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Title: Synthesis and crystal structure of (S, S, S, S)-N, N′-bis[N-(P-toluenesulfonamido)-1,2-diphenylethyl]ethylenediamine

Abstract

(S, S, S, S)-N,N′-bis[N-(p-toluenesulfonamido)-1,2-diphenylethyl] ethylenediamine (C{sub 44}H{sub 46}N{sub 4}O{sub 4}S{sub 2}), has been synthesized and structurally characterized by elemental analysis, {sup 1}H-NMR, MS, IR and single-crystal X-ray diffraction. The title compound contains four chiral centers with C atoms in S configuration. Molecules are connected to one another by hydrogen bonds between sulfonamide nitrogen and sulfonyl oxygen to form chains alone a axis.

Authors:
; ; ;  [1]
  1. Hangzhou Normal University, College of Material Chemistry and Chemical Engineering (China)
Publication Date:
OSTI Identifier:
22311405
Resource Type:
Journal Article
Resource Relation:
Journal Name: Crystallography Reports; Journal Volume: 58; Journal Issue: 7; Other Information: Copyright (c) 2013 Pleiades Publishing, Inc.; http://www.springer-ny.com; Country of input: International Atomic Energy Agency (IAEA)
Country of Publication:
United States
Language:
English
Subject:
75 CONDENSED MATTER PHYSICS, SUPERCONDUCTIVITY AND SUPERFLUIDITY; 36 MATERIALS SCIENCE; AMINES; CARBON; CRYSTAL STRUCTURE; INFRARED SPECTRA; MONOCRYSTALS; NUCLEAR MAGNETIC RESONANCE; STRUCTURAL CHEMICAL ANALYSIS; STYRENE; SULFONAMIDES; TOLUENE; X-RAY DIFFRACTION

Citation Formats

Liu, X.-G., Zhang, T., Hu, Y.-Y., and Shen, L., E-mail: shenchem@hotmail.com. Synthesis and crystal structure of (S, S, S, S)-N, N′-bis[N-(P-toluenesulfonamido)-1,2-diphenylethyl]ethylenediamine. United States: N. p., 2013. Web. doi:10.1134/S1063774513080063.
Liu, X.-G., Zhang, T., Hu, Y.-Y., & Shen, L., E-mail: shenchem@hotmail.com. Synthesis and crystal structure of (S, S, S, S)-N, N′-bis[N-(P-toluenesulfonamido)-1,2-diphenylethyl]ethylenediamine. United States. doi:10.1134/S1063774513080063.
Liu, X.-G., Zhang, T., Hu, Y.-Y., and Shen, L., E-mail: shenchem@hotmail.com. Sun . "Synthesis and crystal structure of (S, S, S, S)-N, N′-bis[N-(P-toluenesulfonamido)-1,2-diphenylethyl]ethylenediamine". United States. doi:10.1134/S1063774513080063.
@article{osti_22311405,
title = {Synthesis and crystal structure of (S, S, S, S)-N, N′-bis[N-(P-toluenesulfonamido)-1,2-diphenylethyl]ethylenediamine},
author = {Liu, X.-G. and Zhang, T. and Hu, Y.-Y. and Shen, L., E-mail: shenchem@hotmail.com},
abstractNote = {(S, S, S, S)-N,N′-bis[N-(p-toluenesulfonamido)-1,2-diphenylethyl] ethylenediamine (C{sub 44}H{sub 46}N{sub 4}O{sub 4}S{sub 2}), has been synthesized and structurally characterized by elemental analysis, {sup 1}H-NMR, MS, IR and single-crystal X-ray diffraction. The title compound contains four chiral centers with C atoms in S configuration. Molecules are connected to one another by hydrogen bonds between sulfonamide nitrogen and sulfonyl oxygen to form chains alone a axis.},
doi = {10.1134/S1063774513080063},
journal = {Crystallography Reports},
number = 7,
volume = 58,
place = {United States},
year = {Sun Dec 15 00:00:00 EST 2013},
month = {Sun Dec 15 00:00:00 EST 2013}
}