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Title: Calcium and zirconium as texture modifiers during rolling and annealing of magnesium–zinc alloys

Abstract

Rolling experiments were carried out on a ternary Mg–Zn–Ca alloy and its modification with zirconium. Short time annealing of as-rolled sheets is used to reveal the microstructure and texture development. The texture of the as-rolled sheets can be characterised by basal pole figures with split peak towards the rolling direction (RD) and a broad transverse angular spread of basal planes towards the transverse direction (TD). During annealing the RD split peaks as well as orientations in the sheet plane vanish whereas the distribution of orientations tilted towards the TD remains. It is shown in EBSD measurements that during rolling bands of twin containing structures form. During subsequent annealing basal orientations close to the sheet plane vanish based on a grain nucleation and growth mechanism of recrystallisation. Orientations with tilt towards the TD remain in grains that do not undergo such a mechanism. The addition of Zr delays texture weakening. - Highlights: • Ca in Mg–Zn-alloys contributes to a significant texture weakening during rolling and annealing. • Grain nucleation and growth in structures consisting of twins explain a texture randomisation during annealing. • Grains with transverse tilt of basal planes preferentially do not undergo a grain nucleation and growth mechanism. •more » Zr delays the microstructure and texture development.« less

Authors:
; ; ; ; ;
Publication Date:
OSTI Identifier:
22476059
Resource Type:
Journal Article
Resource Relation:
Journal Name: Materials Characterization; Journal Volume: 101; Other Information: Copyright (c) 2015 Elsevier Science B.V., Amsterdam, The Netherlands, All rights reserved.; Country of input: International Atomic Energy Agency (IAEA)
Country of Publication:
United States
Language:
English
Subject:
36 MATERIALS SCIENCE; ANNEALING; BACKSCATTERING; CALCIUM ADDITIONS; DISTRIBUTION; ELECTRON DIFFRACTION; MAGNESIUM ALLOYS; MICROSTRUCTURE; MODIFICATIONS; RECRYSTALLIZATION; TEXTURE; X-RAY DIFFRACTION; ZINC ALLOYS; ZIRCONIUM ADDITIONS

Citation Formats

Bohlen, Jan, E-mail: jan.bohlen@hzg.de, Wendt, Joachim, Nienaber, Maria, Kainer, Karl Ulrich, Stutz, Lennart, and Letzig, Dietmar. Calcium and zirconium as texture modifiers during rolling and annealing of magnesium–zinc alloys. United States: N. p., 2015. Web. doi:10.1016/J.MATCHAR.2015.02.002.
Bohlen, Jan, E-mail: jan.bohlen@hzg.de, Wendt, Joachim, Nienaber, Maria, Kainer, Karl Ulrich, Stutz, Lennart, & Letzig, Dietmar. Calcium and zirconium as texture modifiers during rolling and annealing of magnesium–zinc alloys. United States. doi:10.1016/J.MATCHAR.2015.02.002.
Bohlen, Jan, E-mail: jan.bohlen@hzg.de, Wendt, Joachim, Nienaber, Maria, Kainer, Karl Ulrich, Stutz, Lennart, and Letzig, Dietmar. Sun . "Calcium and zirconium as texture modifiers during rolling and annealing of magnesium–zinc alloys". United States. doi:10.1016/J.MATCHAR.2015.02.002.
@article{osti_22476059,
title = {Calcium and zirconium as texture modifiers during rolling and annealing of magnesium–zinc alloys},
author = {Bohlen, Jan, E-mail: jan.bohlen@hzg.de and Wendt, Joachim and Nienaber, Maria and Kainer, Karl Ulrich and Stutz, Lennart and Letzig, Dietmar},
abstractNote = {Rolling experiments were carried out on a ternary Mg–Zn–Ca alloy and its modification with zirconium. Short time annealing of as-rolled sheets is used to reveal the microstructure and texture development. The texture of the as-rolled sheets can be characterised by basal pole figures with split peak towards the rolling direction (RD) and a broad transverse angular spread of basal planes towards the transverse direction (TD). During annealing the RD split peaks as well as orientations in the sheet plane vanish whereas the distribution of orientations tilted towards the TD remains. It is shown in EBSD measurements that during rolling bands of twin containing structures form. During subsequent annealing basal orientations close to the sheet plane vanish based on a grain nucleation and growth mechanism of recrystallisation. Orientations with tilt towards the TD remain in grains that do not undergo such a mechanism. The addition of Zr delays texture weakening. - Highlights: • Ca in Mg–Zn-alloys contributes to a significant texture weakening during rolling and annealing. • Grain nucleation and growth in structures consisting of twins explain a texture randomisation during annealing. • Grains with transverse tilt of basal planes preferentially do not undergo a grain nucleation and growth mechanism. • Zr delays the microstructure and texture development.},
doi = {10.1016/J.MATCHAR.2015.02.002},
journal = {Materials Characterization},
number = ,
volume = 101,
place = {United States},
year = {Sun Mar 15 00:00:00 EDT 2015},
month = {Sun Mar 15 00:00:00 EDT 2015}
}