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Title: A facile mechanochemical approach to synthesize Zn-Al layered double hydroxide

Abstract

In this study, a mechanochemical route to synthesize Zn-Al layered double hydroxide (LDH) was introduced, in which Zn basic carbonate and Al hydroxide were first dry milled into an activated state and then agitated in water to obtain the final products. The as-prepared samples were characterized by X-ray diffraction (XRD), Fourier transform infrared spectroscopy (FT-IR), Thermogravimetry (TG) and Scanning electron microscopy (SEM). The products possessed a high crystallinity of Zn–Al LDH phase without any other impurities, proving a facile and effective preparation of Zn–Al LDH by using non-heating mechanochemical approach. - Highlights: • A non-heating mechanochemical route to synthesize Zn-Al LDH. • The products possessed high crystalline Zn-Al LDH phase. • No emission of other impurities or wastewater.

Authors:
 [1]; ; ;  [1];  [1];  [2]
  1. School of Resources and Environmental Engineering, Wuhan University of Technology, Luoshi Road 122, Wuhan, Hubei 430070 (China)
  2. College of Ecological Environment and Urban Construction, Fujian University of Technology, Fuzhou 350118 (China)
Publication Date:
OSTI Identifier:
22658282
Resource Type:
Journal Article
Resource Relation:
Journal Name: Journal of Solid State Chemistry; Journal Volume: 250; Other Information: Copyright (c) 2017 Elsevier Science B.V., Amsterdam, The Netherlands, All rights reserved.; Country of input: International Atomic Energy Agency (IAEA)
Country of Publication:
United States
Language:
English
Subject:
37 INORGANIC, ORGANIC, PHYSICAL AND ANALYTICAL CHEMISTRY; ALUMINIUM COMPOUNDS; EXPERIMENTAL DATA; FOURIER TRANSFORM SPECTROMETERS; INFRARED SPECTRA; SCANNING ELECTRON MICROSCOPY; SYNTHESIS; THERMAL GRAVIMETRIC ANALYSIS; WASTE WATER; X-RAY DIFFRACTION; ZINC COMPOUNDS

Citation Formats

Qu, Jun, E-mail: forsjun@whut.edu.cn, He, Xiaoman, Chen, Min, Huang, Pengwu, Zhang, Qiwu, E-mail: zhangqw@whut.edu.cn, and Liu, Xinzhong. A facile mechanochemical approach to synthesize Zn-Al layered double hydroxide. United States: N. p., 2017. Web. doi:10.1016/J.JSSC.2017.03.013.
Qu, Jun, E-mail: forsjun@whut.edu.cn, He, Xiaoman, Chen, Min, Huang, Pengwu, Zhang, Qiwu, E-mail: zhangqw@whut.edu.cn, & Liu, Xinzhong. A facile mechanochemical approach to synthesize Zn-Al layered double hydroxide. United States. doi:10.1016/J.JSSC.2017.03.013.
Qu, Jun, E-mail: forsjun@whut.edu.cn, He, Xiaoman, Chen, Min, Huang, Pengwu, Zhang, Qiwu, E-mail: zhangqw@whut.edu.cn, and Liu, Xinzhong. Thu . "A facile mechanochemical approach to synthesize Zn-Al layered double hydroxide". United States. doi:10.1016/J.JSSC.2017.03.013.
@article{osti_22658282,
title = {A facile mechanochemical approach to synthesize Zn-Al layered double hydroxide},
author = {Qu, Jun, E-mail: forsjun@whut.edu.cn and He, Xiaoman and Chen, Min and Huang, Pengwu and Zhang, Qiwu, E-mail: zhangqw@whut.edu.cn and Liu, Xinzhong},
abstractNote = {In this study, a mechanochemical route to synthesize Zn-Al layered double hydroxide (LDH) was introduced, in which Zn basic carbonate and Al hydroxide were first dry milled into an activated state and then agitated in water to obtain the final products. The as-prepared samples were characterized by X-ray diffraction (XRD), Fourier transform infrared spectroscopy (FT-IR), Thermogravimetry (TG) and Scanning electron microscopy (SEM). The products possessed a high crystallinity of Zn–Al LDH phase without any other impurities, proving a facile and effective preparation of Zn–Al LDH by using non-heating mechanochemical approach. - Highlights: • A non-heating mechanochemical route to synthesize Zn-Al LDH. • The products possessed high crystalline Zn-Al LDH phase. • No emission of other impurities or wastewater.},
doi = {10.1016/J.JSSC.2017.03.013},
journal = {Journal of Solid State Chemistry},
number = ,
volume = 250,
place = {United States},
year = {Thu Jun 15 00:00:00 EDT 2017},
month = {Thu Jun 15 00:00:00 EDT 2017}
}