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Title: Efficient graphite ring heater suitable for diamond-anvil cells to 1300 K

Journal Article · · Review of Scientific Instruments
DOI:https://doi.org/10.1063/1.4792395· OSTI ID:22105415
; ;  [1];  [1]
  1. Department of Geology and Geophysics, Yale University, New Haven, Connecticut 06511 (United States)

In order to generate homogeneous high temperatures at high pressures, a ring-shaped graphite heater has been developed to resistively heat diamond-anvil cell (DAC) samples up to 1300 K. By putting the heater in direct contact with the diamond anvils, this graphite heater design features the following advantages: (1) efficient heating: sample can be heated to 1300 K while the DAC body temperature remains less than 800 K, eliminating the requirement of a special alloy for the DAC; (2) compact design: the sample can be analyzed with in situ measurements, e.g., x-ray, optical, and electrical probes are possible. In particular, the side access of the heater allows for radial x-ray diffraction (XRD) measurements in addition to traditional axial XRD.

OSTI ID:
22105415
Journal Information:
Review of Scientific Instruments, Vol. 84, Issue 2; Other Information: (c) 2013 American Institute of Physics; Country of input: International Atomic Energy Agency (IAEA); ISSN 0034-6748
Country of Publication:
United States
Language:
English

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