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Title: Spectroscopic studies and crystal structure of (E)-N Prime -(2-hydroxy-3-methoxybenzylidene)isonicotinohydrazide

Abstract

The structure of compound has also been examined cyrstallographically. It crystallizes in the monoclinic space group P2{sub 1}/c with a = 7.673(1), b = 16.251(2), c = 10.874(1) A, {beta} = 110.42(1) Degree-Sign , V = 1270.7(3) A{sup 3}, D{sub x} = 1.418 g cm{sup -3}, R{sub 1} = 0.0349 and wR{sub 2} = 0.0935 [I > 2{sigma}(I)], respectively. The title compound has been synthesized from the reaction of isonicotinohydrazide with 2-hydroxy-3-methoxybenzaldehyde. It has been characterized by using elemental analysis, MS, IR, {sup 1}H NMR, {sup 13}C NMR and UV-Visible spectroscopic techniques.

Authors:
;  [1];  [2];  [3]
  1. Canakkaale Onsekiz Mart University, Department of Chemistry, Faculty of Science and Arts (Turkey)
  2. Ankara University, Department of Physics, Faculty of Science (Turkey)
  3. Near East University, Ataturk Faculty of Education (Turkey)
Publication Date:
OSTI Identifier:
22156466
Resource Type:
Journal Article
Resource Relation:
Journal Name: Crystallography Reports; Journal Volume: 58; Journal Issue: 1; Other Information: Copyright (c) 2013 Pleiades Publishing, Ltd.; Country of input: International Atomic Energy Agency (IAEA)
Country of Publication:
United States
Language:
English
Subject:
36 MATERIALS SCIENCE; MONOCLINIC LATTICES; NUCLEAR MAGNETIC RESONANCE; SPACE GROUPS

Citation Formats

Ozay, H., E-mail: havaozay@hotmail.com, Yildiz, M., Unver, H., and Kiraz, A.. Spectroscopic studies and crystal structure of (E)-N Prime -(2-hydroxy-3-methoxybenzylidene)isonicotinohydrazide. United States: N. p., 2013. Web. doi:10.1134/S1063774513010264.
Ozay, H., E-mail: havaozay@hotmail.com, Yildiz, M., Unver, H., & Kiraz, A.. Spectroscopic studies and crystal structure of (E)-N Prime -(2-hydroxy-3-methoxybenzylidene)isonicotinohydrazide. United States. doi:10.1134/S1063774513010264.
Ozay, H., E-mail: havaozay@hotmail.com, Yildiz, M., Unver, H., and Kiraz, A.. Tue . "Spectroscopic studies and crystal structure of (E)-N Prime -(2-hydroxy-3-methoxybenzylidene)isonicotinohydrazide". United States. doi:10.1134/S1063774513010264.
@article{osti_22156466,
title = {Spectroscopic studies and crystal structure of (E)-N Prime -(2-hydroxy-3-methoxybenzylidene)isonicotinohydrazide},
author = {Ozay, H., E-mail: havaozay@hotmail.com and Yildiz, M. and Unver, H. and Kiraz, A.},
abstractNote = {The structure of compound has also been examined cyrstallographically. It crystallizes in the monoclinic space group P2{sub 1}/c with a = 7.673(1), b = 16.251(2), c = 10.874(1) A, {beta} = 110.42(1) Degree-Sign , V = 1270.7(3) A{sup 3}, D{sub x} = 1.418 g cm{sup -3}, R{sub 1} = 0.0349 and wR{sub 2} = 0.0935 [I > 2{sigma}(I)], respectively. The title compound has been synthesized from the reaction of isonicotinohydrazide with 2-hydroxy-3-methoxybenzaldehyde. It has been characterized by using elemental analysis, MS, IR, {sup 1}H NMR, {sup 13}C NMR and UV-Visible spectroscopic techniques.},
doi = {10.1134/S1063774513010264},
journal = {Crystallography Reports},
number = 1,
volume = 58,
place = {United States},
year = {Tue Jan 15 00:00:00 EST 2013},
month = {Tue Jan 15 00:00:00 EST 2013}
}