Temperature Gradient Li, Jiahan; Yuan, Chao; Elias, Christine Chemistry of Materials, Vol. 32, Issue 12 https://doi.org/10.1021/acs.chemmater.0c00830	journal	May 2020

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