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Title: Facile synthesis of α-Fe{sub 2}O{sub 3} nanoparticles for high-performance CO gas sensor

Abstract

Highlights: • We have demonstrated a facile method to prepare Fe{sub 2}O{sub 3} nanoparticles. • The gas sensing properties of α-Fe{sub 2}O{sub 3} have been invested. • The results show potential application of α-Fe{sub 2}O{sub 3} NPs for CO sensors in environmental monitoring. - Abstract: Iron oxide nanoparticles (NPs) were prepared via a simple hydrothermal method for high performance CO gas sensor. The synthesized α-Fe{sub 2}O{sub 3} NPs were characterized by X-ray diffraction, nitrogen adsorption/desorption isotherm, scanning electron microscopy (SEM), transmission electron microscopy (TEM), high-resolution transmission electron microscopy (HRTEM), and selected area electron diffraction (SAED). The SEM, TEM results revealed that obtained α-Fe{sub 2}O{sub 3} particles had a peanut-like geometry with hemispherical ends. The response of the α-Fe{sub 2}O{sub 3} NPs based sensor to carbon monoxide (CO) and various concentrations of other gases were measured at different temperatures. It found that the sensor based on the peanut-like α-Fe{sub 2}O{sub 3} NPs exhibited high response, fast response–recovery, and good selectivity to CO at 300 °C. The experimental results clearly demonstrated the potential application of α-Fe{sub 2}O{sub 3} NPs as a good sensing material in the fabrication of CO sensor.

Authors:
;  [1];  [2];  [3];  [4];  [5]
  1. College of Sciences, Hue University, 77 Nguyen Hue, Phu Nhuan Ward, Hue City (Viet Nam)
  2. College of Education, Hue University, 34 Le Loi, Hue City (Viet Nam)
  3. Centre for Environmental Technology and Sustainable Development (CETASD), Hanoi University of Science, 334 Nguyen Trai, Hanoi (Viet Nam)
  4. Graduate University of Science and Technology, Vietnamese Academy of Science and Technology, Hanoi (Viet Nam)
  5. International Training Institute for Materials Science (ITIMS), Hanoi University of Science and Technology (HUST), No. 1, Dai Co Viet, Hanoi (Viet Nam)
Publication Date:
OSTI Identifier:
22475858
Resource Type:
Journal Article
Journal Name:
Materials Research Bulletin
Additional Journal Information:
Journal Volume: 68; Other Information: Copyright (c) 2015 Elsevier Science B.V., Amsterdam, The Netherlands, All rights reserved.; Country of input: International Atomic Energy Agency (IAEA); Journal ID: ISSN 0025-5408
Country of Publication:
United States
Language:
English
Subject:
77 NANOSCIENCE AND NANOTECHNOLOGY; ABUNDANCE; ADSORPTION; CARBON MONOXIDE; ELECTRON DIFFRACTION; GASES; HYDROTHERMAL SYNTHESIS; IRON OXIDES; IRON-ALPHA; ISOTHERMS; NANOPARTICLES; NITROGEN; PERFORMANCE; RESOLUTION; SCANNING ELECTRON MICROSCOPY; SENSORS; TRANSMISSION ELECTRON MICROSCOPY; X-RAY DIFFRACTION

Citation Formats

Cuong, Nguyen Duc, E-mail: nguyenduccuong@hueuni.edu.vn, Faculty of Hospitality and Tourism, Hue University, 22 Lam Hoang, Vy Da Ward, Hue City, Khieu, Dinh Quang, Hoa, Tran Thai, Quang, Duong Tuan, Viet, Pham Hung, Lam, Tran Dai, Hoa, Nguyen Duc, and Hieu, Nguyen Van, E-mail: hieu@itims.edu.vn. Facile synthesis of α-Fe{sub 2}O{sub 3} nanoparticles for high-performance CO gas sensor. United States: N. p., 2015. Web. doi:10.1016/J.MATERRESBULL.2015.03.069.
Cuong, Nguyen Duc, E-mail: nguyenduccuong@hueuni.edu.vn, Faculty of Hospitality and Tourism, Hue University, 22 Lam Hoang, Vy Da Ward, Hue City, Khieu, Dinh Quang, Hoa, Tran Thai, Quang, Duong Tuan, Viet, Pham Hung, Lam, Tran Dai, Hoa, Nguyen Duc, & Hieu, Nguyen Van, E-mail: hieu@itims.edu.vn. Facile synthesis of α-Fe{sub 2}O{sub 3} nanoparticles for high-performance CO gas sensor. United States. doi:10.1016/J.MATERRESBULL.2015.03.069.
Cuong, Nguyen Duc, E-mail: nguyenduccuong@hueuni.edu.vn, Faculty of Hospitality and Tourism, Hue University, 22 Lam Hoang, Vy Da Ward, Hue City, Khieu, Dinh Quang, Hoa, Tran Thai, Quang, Duong Tuan, Viet, Pham Hung, Lam, Tran Dai, Hoa, Nguyen Duc, and Hieu, Nguyen Van, E-mail: hieu@itims.edu.vn. Sat . "Facile synthesis of α-Fe{sub 2}O{sub 3} nanoparticles for high-performance CO gas sensor". United States. doi:10.1016/J.MATERRESBULL.2015.03.069.
@article{osti_22475858,
title = {Facile synthesis of α-Fe{sub 2}O{sub 3} nanoparticles for high-performance CO gas sensor},
author = {Cuong, Nguyen Duc, E-mail: nguyenduccuong@hueuni.edu.vn and Faculty of Hospitality and Tourism, Hue University, 22 Lam Hoang, Vy Da Ward, Hue City and Khieu, Dinh Quang and Hoa, Tran Thai and Quang, Duong Tuan and Viet, Pham Hung and Lam, Tran Dai and Hoa, Nguyen Duc and Hieu, Nguyen Van, E-mail: hieu@itims.edu.vn},
abstractNote = {Highlights: • We have demonstrated a facile method to prepare Fe{sub 2}O{sub 3} nanoparticles. • The gas sensing properties of α-Fe{sub 2}O{sub 3} have been invested. • The results show potential application of α-Fe{sub 2}O{sub 3} NPs for CO sensors in environmental monitoring. - Abstract: Iron oxide nanoparticles (NPs) were prepared via a simple hydrothermal method for high performance CO gas sensor. The synthesized α-Fe{sub 2}O{sub 3} NPs were characterized by X-ray diffraction, nitrogen adsorption/desorption isotherm, scanning electron microscopy (SEM), transmission electron microscopy (TEM), high-resolution transmission electron microscopy (HRTEM), and selected area electron diffraction (SAED). The SEM, TEM results revealed that obtained α-Fe{sub 2}O{sub 3} particles had a peanut-like geometry with hemispherical ends. The response of the α-Fe{sub 2}O{sub 3} NPs based sensor to carbon monoxide (CO) and various concentrations of other gases were measured at different temperatures. It found that the sensor based on the peanut-like α-Fe{sub 2}O{sub 3} NPs exhibited high response, fast response–recovery, and good selectivity to CO at 300 °C. The experimental results clearly demonstrated the potential application of α-Fe{sub 2}O{sub 3} NPs as a good sensing material in the fabrication of CO sensor.},
doi = {10.1016/J.MATERRESBULL.2015.03.069},
journal = {Materials Research Bulletin},
issn = {0025-5408},
number = ,
volume = 68,
place = {United States},
year = {2015},
month = {8}
}