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Title: Crystal structure of 2-(thiophen-2-yl)-1-(5-thioxo-4,5-dihydro-1,3,4-oxadiazol-2-yl) ethenyl]benzamide: N,N-dimethylformamide (1 : 1)

Abstract

The title compound, 2-(thiophen-2-yl)-1-(5-thioxo-4,5-dihydro-1,3,4-oxadiazol-2-yl)ethenyl] benzamide:N,N-dimethylformamide (1: 1), (C{sub 15}H{sub 11}N{sub 3}O{sub 2}S{sub 2} · C{sub 3}H{sub 7}NO), was synthesized, and its structure was established by spectral analysis and X-ray diffraction studies. The compound crystallizes in the monoclinic space group P2{sub 1}/n with a = 10.8714(7), b = 9.0497(5), c = 19.8347(13) Å, β = 91.093(5)°, Z = 4. The crystal structure is stabilized by N–H···S, C–H···O and N–H···O hydrogen bonds. The π···π interactions are also observed between the rings.

Authors:
 [1]; ;  [2];  [3];  [1]
  1. University of Jammu, X-ray Crystallography Laboratory, Department of Physics (India)
  2. Mangalore University, Department of Chemistry (India)
  3. Mangalore University, Industrial Chemistry Division, Department of Studies in Chemistry (India)
Publication Date:
OSTI Identifier:
22645578
Resource Type:
Journal Article
Resource Relation:
Journal Name: Crystallography Reports; Journal Volume: 61; Journal Issue: 2; Other Information: Copyright (c) 2016 Pleiades Publishing, Inc.; Country of input: International Atomic Energy Agency (IAEA)
Country of Publication:
United States
Language:
English
Subject:
75 CONDENSED MATTER PHYSICS, SUPERCONDUCTIVITY AND SUPERFLUIDITY; CRYSTAL STRUCTURE; MONOCLINIC LATTICES; SPACE GROUPS; X-RAY DIFFRACTION

Citation Formats

Sharma, P., Subbulakshmi, K. N., Narayana, B., Sarojini, B. K., and Kant, R., E-mail: rkant.ju@gmail.com. Crystal structure of 2-(thiophen-2-yl)-1-(5-thioxo-4,5-dihydro-1,3,4-oxadiazol-2-yl) ethenyl]benzamide: N,N-dimethylformamide (1 : 1). United States: N. p., 2016. Web. doi:10.1134/S106377451602022X.
Sharma, P., Subbulakshmi, K. N., Narayana, B., Sarojini, B. K., & Kant, R., E-mail: rkant.ju@gmail.com. Crystal structure of 2-(thiophen-2-yl)-1-(5-thioxo-4,5-dihydro-1,3,4-oxadiazol-2-yl) ethenyl]benzamide: N,N-dimethylformamide (1 : 1). United States. doi:10.1134/S106377451602022X.
Sharma, P., Subbulakshmi, K. N., Narayana, B., Sarojini, B. K., and Kant, R., E-mail: rkant.ju@gmail.com. Tue . "Crystal structure of 2-(thiophen-2-yl)-1-(5-thioxo-4,5-dihydro-1,3,4-oxadiazol-2-yl) ethenyl]benzamide: N,N-dimethylformamide (1 : 1)". United States. doi:10.1134/S106377451602022X.
@article{osti_22645578,
title = {Crystal structure of 2-(thiophen-2-yl)-1-(5-thioxo-4,5-dihydro-1,3,4-oxadiazol-2-yl) ethenyl]benzamide: N,N-dimethylformamide (1 : 1)},
author = {Sharma, P. and Subbulakshmi, K. N. and Narayana, B. and Sarojini, B. K. and Kant, R., E-mail: rkant.ju@gmail.com},
abstractNote = {The title compound, 2-(thiophen-2-yl)-1-(5-thioxo-4,5-dihydro-1,3,4-oxadiazol-2-yl)ethenyl] benzamide:N,N-dimethylformamide (1: 1), (C{sub 15}H{sub 11}N{sub 3}O{sub 2}S{sub 2} · C{sub 3}H{sub 7}NO), was synthesized, and its structure was established by spectral analysis and X-ray diffraction studies. The compound crystallizes in the monoclinic space group P2{sub 1}/n with a = 10.8714(7), b = 9.0497(5), c = 19.8347(13) Å, β = 91.093(5)°, Z = 4. The crystal structure is stabilized by N–H···S, C–H···O and N–H···O hydrogen bonds. The π···π interactions are also observed between the rings.},
doi = {10.1134/S106377451602022X},
journal = {Crystallography Reports},
number = 2,
volume = 61,
place = {United States},
year = {Tue Mar 15 00:00:00 EDT 2016},
month = {Tue Mar 15 00:00:00 EDT 2016}
}