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Title: Quantitative studies on inner interfaces in conical metal joints using hard x-ray inline phase contrast radiography

Journal Article · · Review of Scientific Instruments
DOI:https://doi.org/10.1063/1.3495966· OSTI ID:22055741
 [1]; ;  [2];  [3]
  1. Institute for Materials Science, Technical University of Berlin, EB 13, Strasse des 17, Juni 135, D-10623 Berlin (Germany)
  2. Clinic for Oral and Maxifacial Surgery, Charite University Medicine, Augustenburger Platz 1, D-13353 Berlin (Germany)
  3. European Synchrotron Radiation Facility, 6 rue Jules Horowitz, BP 220, F-38043 Grenoble (France)

Quantitative investigation of micrometer and submicrometer gaps between joining metal surfaces is applied to conical plug-socket connections in dental titanium implants. Microgaps of widths well beyond the resolving power of industrial x-ray systems are imaged by synchrotron phase contrast radiography. Furthermore, by using an analytical model for the relatively simple sample geometry and applying it to numerical forward simulations of the optical Fresnel propagation, we show that quantitative measurements of the microgap width down to 0.1 {mu}m are possible. Image data recorded at the BAMline (BESSY-II light source, Germany) are presented, with the resolving power of the imaging system being 4 {mu}m in absorption mode and {approx}14 {mu}m in phase contrast mode (z{sub 2}=0.74 m). Thus, phase contrast radiography, combined with numerical forward simulations, is capable of measuring the widths of gaps that are two orders of magnitude thinner than the conventional detection limit.

OSTI ID:
22055741
Journal Information:
Review of Scientific Instruments, Vol. 81, Issue 10; Other Information: (c) 2010 American Institute of Physics; Country of input: International Atomic Energy Agency (IAEA); ISSN 0034-6748
Country of Publication:
United States
Language:
English