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Title: Synthesis and magnetic properties of Ta/NdFeB-based composite microwires

Abstract

Magnetic NdFeB-based microwire composites have been prepared by the direct current magnetron sputtering technique in a specifically designed sputtering chamber for thin-film deposition in wire geometry. As substrate wire material, we have employed steel and Ta. Annealing of the substrate wires during the deposition process was performed by ohmic heating through the application of a direct current. Samples were characterized by means of vibrating sample magnetometry (VSM) and scanning electron microscopy. Best properties have been encountered when using Ta wires as core (substrate) material. The VSM data show a dramatic impact of the current applied during the deposition process on the magnetic properties. For higher current values, i.e., higher annealing temperatures, the wires exhibit a reversal process that is typical for a two-phase system. Moreover, an increase of the coercive field (and remanent magnetization) is observed, which is ascribed to a modification of the magnetic phase present in the sample due to the annealing. We find an indication for the formation of a magnetic easy-axis direction which is azimuthally oriented around the wire axis.

Authors:
; ;  [1]; ; ; ;  [2]
  1. Physics and Materials Science Research Unit, University of Luxembourg, 162 Avenue de la Faïencerie, L-1511 Luxembourg, Grand Duchy of Luxembourg (Luxembourg)
  2. Science and Analysis of Materials (SAM), Centre de Recherche Public—Gabriel Lippmann, 41, rue du Brill, L-4422 Belvaux, Grand Duchy of Luxembourg (Luxembourg)
Publication Date:
OSTI Identifier:
22410065
Resource Type:
Journal Article
Journal Name:
Journal of Applied Physics
Additional Journal Information:
Journal Volume: 117; Journal Issue: 17; Other Information: (c) 2015 AIP Publishing LLC; Country of input: International Atomic Energy Agency (IAEA); Journal ID: ISSN 0021-8979
Country of Publication:
United States
Language:
English
Subject:
75 CONDENSED MATTER PHYSICS, SUPERCONDUCTIVITY AND SUPERFLUIDITY; ANNEALING; DEPOSITION; DIRECT CURRENT; HEATING; IRON BORIDES; MAGNETIC PROPERTIES; MAGNETIZATION; NEODYMIUM COMPOUNDS; SCANNING ELECTRON MICROSCOPY; SPUTTERING; STEELS; SUBSTRATES; SYNTHESIS; TANTALUM; TEMPERATURE DEPENDENCE; THIN FILMS; VIBRATING SAMPLE MAGNETOMETERS; WIRES

Citation Formats

Szary, P., E-mail: philipp.szary@uni.lu, Périgo, E. A., Michels, A., Luciu, I., Duday, D., Wirtz, T., and Choquet, P. Synthesis and magnetic properties of Ta/NdFeB-based composite microwires. United States: N. p., 2015. Web. doi:10.1063/1.4917058.
Szary, P., E-mail: philipp.szary@uni.lu, Périgo, E. A., Michels, A., Luciu, I., Duday, D., Wirtz, T., & Choquet, P. Synthesis and magnetic properties of Ta/NdFeB-based composite microwires. United States. doi:10.1063/1.4917058.
Szary, P., E-mail: philipp.szary@uni.lu, Périgo, E. A., Michels, A., Luciu, I., Duday, D., Wirtz, T., and Choquet, P. Thu . "Synthesis and magnetic properties of Ta/NdFeB-based composite microwires". United States. doi:10.1063/1.4917058.
@article{osti_22410065,
title = {Synthesis and magnetic properties of Ta/NdFeB-based composite microwires},
author = {Szary, P., E-mail: philipp.szary@uni.lu and Périgo, E. A. and Michels, A. and Luciu, I. and Duday, D. and Wirtz, T. and Choquet, P.},
abstractNote = {Magnetic NdFeB-based microwire composites have been prepared by the direct current magnetron sputtering technique in a specifically designed sputtering chamber for thin-film deposition in wire geometry. As substrate wire material, we have employed steel and Ta. Annealing of the substrate wires during the deposition process was performed by ohmic heating through the application of a direct current. Samples were characterized by means of vibrating sample magnetometry (VSM) and scanning electron microscopy. Best properties have been encountered when using Ta wires as core (substrate) material. The VSM data show a dramatic impact of the current applied during the deposition process on the magnetic properties. For higher current values, i.e., higher annealing temperatures, the wires exhibit a reversal process that is typical for a two-phase system. Moreover, an increase of the coercive field (and remanent magnetization) is observed, which is ascribed to a modification of the magnetic phase present in the sample due to the annealing. We find an indication for the formation of a magnetic easy-axis direction which is azimuthally oriented around the wire axis.},
doi = {10.1063/1.4917058},
journal = {Journal of Applied Physics},
issn = {0021-8979},
number = 17,
volume = 117,
place = {United States},
year = {2015},
month = {5}
}