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Title: Phase stability, porosity distribution and microstructural evolution of amorphous Al{sub 50}Ti{sub 50} powders consolidated by electrical resistance sintering

Abstract

The effect of intensity and duration of the electrical resistance sintering process on the phase stability, porosity distribution and microstructural evolution of Al{sub 50}Ti{sub 50} amorphous powders is studied. The phase transformations during the consolidation process were determined by X-ray diffraction. The porosity distribution was observed by optical and scanning electron microscopy. The amorphous phase is partially transformed to the crystalline phase during the sintering process, and formation of AlTi and AlTi{sub 3} intermetallic compounds occurs for temperatures higher than 300 °C. Finally, it is observed that the compacts core have lower porosity and a higher tendency to the amorphous-crystalline phase transformation than the periphery.

Authors:
; ;  [1];  [2]
  1. University of Seville, Department of Mechanical and Materials Engineering, ETSI, Camino de los Descubrimientos s/n, Seville, 41092 (Spain)
  2. University of Huelva, Department of Chemistry and Materials Science, ETSI, Campus La Rábida, Carretera Palos s/n, Palos de la Frontera, Huelva, 21819 (Spain)
Publication Date:
OSTI Identifier:
22391340
Resource Type:
Journal Article
Resource Relation:
Journal Name: AIP Conference Proceedings; Journal Volume: 1653; Journal Issue: 1; Conference: APMAS 2014: 4. International Congress in Advances in Applied Physics and Materials Science, Fethiye (Turkey), 24-27 Apr 2014; Other Information: (c) 2015 AIP Publishing LLC; Country of input: International Atomic Energy Agency (IAEA)
Country of Publication:
United States
Language:
English
Subject:
36 MATERIALS SCIENCE; ALUMINIUM; AMORPHOUS STATE; ELECTRIC CONDUCTIVITY; INTERMETALLIC COMPOUNDS; MICROSTRUCTURE; PHASE STABILITY; PHASE TRANSFORMATIONS; POROSITY; POWDERS; SCANNING ELECTRON MICROSCOPY; SINTERING; TEMPERATURE DEPENDENCE; TITANIUM; X-RAY DIFFRACTION

Citation Formats

Urban, P., E-mail: purban@us.es, Montes, J. M., Cintas, J., and Cuevas, F. G., E-mail: fgcuevas@dqcm.uhu.es. Phase stability, porosity distribution and microstructural evolution of amorphous Al{sub 50}Ti{sub 50} powders consolidated by electrical resistance sintering. United States: N. p., 2015. Web. doi:10.1063/1.4914291.
Urban, P., E-mail: purban@us.es, Montes, J. M., Cintas, J., & Cuevas, F. G., E-mail: fgcuevas@dqcm.uhu.es. Phase stability, porosity distribution and microstructural evolution of amorphous Al{sub 50}Ti{sub 50} powders consolidated by electrical resistance sintering. United States. doi:10.1063/1.4914291.
Urban, P., E-mail: purban@us.es, Montes, J. M., Cintas, J., and Cuevas, F. G., E-mail: fgcuevas@dqcm.uhu.es. Mon . "Phase stability, porosity distribution and microstructural evolution of amorphous Al{sub 50}Ti{sub 50} powders consolidated by electrical resistance sintering". United States. doi:10.1063/1.4914291.
@article{osti_22391340,
title = {Phase stability, porosity distribution and microstructural evolution of amorphous Al{sub 50}Ti{sub 50} powders consolidated by electrical resistance sintering},
author = {Urban, P., E-mail: purban@us.es and Montes, J. M. and Cintas, J. and Cuevas, F. G., E-mail: fgcuevas@dqcm.uhu.es},
abstractNote = {The effect of intensity and duration of the electrical resistance sintering process on the phase stability, porosity distribution and microstructural evolution of Al{sub 50}Ti{sub 50} amorphous powders is studied. The phase transformations during the consolidation process were determined by X-ray diffraction. The porosity distribution was observed by optical and scanning electron microscopy. The amorphous phase is partially transformed to the crystalline phase during the sintering process, and formation of AlTi and AlTi{sub 3} intermetallic compounds occurs for temperatures higher than 300 °C. Finally, it is observed that the compacts core have lower porosity and a higher tendency to the amorphous-crystalline phase transformation than the periphery.},
doi = {10.1063/1.4914291},
journal = {AIP Conference Proceedings},
number = 1,
volume = 1653,
place = {United States},
year = {Mon Mar 30 00:00:00 EDT 2015},
month = {Mon Mar 30 00:00:00 EDT 2015}
}