High T{sub g} and fast curing epoxy-based anisotropic conductive paste for electronic packaging
- Department of Chemical Engineering, Faculty of Engineering, Chulalongkorn University, Bangkok, 10330 (Thailand)
Herein, our main objective is to prepare the fast curing epoxy system with high glass transition temperature (T{sub g}) by incorporating the multifunctional epoxy resin into the mixture of diglycidyl ether of bisphenol A (DGEBA) as a major epoxy component and aromatic diamine as a hardener. Furthermore, the curing behavior as well as thermal and thermomechanical properties were investigated by differential scanning calorimetry (DSC), dynamic mechanical analysis (DMA) and thermomechanical analysis (TMA). It was found that T{sub g} obtained from tan δ of DGEBA/aromatic diamine system increased from 100 °C to 205 °C with the presence of 30 percentage by weight of multifunctional epoxy resin. Additionally, the isothermal DSC results showed that the multifunctional epoxy resin can accelerate the curing reaction of DGEBA/aromatic diamine system. Namely, a high degree of curing (∼90%) was achieved after a few minutes of curing at low temperature of 130 °C, owing to a large number of epoxy ring of multifunctional epoxy resin towards the active hydrogen atoms of aromatic diamine.
- OSTI ID:
- 22589319
- Journal Information:
- AIP Conference Proceedings, Vol. 1713, Issue 1; Conference: PPS-31: 31. international conference of the Polymer Processing Society, Jeju Island (Korea, Republic of), 7-11 Jun 2015; Other Information: (c) 2016 AIP Publishing LLC; Country of input: International Atomic Energy Agency (IAEA); ISSN 0094-243X
- Country of Publication:
- United States
- Language:
- English
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Related Subjects
ORGANIC
PHYSICAL AND ANALYTICAL CHEMISTRY
71 CLASSICAL AND QUANTUM MECHANICS
GENERAL PHYSICS
AMINES
ANISOTROPY
CALORIMETRY
CURING
DIFFERENTIAL THERMAL ANALYSIS
ELECTRIC CONDUCTIVITY
EPOXIDES
ETHERS
GLASS
HYDROGEN
MIXTURES
RELAXATION LOSSES
RESINS
TEMPERATURE DEPENDENCE
TRANSITION TEMPERATURE