Software for HUBER-5042 diffractometer with Displex DE-202 helium cryostat
- Russian Academy of Sciences, Shubnikov Institute of Crystallography (Russian Federation)
A software for structural studies on a Huber-5042 diffractometer with a point detector and closed-cycle Displex DE-202 helium cryostat has been developed. The software package includes programs for the preliminary stage of experiment, planning, data collection, profile analysis of reflections, etc. The measurement of reflections in the 2θ angular range from 0° to 152° is provided, which is unique for Eulerian goniometers. Tools for enhancing data collection are demonstrated. Accurate experimental data are obtained for a test CaF{sub 2} crystal (sp. gr. Fm3̄m, Z = 4, resolution sinθ/λ{sub max} ≈ 1.354 Å{sup −1}, 121 reflections, 16 parameters in refinement, R/wR = 0.31/0.34%, Δρ{sub min}/Δρ{sub max} = −0.08/+0.07 e/Å{sup 3}).
- OSTI ID:
- 22722870
- Journal Information:
- Crystallography Reports, Vol. 60, Issue 2; Other Information: Copyright (c) 2015 Pleiades Publishing, Inc.; Country of input: International Atomic Energy Agency (IAEA); ISSN 1063-7745
- Country of Publication:
- United States
- Language:
- English
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