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Title: The belok station for protein crystallography on the synchrotron radiation beam from the bending magnet in the Sibir-2 storage ring

Abstract

Design modifications made in the initial project of the Belok station in the Sibir-2 storage ring and the alignment and calibration methods are considered. The main operating parameters of the station are reported. Protein single crystals in a capillary at T = 293 K and without a capillary at T = 95 K, powders (angular resolution {delta}2{theta} = 0.04 deg.), and nanocrystalline Na and Cl{sub 2} precipitates (sizes, shape, and orientation) in electron-irradiated NaCl crystals have been investigated. The problem of focusing of a short-wavelength synchrotron radiation beam with sagittal bending of the second crystal in the double-crystal monochromator at a limited source-to-sample distance is solved in the Belok project.

Authors:
; ; ; ; ; ;  [1]
  1. Russian Academy of Sciences, Shubnikov Institute of Crystallography (Russian Federation)
Publication Date:
OSTI Identifier:
21090934
Resource Type:
Journal Article
Resource Relation:
Journal Name: Crystallography Reports; Journal Volume: 52; Journal Issue: 2; Other Information: DOI: 10.1134/S1063774507020320; Copyright (c) 2007 Nauka/Interperiodica; Article Copyright (c) 2007 Pleiades Publishing, Inc; Country of input: International Atomic Energy Agency (IAEA)
Country of Publication:
United States
Language:
English
Subject:
75 CONDENSED MATTER PHYSICS, SUPERCONDUCTIVITY AND SUPERFLUIDITY; CALIBRATION; CRYSTALLOGRAPHY; ELECTRON BEAMS; IRRADIATION; MAGNETS; MONOCRYSTALS; NANOSTRUCTURES; PRECIPITATION; PROTEINS; STORAGE RINGS; SYNCHROTRON RADIATION; TEMPERATURE RANGE 0065-0273 K; TEMPERATURE RANGE 0273-0400 K

Citation Formats

Kheiker, D. M., E-mail: kheiker@ns.crys.ras.ru, Kovalchuk, M. V., Shilin, Yu. N., Shishkov, V. A., Sulyanov, S. N., Dorovatovskii, P. V., and Rusakov, A. A.. The belok station for protein crystallography on the synchrotron radiation beam from the bending magnet in the Sibir-2 storage ring. United States: N. p., 2007. Web. doi:10.1134/S1063774507020320.
Kheiker, D. M., E-mail: kheiker@ns.crys.ras.ru, Kovalchuk, M. V., Shilin, Yu. N., Shishkov, V. A., Sulyanov, S. N., Dorovatovskii, P. V., & Rusakov, A. A.. The belok station for protein crystallography on the synchrotron radiation beam from the bending magnet in the Sibir-2 storage ring. United States. doi:10.1134/S1063774507020320.
Kheiker, D. M., E-mail: kheiker@ns.crys.ras.ru, Kovalchuk, M. V., Shilin, Yu. N., Shishkov, V. A., Sulyanov, S. N., Dorovatovskii, P. V., and Rusakov, A. A.. Thu . "The belok station for protein crystallography on the synchrotron radiation beam from the bending magnet in the Sibir-2 storage ring". United States. doi:10.1134/S1063774507020320.
@article{osti_21090934,
title = {The belok station for protein crystallography on the synchrotron radiation beam from the bending magnet in the Sibir-2 storage ring},
author = {Kheiker, D. M., E-mail: kheiker@ns.crys.ras.ru and Kovalchuk, M. V. and Shilin, Yu. N. and Shishkov, V. A. and Sulyanov, S. N. and Dorovatovskii, P. V. and Rusakov, A. A.},
abstractNote = {Design modifications made in the initial project of the Belok station in the Sibir-2 storage ring and the alignment and calibration methods are considered. The main operating parameters of the station are reported. Protein single crystals in a capillary at T = 293 K and without a capillary at T = 95 K, powders (angular resolution {delta}2{theta} = 0.04 deg.), and nanocrystalline Na and Cl{sub 2} precipitates (sizes, shape, and orientation) in electron-irradiated NaCl crystals have been investigated. The problem of focusing of a short-wavelength synchrotron radiation beam with sagittal bending of the second crystal in the double-crystal monochromator at a limited source-to-sample distance is solved in the Belok project.},
doi = {10.1134/S1063774507020320},
journal = {Crystallography Reports},
number = 2,
volume = 52,
place = {United States},
year = {Thu Mar 15 00:00:00 EDT 2007},
month = {Thu Mar 15 00:00:00 EDT 2007}
}