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Title: Portable ultrahigh-vacuum sample storage system for polarization-dependent total-reflection fluorescence x-ray absorption fine structure spectroscopy

Abstract

A portable ultrahigh-vacuum sample storage system was designed and built to investigate the detailed geometric structures of mass-selected metal clusters on oxide substrates by polarization-dependent total-reflection fluorescence x-ray absorption fine structure spectroscopy (PTRF-XAFS). This ultrahigh-vacuum (UHV) sample storage system provides the handover of samples between two different sample manipulating systems. The sample storage system is adaptable for public transportation, facilitating experiments using air-sensitive samples in synchrotron radiation or other quantum beam facilities. The samples were transferred by the developed portable UHV transfer system via a public transportation at a distance over 400 km. The performance of the transfer system was demonstrated by a successful PTRF-XAFS study of Pt{sub 4} clusters deposited on a TiO{sub 2}(110) surface.

Authors:
; ; ; ;  [1]; ; ;  [2];  [3]
  1. Toyota Central R&D Labs., Inc., Yokomichi 41-1, Nagakute, Aichi 480-1192 (Japan)
  2. Catalysis Research Center, Hokkaido University, Kita 21-10, Sapporo, Hokkaido 001-0021 (Japan)
  3. AVC Co., Ltd., Inada 1450-6, Hitachinaka, Ibaraki 312-0061 (Japan)
Publication Date:
OSTI Identifier:
22489813
Resource Type:
Journal Article
Resource Relation:
Journal Name: Journal of Vacuum Science and Technology. A, Vacuum, Surfaces and Films; Journal Volume: 34; Journal Issue: 2; Other Information: (c) 2015 American Vacuum Society; Country of input: International Atomic Energy Agency (IAEA)
Country of Publication:
United States
Language:
English
Subject:
37 INORGANIC, ORGANIC, PHYSICAL AND ANALYTICAL CHEMISTRY; 42 ENGINEERING; ABSORPTION SPECTROSCOPY; DESIGN; FINE STRUCTURE; FLUORESCENCE; POLARIZATION; PRESSURE RANGE BELOW 1 NANO PA; SUBSTRATES; SURFACES; SYNCHROTRON RADIATION; TITANIUM OXIDES; X-RAY SPECTROSCOPY

Citation Formats

Watanabe, Yoshihide, E-mail: e0827@mosk.tytlabs.co.jp, Nishimura, Yusaku F., Suzuki, Ryo, Beniya, Atsushi, Isomura, Noritake, Uehara, Hiromitsu, Asakura, Kiyotaka, Takakusagi, Satoru, and Nimura, Tomoyuki. Portable ultrahigh-vacuum sample storage system for polarization-dependent total-reflection fluorescence x-ray absorption fine structure spectroscopy. United States: N. p., 2016. Web. doi:10.1116/1.4936344.
Watanabe, Yoshihide, E-mail: e0827@mosk.tytlabs.co.jp, Nishimura, Yusaku F., Suzuki, Ryo, Beniya, Atsushi, Isomura, Noritake, Uehara, Hiromitsu, Asakura, Kiyotaka, Takakusagi, Satoru, & Nimura, Tomoyuki. Portable ultrahigh-vacuum sample storage system for polarization-dependent total-reflection fluorescence x-ray absorption fine structure spectroscopy. United States. doi:10.1116/1.4936344.
Watanabe, Yoshihide, E-mail: e0827@mosk.tytlabs.co.jp, Nishimura, Yusaku F., Suzuki, Ryo, Beniya, Atsushi, Isomura, Noritake, Uehara, Hiromitsu, Asakura, Kiyotaka, Takakusagi, Satoru, and Nimura, Tomoyuki. Tue . "Portable ultrahigh-vacuum sample storage system for polarization-dependent total-reflection fluorescence x-ray absorption fine structure spectroscopy". United States. doi:10.1116/1.4936344.
@article{osti_22489813,
title = {Portable ultrahigh-vacuum sample storage system for polarization-dependent total-reflection fluorescence x-ray absorption fine structure spectroscopy},
author = {Watanabe, Yoshihide, E-mail: e0827@mosk.tytlabs.co.jp and Nishimura, Yusaku F. and Suzuki, Ryo and Beniya, Atsushi and Isomura, Noritake and Uehara, Hiromitsu and Asakura, Kiyotaka and Takakusagi, Satoru and Nimura, Tomoyuki},
abstractNote = {A portable ultrahigh-vacuum sample storage system was designed and built to investigate the detailed geometric structures of mass-selected metal clusters on oxide substrates by polarization-dependent total-reflection fluorescence x-ray absorption fine structure spectroscopy (PTRF-XAFS). This ultrahigh-vacuum (UHV) sample storage system provides the handover of samples between two different sample manipulating systems. The sample storage system is adaptable for public transportation, facilitating experiments using air-sensitive samples in synchrotron radiation or other quantum beam facilities. The samples were transferred by the developed portable UHV transfer system via a public transportation at a distance over 400 km. The performance of the transfer system was demonstrated by a successful PTRF-XAFS study of Pt{sub 4} clusters deposited on a TiO{sub 2}(110) surface.},
doi = {10.1116/1.4936344},
journal = {Journal of Vacuum Science and Technology. A, Vacuum, Surfaces and Films},
number = 2,
volume = 34,
place = {United States},
year = {Tue Mar 15 00:00:00 EDT 2016},
month = {Tue Mar 15 00:00:00 EDT 2016}
}