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Title: Effect of gamma irradiation on the structural and magnetic properties of Co–Zn spinel ferrite nanoparticles

Abstract

Highlights: • Co–Zn ferrite nanoparticles were examined before and after γ-irradiation. • Single phase cubic spinel structure of Co–Zn was confirmed by XRD data. • The grain size was reported in the range of 52–62 nm after γ-irradiation. • Ms, Hc, n{sub B} were reported to be increased after gamma irradiation. - Abstract: In this work, the structural and magnetic properties of Co{sub 1−x}Zn{sub x}Fe{sub 2}O{sub 4} (0.0 ≤ x ≤ 1.0) ferrite nanoparticles were studied before and after gamma irradiation. The as-synthesized samples of Co–Zn ferrite nanoparticles prepared by sol–gel auto-combustion technique were analysed by XRD which suggested the single phase; cubic spinel structure of the material. Crystal defects produced in the spinel lattice were studied before and after Co{sup 60} γ-irradiation in a gamma cell with a dose rate of 0.1 Mrad/h in order to report the changes in structural and magnetic properties of the Co–Zn ferrite nanoparticles. The average crystallite size (t), lattice parameter (α) and other structural parameters of gamma-irradiated and un-irradiated Co{sub 1−x}Zn{sub x}Fe{sub 2}O{sub 4} spinel ferrite system was calculated from XRD data. The morphological characterizations were performed using scanning electron microscopy (SEM). The magnetic properties were measured using pulse field hysteresis loop tracermore » by applying magnetic field of 1000 Oe, and the analysis of data obtained revealed that the magnetic property such as saturation magnetization (Ms), coecivity (Hc), magneton number (n{sub B}) etc. magnetic parameters were increased after irradiation.« less

Authors:
 [1];  [2];  [3]
  1. Milind College of Science, Aurangabad 431004, (M.S.) India (India)
  2. Vivekanand Arts, Sardar Dalipsingh Commerce and Science College, Aurangabad 431004, (M.S.) India (India)
  3. Department of Physics, Dr. Babasaheb Ambedkar Marathwada University, Aurangabad 431004, (M.S.) India (India)
Publication Date:
OSTI Identifier:
22420834
Resource Type:
Journal Article
Journal Name:
Materials Research Bulletin
Additional Journal Information:
Journal Volume: 63; Other Information: Copyright (c) 2014 Elsevier Science B.V., Amsterdam, The Netherlands, All rights reserved.; Country of input: International Atomic Energy Agency (IAEA); Journal ID: ISSN 0025-5408
Country of Publication:
United States
Language:
English
Subject:
36 MATERIALS SCIENCE; COBALT COMPOUNDS; CRYSTAL DEFECTS; DATA ANALYSIS; DOSE RATES; FERRITES; GAMMA RADIATION; GRAIN SIZE; IRRADIATION; LATTICE PARAMETERS; MAGNETIC FIELDS; MAGNETIC PROPERTIES; MAGNETIZATION; NANOPARTICLES; RADIATION EFFECTS; SCANNING ELECTRON MICROSCOPY; SPINELS; X-RAY DIFFRACTION; ZINC COMPOUNDS

Citation Formats

Raut, Anil V., E-mail: nano9993@gmail.com, Kurmude, D. V., Shengule, D. R., and Jadhav, K. M. Effect of gamma irradiation on the structural and magnetic properties of Co–Zn spinel ferrite nanoparticles. United States: N. p., 2015. Web. doi:10.1016/J.MATERRESBULL.2014.11.051.
Raut, Anil V., E-mail: nano9993@gmail.com, Kurmude, D. V., Shengule, D. R., & Jadhav, K. M. Effect of gamma irradiation on the structural and magnetic properties of Co–Zn spinel ferrite nanoparticles. United States. doi:10.1016/J.MATERRESBULL.2014.11.051.
Raut, Anil V., E-mail: nano9993@gmail.com, Kurmude, D. V., Shengule, D. R., and Jadhav, K. M. Sun . "Effect of gamma irradiation on the structural and magnetic properties of Co–Zn spinel ferrite nanoparticles". United States. doi:10.1016/J.MATERRESBULL.2014.11.051.
@article{osti_22420834,
title = {Effect of gamma irradiation on the structural and magnetic properties of Co–Zn spinel ferrite nanoparticles},
author = {Raut, Anil V., E-mail: nano9993@gmail.com and Kurmude, D. V. and Shengule, D. R. and Jadhav, K. M.},
abstractNote = {Highlights: • Co–Zn ferrite nanoparticles were examined before and after γ-irradiation. • Single phase cubic spinel structure of Co–Zn was confirmed by XRD data. • The grain size was reported in the range of 52–62 nm after γ-irradiation. • Ms, Hc, n{sub B} were reported to be increased after gamma irradiation. - Abstract: In this work, the structural and magnetic properties of Co{sub 1−x}Zn{sub x}Fe{sub 2}O{sub 4} (0.0 ≤ x ≤ 1.0) ferrite nanoparticles were studied before and after gamma irradiation. The as-synthesized samples of Co–Zn ferrite nanoparticles prepared by sol–gel auto-combustion technique were analysed by XRD which suggested the single phase; cubic spinel structure of the material. Crystal defects produced in the spinel lattice were studied before and after Co{sup 60} γ-irradiation in a gamma cell with a dose rate of 0.1 Mrad/h in order to report the changes in structural and magnetic properties of the Co–Zn ferrite nanoparticles. The average crystallite size (t), lattice parameter (α) and other structural parameters of gamma-irradiated and un-irradiated Co{sub 1−x}Zn{sub x}Fe{sub 2}O{sub 4} spinel ferrite system was calculated from XRD data. The morphological characterizations were performed using scanning electron microscopy (SEM). The magnetic properties were measured using pulse field hysteresis loop tracer by applying magnetic field of 1000 Oe, and the analysis of data obtained revealed that the magnetic property such as saturation magnetization (Ms), coecivity (Hc), magneton number (n{sub B}) etc. magnetic parameters were increased after irradiation.},
doi = {10.1016/J.MATERRESBULL.2014.11.051},
journal = {Materials Research Bulletin},
issn = {0025-5408},
number = ,
volume = 63,
place = {United States},
year = {2015},
month = {3}
}