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Title: Study of various Sb{sub 2}S{sub 3} nanostructures synthesized by simple solvothermal and hydrothermal methods

Abstract

Controlling the size and morphology of the antimony sulfide nanostructures is important for photocatalytic and photovoltaic applications. Herein, we report a systematic approach to synthesize various nanostructures of antimony sulfide. Based on simple solvothermal and hydrothermal routes antimony sulfide nanorods have been synthesized at different temperatures. The size of the nanorods and the morphology of the constituent nano-units, in the form of nanorods, dumbbell and sphere have been controlled by adjusting the temperature. The changes have been confirmed by scanning electron microscope and transmission electron microscope analysis. - Highlights: • We prepared dumbbell structured Sb{sub 2}Sb{sub 3} by simple solvothermal and hydrothermal method. • Investigated the importance of bath temperature on the formation of various structures. • Growth mechanism of dumbbell like structured Sb{sub 2}S{sub 3} nanorods was estimated.

Authors:
 [1];  [2];  [3];  [1]
  1. Department of Chemistry, Yeungnam University, Gyeongsan, Gyeongbuk 712–749 (Korea, Republic of)
  2. (India)
  3. Department of Physics, Coimbatore Institute of Technology, Coimbatore (India)
Publication Date:
OSTI Identifier:
22403545
Resource Type:
Journal Article
Journal Name:
Materials Characterization
Additional Journal Information:
Journal Volume: 95; Other Information: Copyright (c) 2014 Elsevier Science B.V., Amsterdam, The Netherlands, All rights reserved.; Country of input: International Atomic Energy Agency (IAEA); Journal ID: ISSN 1044-5803
Country of Publication:
United States
Language:
English
Subject:
36 MATERIALS SCIENCE; 77 NANOSCIENCE AND NANOTECHNOLOGY; ANTIMONY SULFIDES; CRYSTAL GROWTH; HYDROTHERMAL SYNTHESIS; MORPHOLOGY; NANOSTRUCTURES; PHOTOCATALYSIS; PHOTOVOLTAIC EFFECT; SCANNING ELECTRON MICROSCOPY; TEMPERATURE DEPENDENCE; TRANSMISSION ELECTRON MICROSCOPY

Citation Formats

Senthil, T.S., Department of Physics, Erode Sengunthar Engineering College, Erode, Muthukumarasamy, N., and Kang, Misook, E-mail: mskang@ynu.ac.kr. Study of various Sb{sub 2}S{sub 3} nanostructures synthesized by simple solvothermal and hydrothermal methods. United States: N. p., 2014. Web. doi:10.1016/J.MATCHAR.2014.06.014.
Senthil, T.S., Department of Physics, Erode Sengunthar Engineering College, Erode, Muthukumarasamy, N., & Kang, Misook, E-mail: mskang@ynu.ac.kr. Study of various Sb{sub 2}S{sub 3} nanostructures synthesized by simple solvothermal and hydrothermal methods. United States. doi:10.1016/J.MATCHAR.2014.06.014.
Senthil, T.S., Department of Physics, Erode Sengunthar Engineering College, Erode, Muthukumarasamy, N., and Kang, Misook, E-mail: mskang@ynu.ac.kr. Mon . "Study of various Sb{sub 2}S{sub 3} nanostructures synthesized by simple solvothermal and hydrothermal methods". United States. doi:10.1016/J.MATCHAR.2014.06.014.
@article{osti_22403545,
title = {Study of various Sb{sub 2}S{sub 3} nanostructures synthesized by simple solvothermal and hydrothermal methods},
author = {Senthil, T.S. and Department of Physics, Erode Sengunthar Engineering College, Erode and Muthukumarasamy, N. and Kang, Misook, E-mail: mskang@ynu.ac.kr},
abstractNote = {Controlling the size and morphology of the antimony sulfide nanostructures is important for photocatalytic and photovoltaic applications. Herein, we report a systematic approach to synthesize various nanostructures of antimony sulfide. Based on simple solvothermal and hydrothermal routes antimony sulfide nanorods have been synthesized at different temperatures. The size of the nanorods and the morphology of the constituent nano-units, in the form of nanorods, dumbbell and sphere have been controlled by adjusting the temperature. The changes have been confirmed by scanning electron microscope and transmission electron microscope analysis. - Highlights: • We prepared dumbbell structured Sb{sub 2}Sb{sub 3} by simple solvothermal and hydrothermal method. • Investigated the importance of bath temperature on the formation of various structures. • Growth mechanism of dumbbell like structured Sb{sub 2}S{sub 3} nanorods was estimated.},
doi = {10.1016/J.MATCHAR.2014.06.014},
journal = {Materials Characterization},
issn = {1044-5803},
number = ,
volume = 95,
place = {United States},
year = {2014},
month = {9}
}